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1. 发明授权

US08476047B2 Extraction solvents derived from oil for alcohol removal in extractive fermentation 有权
标题翻译：萃取溶剂中的萃取溶剂，用于萃取发酵中的酒精去除
公开(公告)号：US08476047B2
公开(公告)日：2013-07-02
申请号：US13692254
申请日：2012-12-03
申请人： Keith H. Burlew , Robert Dicosimo , Michael Charles Grady
发明人： Keith H. Burlew , Robert Dicosimo , Michael Charles Grady
IPC分类号： C12P7/02 , C12P7/16
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： In an alcohol fermentation process, oil derived from biomass is hydrolyzed into an extractant available for in situ removal of a product alcohol such as butanol from a fermentation broth. The glycerides in the oil can be catalytically (e.g., enzymatically) hydrolyzed into free fatty acids, which form a fermentation product extractant having a partition coefficient for a product alcohol greater than a partition coefficient of the oil of the biomass for the product alcohol. Oil derived from a feedstock of an alcohol fermentation process can be hydrolyzed by contacting the feedstock including the oil with one or more enzymes whereby at least a portion of the oil is hydrolyzed into free fatty acids forming a fermentation product extractant, or the oil can be separated from the feedstock prior to the feedstock being fed to a fermentation vessel, and the separated oil can be contacted with the enzymes to form the fermentation product extractant. The fermentation product extractant can be contacted with a fermentation broth for in situ removal of a product alcohol.
摘要翻译：在酒精发酵过程中，将来自生物质的油水解成可从发酵液中原位除去产物醇如丁醇的萃取剂。油中的甘油酯可以催化（例如，酶促）水解成游离脂肪酸，其形成产物醇的分配系数大于产物醇的生物质油的分配系数的发酵产物萃取剂。由酒精发酵方法的原料得到的油可以通过使包含油的原料与一种或多种酶接触来水解，由此至少一部分油被水解成形成发酵产物萃取剂的游离脂肪酸，或者油可以是在原料进料到发酵容器之前与原料分离，并且分离的油可以与酶接触以形成发酵产物萃取剂。发酵产物萃取剂可与发酵液接触，用于原位除去产物醇。

2. 发明申请

US20120208246A1 PRODUCTION OF ALCOHOL ESTERS AND IN SITU PRODUCT REMOVAL DURING ALCOHOL FERMENTATION 有权
标题翻译：在酒精发酵期间生产酒精产品和脱除产品
公开(公告)号：US20120208246A1
公开(公告)日：2012-08-16
申请号：US13193147
申请日：2011-07-28
申请人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
发明人： Douglas Robert Anton , Stephane Francois Bazzana , Keith H. Burlew , Jelena Cirakovic , Robert Dicosimo , Bruce A. Diner , Michael Charles Grady , Brian Michael Roesch , Francis J. Woerner
IPC分类号： C12P7/64 , C12N9/16 , A23K1/06 , C12P7/16
CPC分类号： A23K1/007 , A23K10/12 , A23K10/38 , C12P7/16 , C12P7/62 , C12P7/649 , C12P2203/00 , Y02E50/10 , Y02E50/13 , Y02P60/873
摘要： An alcohol fermentation process and composition that includes production of alcohol esters by esterification of product alcohol in a fermentation medium with a carboxylic acid (e.g., fatty acid) and a catalyst (e.g., lipase) capable of esterifying the product alcohol, such as butanol, with the carboxylic acid to form the alcohol esters. The alcohol esters can be extracted from the fermentation medium, and the product alcohol recovered from the alcohol esters. The carboxylic acid can also serve as an extractant for removal of the alcohol esters from the fermentation medium.
摘要翻译：醇发酵方法和组合物，其包括通过在发酵培养基中与产物醇与羧酸（例如，脂肪酸）和能够酯化产物醇（例如丁醇）的催化剂（例如脂肪酶）酯化产生醇酯，与羧酸形成醇酯。醇酯可以从发酵培养基中提取，并从醇酯中回收产物醇。羧酸也可以用作从发酵培养基中除去醇酯的提取剂。

3. 发明申请

US20120035398A1 PROCESS TO REMOVE PRODUCT ALCOHOL FROM A FERMENTATION BY VAPORIZATION UNDER VACUUM 有权
标题翻译：通过真空蒸发从发酵中除去产品酒精的方法
公开(公告)号：US20120035398A1
公开(公告)日：2012-02-09
申请号：US13023134
申请日：2011-02-08
申请人： Michael Charles Grady , William D. Parten , Robert W. Sylvester , Joseph J. Zaher
发明人： Michael Charles Grady , William D. Parten , Robert W. Sylvester , Joseph J. Zaher
IPC分类号： C07C31/12 , B01D3/10 , B01D3/34
CPC分类号： C07C29/80 , B01D3/002 , B01D53/1475 , B01D53/1487 , B01D2251/306 , B01D2251/606 , B01D2252/2025 , B01D2252/20484 , B01D2252/20489 , B01D2257/504 , B01D2257/704 , B01D2257/708 , B01D2257/80 , C07C29/76 , Y02C10/06 , Y02P20/152 , Y02P70/34 , C07C31/12
摘要： A fermentation liquid feed including water and a product alcohol and optionally CO2 is at least partially vaporized such that a vapor stream is produced. The vapor stream is contacted with an absorption liquid under suitable conditions wherein an amount of the product alcohol is absorbed. The portion of the vapor stream that is absorbed can include an amount of each of the water, the product alcohol and optionally the CO2. The temperature at the onset of the absorption of the vapor stream into the absorption liquid can be greater than the temperature at the onset of condensation of the vapor stream in the absence of the absorption liquid. The product alcohol can be separated from the absorption liquid whereby the absorption liquid is regenerated. The absorption liquid can include a water soluble organic molecule such as an amine.
摘要翻译：包括水和产物醇和任选的CO 2的发酵液体进料至少部分蒸发，使得产生蒸汽流。在合适的条件下，蒸气流与吸收液体接触，其中产物醇的量被吸收。被吸收的蒸汽流的部分可以包括一定量的水，产物醇和任选的CO 2。蒸汽流吸收到吸收液体中开始吸收的温度可以大于在不存在吸收液体的情况下蒸气流冷凝开始时的温度。可以将产物醇与吸收液分离，由此吸收液体被再生。吸收液体可以包括水溶性有机分子如胺。

4. 发明申请

US20110312043A1 EXTRACTION SOLVENTS DERIVED FROM OIL FOR ALCOHOL REMOVAL IN EXTRACTIVE FERMENTATION 有权
标题翻译：从油中提取的提取溶剂用于提取发酵中的酒精去除
公开(公告)号：US20110312043A1
公开(公告)日：2011-12-22
申请号：US13162643
申请日：2011-06-17
申请人： KEITH H. BURLEW , ROBERT DICOSIMO , MICHAEL CHARLES GRADY
发明人： KEITH H. BURLEW , ROBERT DICOSIMO , MICHAEL CHARLES GRADY
IPC分类号： C12P7/16 , C12P7/64 , C12P13/02 , C12N9/18 , C12P7/40 , C12P7/62 , C12N9/16 , C12N9/20 , C12P1/00 , C12P7/02
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： In an alcohol fermentation process, oil derived from biomass is hydrolyzed into an extractant available for in situ removal of a product alcohol such as butanol from a fermentation broth. The glycerides in the oil can be catalytically (e.g., enzymatically) hydrolyzed into free fatty acids, which form a fermentation product extractant having a partition coefficient for a product alcohol greater than a partition coefficient of the oil of the biomass for the product alcohol. Oil derived from a feedstock of an alcohol fermentation process can be hydrolyzed by contacting the feedstock including the oil with one or more enzymes whereby at least a portion of the oil is hydrolyzed into free fatty acids forming a fermentation product extractant, or the oil can be separated from the feedstock prior to the feedstock being fed to a fermentation vessel, and the separated oil can be contacted with the enzymes to form the fermentation product extractant. The fermentation product extractant can be contacted with a fermentation broth for in situ removal of a product alcohol.
摘要翻译：在酒精发酵过程中，将来自生物质的油水解成可从发酵液中原位除去产物醇如丁醇的萃取剂。油中的甘油酯可以催化（例如，酶促）水解成游离脂肪酸，其形成产物醇的分配系数大于产物醇的生物质油的分配系数的发酵产物萃取剂。由酒精发酵工艺的原料得到的油可以通过使包含油的原料与一种或多种酶接触来水解，由此至少一部分油被水解成形成发酵产物萃取剂的游离脂肪酸，或者油可以是在原料进料到发酵容器之前与原料分离，并且分离的油可以与酶接触以形成发酵产物萃取剂。发酵产物萃取剂可与发酵液接触，用于原位除去产物醇。

5. 发明申请

US20110288344A1 RECOVERY OF BUTANOL FROM A MIXTURE OF BUTANOL, WATER, AND AN ORGANIC EXTRACTANT 有权
标题翻译：丁醇从丁醇，水和有机提取物的混合物中恢复
公开(公告)号：US20110288344A1
公开(公告)日：2011-11-24
申请号：US12948945
申请日：2010-11-18
申请人： MICHAEL CHARLES GRADY , William D. Parten , Bruce Vrana , Yihui Tom Xu
发明人： MICHAEL CHARLES GRADY , William D. Parten , Bruce Vrana , Yihui Tom Xu
IPC分类号： C07C29/84
CPC分类号： C12P7/16 , C07C29/86 , Y02E50/10 , C07C31/12
摘要： A process for recovering butanol from a mixture comprising a water-immiscible organic extractant, water, butanol, and optionally a non-condensable gas, is provided. The butanol is selected from 1-butanol, 2-butanol, isobutanol, and mixtures thereof. An overhead stream from a first distillation column is condensed to recover a mixed condensate. An entrainer is added to at least one appropriate process stream or vessel such that the mixed condensate comprises sufficient entrainer to provide phase separation of the organic and the aqueous phases to provide for recovery of the butanol.
摘要翻译：提供了一种从包含与水不混溶的有机萃取剂，水，丁醇和任选的不可冷凝气体的混合物中回收丁醇的方法。丁醇选自1-丁醇，2-丁醇，异丁醇及其混合物。将来自第一蒸馏塔的塔顶物流冷凝以回收混合的冷凝物。将夹带剂加入到至少一个合适的工艺流或容器中，使得混合的冷凝物包含足够的夹带剂以提供有机相和水相的相分离以提供丁醇的回收。

6. 发明授权

US07897676B1 Two component coating compositions and coatings produced therefrom 有权
标题翻译：双组分涂料组合物和由其制备的涂料
公开(公告)号：US07897676B1
公开(公告)日：2011-03-01
申请号：US12945935
申请日：2010-11-15
申请人： Robert John Barsotti , Laura Ann Lewin , Carl Brent Douglas , Michael Charles Grady , Donald Albert Paquet, Jr.
发明人： Robert John Barsotti , Laura Ann Lewin , Carl Brent Douglas , Michael Charles Grady , Donald Albert Paquet, Jr.
IPC分类号： C08G18/42 , C08G18/08 , C08L83/00 , C08L51/00 , C08F290/06 , C08F220/06 , C08F283/00 , C08F8/30 , C08C19/00
CPC分类号： C08K5/0025 , C08F2/001 , C08F2/06 , C08F8/30 , C08F2800/20 , C08G18/6229 , C08G18/792 , C08L79/00 , C08L2312/00 , C09D133/04 , C09D133/14 , C08L33/06 , C08L2666/20 , C08F2220/1866
摘要： The present invention is directed to two component coating compositions that cure under ambient conditions and more particularly to those having low VOC (volatile organic content) that are suitable for use in automotive refinish and Original Equipment Manufacturing (OEM) applications. The coating composition includes crosslinkable and crosslinking components, wherein the crosslinkable component includes a low polydispersity, low molecular weight copolymer having on an average 2 to 25 functional groups, such as hydroxyl, carboxyl, acetoacetoxy, primary and secondary amine, and epoxy. The copolymer is polymerized from a monomer mixture that includes one or more non-functional acrylate monomers and one or more functional methacrylate monomers provided with the functional groups. The crosslinking component includes polyisocyanate, polyamine, ketimine, melamine, epoxy, polyacid or a combination thereof. The invention is also directed to coating produced from the coating composition.
摘要翻译：本发明涉及在环境条件下固化的二组分涂料组合物，更具体地涉及适用于汽车修补漆和原始设备制造（OEM）应用的具有低VOC（挥发性有机物含量）的组分涂料组合物。涂料组合物包括可交联和交联组分，其中可交联组分包括具有平均2至25个官能团的低分子量低分子量共聚物，例如羟基，羧基，乙酰乙酰氧基，伯胺和仲胺和环氧基。共聚物由包括一种或多种非官能丙烯酸酯单体和一个或多个配有官能团的官能甲基丙烯酸酯单体的单体混合物聚合。交联组分包括多异氰酸酯，多胺，酮亚胺，三聚氰胺，环氧树脂，多元酸或它们的组合。本发明还涉及由涂料组合物制备的涂料。

7. 发明授权

US06989421B2 Two component coating compositions and coatings produced therefrom 有权
标题翻译：双组分涂料组合物和由其制备的涂料
公开(公告)号：US06989421B2
公开(公告)日：2006-01-24
申请号：US10612495
申请日：2003-07-02
申请人： Michael Charles Grady
发明人： Michael Charles Grady
IPC分类号： C08F8/30
CPC分类号： C09D133/14 , B05D3/0254 , B05D7/16 , C08G18/6229 , C08G18/792 , C08L2312/00 , C09D175/04 , C08L2666/20 , C08L2666/02
摘要： The present invention is directed to two component coating compositions that cure under ambient conditions and more particularly to those having low VOC (volatile organic content) that are suitable for use in automotive refinish and Original Equipment Manufacturing (OEM) applications. The coating composition includes crosslinkable and crosslinking components, wherein the crosslinkable component includes a low polydispersity, low molecular weight copolymer having on an average 2 to 25 crosslinkable functional groups, such as hydroxyl, acetoacetoxy, carboxyl, epoxy, primary amine and secondary amine. The copolymer is polymerized from a monomer mixture that includes one or more non-functional methacrylate monomers and one or more functional acrylate monomers provided with the functional groups. The crosslinking component includes polyisocyanate, polyamine, epoxy, polyacid, ketimine, melamine, or a combination thereof. The invention is also directed to coating produced from the coating composition.
摘要翻译：本发明涉及在环境条件下固化的二组分涂料组合物，更具体地涉及适用于汽车修补漆和原始设备制造（OEM）应用的具有低VOC（挥发性有机物含量）的组分涂料组合物。涂料组合物包括可交联和交联组分，其中可交联组分包括具有平均2至25个可交联官能团的低分子量低分子量共聚物，例如羟基，乙酰乙酰氧基，羧基，环氧基，伯胺和仲胺。共聚物由包含一种或多种非官能的甲基丙烯酸酯单体和一个或多个提供有官能团的官能丙烯酸酯单体的单体混合物聚合。交联组分包括多异氰酸酯，多胺，环氧，多酸，酮亚胺，三聚氰胺或其组合。本发明还涉及由涂料组合物制备的涂料。

8. 发明授权

US08563788B2 Recovery of butanol from a mixture of butanol, water, and an organic extractant 有权
公开(公告)号：US08563788B2
公开(公告)日：2013-10-22
申请号：US13611125
申请日：2012-09-12
申请人： Michael Charles Grady , William D Parten , Bruce M Vrana , Yihui Tom Xu , Joseph J Zaher
发明人： Michael Charles Grady , William D Parten , Bruce M Vrana , Yihui Tom Xu , Joseph J Zaher
IPC分类号： C07C29/80 , C07C29/84
CPC分类号： C12P7/16 , C07C29/80 , Y02E50/10 , C07C31/12
摘要： A process for recovering butanol from a mixture comprising a water-immiscible organic extractant, water, butanol, and optionally a non-condensable gas, is provided. The butanol is selected from 1-butanol, 2-butanol, isobutanol, and mixtures thereof. The extractant comprises at least one solvent selected from the group consisting of C7 to C22 fatty alcohols, C7 to C22 fatty acids, esters of C7 to C22 fatty acids, C7 to C22 fatty aldehydes, and mixtures thereof.

9. 发明申请

US20130089900A1 Extraction Solvents Derived from Oil for Alcohol Removal in Extractive Fermentation 有权
公开(公告)号：US20130089900A1
公开(公告)日：2013-04-11
申请号：US13692254
申请日：2012-12-03
申请人： Keith H. Burlew , Robert Dicosimo , Michael Charles Grady
发明人： Keith H. Burlew , Robert Dicosimo , Michael Charles Grady
IPC分类号： C12P7/16
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： In an alcohol fermentation process, oil derived from biomass is hydrolyzed into an extractant available for in situ removal of a product alcohol such as butanol from a fermentation broth. The glycerides in the oil can be catalytically (e.g., enzymatically) hydrolyzed into free fatty acids, which form a fermentation product extractant having a partition coefficient for a product alcohol greater than a partition coefficient of the oil of the biomass for the product alcohol. Oil derived from a feedstock of an alcohol fermentation process can be hydrolyzed by contacting the feedstock including the oil with one or more enzymes whereby at least a portion of the oil is hydrolyzed into free fatty acids forming a fermentation product extractant, or the oil can be separated from the feedstock prior to the feedstock being fed to a fermentation vessel, and the separated oil can be contacted with the enzymes to form the fermentation product extractant. The fermentation product extractant can be contacted with a fermentation broth for in situ removal of a product alcohol.

10. 发明申请

US20130001062A1 RECOVERY OF BUTANOL FROM A MIXTURE OF BUTANOL, WATER, AND AN ORGANIC EXTRACTANT 有权
标题翻译：丁醇从丁醇，水和有机提取物的混合物中恢复
公开(公告)号：US20130001062A1
公开(公告)日：2013-01-03
申请号：US13611125
申请日：2012-09-12
申请人： MICHAEL CHARLES GRADY , William D. Parten , Bruce M. Vrana , Yihui Tom Xu , Joseph J. Zaher
发明人： MICHAEL CHARLES GRADY , William D. Parten , Bruce M. Vrana , Yihui Tom Xu , Joseph J. Zaher
IPC分类号： C07C29/84 , B01D3/14
CPC分类号： C12P7/16 , C07C29/80 , Y02E50/10 , C07C31/12
摘要： A process for recovering butanol from a mixture comprising a water-immiscible organic extractant, water, butanol, and optionally a non-condensable gas, is provided. The butanol is selected from 1-butanol, 2-butanol, isobutanol, and mixtures thereof. The extractant comprises at least one solvent selected from the group consisting of C7 to C22 fatty alcohols, C7 to C22 fatty acids, esters of C7 to C22 fatty acids, C7 to C22 fatty aldehydes, and mixtures thereof.
摘要翻译：提供了一种从包含与水不混溶的有机萃取剂，水，丁醇和任选的不可冷凝气体的混合物中回收丁醇的方法。丁醇选自1-丁醇，2-丁醇，异丁醇及其混合物。萃取剂包含至少一种选自C7至C22脂肪醇，C7至C22脂肪酸，C7至C22脂肪酸酯，C7至C22脂肪醛及其混合物的溶剂。

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