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    • 3. 发明授权
    • Method of preparation of the surfaces of products made of iron alloys,
preceding the process of hot-dip aluminizing
    • 在热浸镀铝工艺之前,制备由铁合金制成的产品表面的方法
    • US4158710A
    • 1979-06-19
    • US865780
    • 1977-12-29
    • Adam GierekLech BajkaDanuta Adamczyk
    • Adam GierekLech BajkaDanuta Adamczyk
    • C23C2/12C23C1/08C23C1/12
    • C23C2/12
    • The work-pieces are mechanically cleaned, degreased and washed, and then etched in an aqueous solution containing 0.5-1.0% by weight of citric acid, and 16-24% by weight of hydrochloric acid, having a temperature of 15.degree.-30.degree. C., preferably of 20.degree.-25.degree. C., for the time of 1-20 minutes, preferably 2-5 minutes, whereafter the work-pieces are neutralized in an aqueous ammonia solution having a concentration not exceeding 1% by weight, at a temperature of 15.degree.-25.degree. C., in a time not shorter than 1 minute. After being washed in water at a temperature not exceeding 35.degree. C. in a time not shorter than 1 minute, they are dipped in an agitated aqueous solution of the flux, containing 1.8-2.5% by weight of potassium fluoride, 0.8-1.5% by weight of sodium fluoride, and 1.5-3.0% by weight of potassium fluorozirconate, having a temperature of 40.degree.-80.degree. C. After at least two minutes of holding in the flux, the work-pieces are dried and finally dipped in a melt of aluminum or alloys thereof. Alternatively a flux having composition 1.5-2.0% by weight of potassium fluoride, 1.5-2.0% by weight of sodium fluoride, 6.0-10.0% by weight of sodium tetraborate and 2.5-5.0% by weight of acetic acid, having a temperature of 15.degree.-40.degree. C. may be used, for a period not shorter than 2 minutes.
    • 将工件机械地清洗,脱脂和洗涤,然后在含有0.5-1.0重量%柠檬酸和16-24重量%盐酸的水溶液中蚀刻,温度为15-30℃ 优选20°-25℃,时间为1-20分钟,优选2-5分钟,然后将工件在浓度不超过1重量%的氨水溶液中中和, 在15°-25℃的温度下,在不短于1分钟的时间内。 在不超过35℃的温度下在不短于1分钟的时间内在水中洗涤后,将其浸入搅拌的助熔剂水溶液中,该溶液含有1.8-2.5重量%的氟化钾,0.8-1.5重量% 的氟化钠和1.5-3.0重量%的氟锆酸钾,温度为40-80℃。在焊剂中保持至少两分钟后,将工件干燥并最终浸入 铝的熔化或其合金。 或者,具有组成为氟化钾1.5-2.0重量%,氟化钠1.5-2.0重量%,四硼酸钠6.0-10.0重量%和乙酸2.5-5.0重量%的助熔剂,温度为15 可以使用-40℃-40℃,时间不短于2分钟。