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1. 发明授权

US08524808B2 Radiation curable compositions 有权
标题翻译：辐射固化组合物
公开(公告)号：US08524808B2
公开(公告)日：2013-09-03
申请号：US11791411
申请日：2005-11-12
申请人： Rainer Hoefer , Laurence Druene , Jean-Marc Ballin , Morgan Garinet
发明人： Rainer Hoefer , Laurence Druene , Jean-Marc Ballin , Morgan Garinet
IPC分类号： C08L63/00
CPC分类号： C08G59/1466 , C09D5/002 , C09D5/02 , C09D163/10
摘要： The invention is a radiation curable coating composition containing epoxyacrylate formed by ring opening reaction between (meth)acrylic acid and a self-dispersing epoxy resin in an aqueous system.
摘要翻译：本发明是一种包含环氧丙烯酸酯的可辐射固化涂料组合物，其通过在（水）体系中的（甲基）丙烯酸和自分散环氧树脂之间的开环反应形成。

2. 发明申请

US20130109784A1 AQUEOUS RADIATION-CURABLE EPOXY ACRYLATE DISPERSIONS 审中-公开
标题翻译：水性可辐射固化环氧丙烯酸酯分散体
公开(公告)号：US20130109784A1
公开(公告)日：2013-05-02
申请号：US13497457
申请日：2010-09-13
申请人： Juergen Baro , Laurence Druene , Paul Birnbrich , Hans-Josef Thomas
发明人： Juergen Baro , Laurence Druene , Paul Birnbrich , Hans-Josef Thomas
IPC分类号： C09D163/00
CPC分类号： C09D163/00 , C08G59/1466 , C08G59/182 , C08G2650/58 , C08L63/10 , C08L71/02 , C09D5/022 , C09D5/027 , C08L2666/22
摘要： The invention relates to aqueous radiation-hardenable epoxy acrylate dispersions comprising (a) an epoxy acrylate resin (P*) with at least two acrylate groups per molecule, wherein at 25 degrees Celsius, said epoxy acrylate resin is not self-disperging in water; and (b) a dispergator (D*) with at least one acrylate group per molecule, wherein said dispersions can be produced by converting, in a first step (i), in the presence of a catalyst if need be, one or several compounds (A) selected from the group of non-ionic compounds having a HLB value of less than 12, and containing at least two oxirane groups per molecule, with one or several compounds (B) selected from the group of non-ionic compounds having a HLB value in the range from 12 to 20, and which contain at least one h-acid group (ZH) per molecule. The compounds (A) and (B) are employed at an equivalence ratio EpO (A):ZH (B) in the range from 1.3:1 to 400:1, and in a second step (ii), the reactive mixture thus obtained is converted, in the presence of a catalyst if need be, with one or several non-ionic compounds having a HLB value of less than 12, and containing at least two oxirane groups per molecule (compounds A), and with one or several compounds (C) selected from the group of non-ionic compounds having a HLB value of less than 12, and which contain at least two H-acid groups. The compounds (A) and (C) are employed at an equivalence ratio EpO (A):ZH (C) in the range from 1.1:1 to 20:1. In a third step (iii), the reactive mixture thus obtained is converted, in the presence of a catalyst if need be, with acrylic acid by ring opening of all epoxy groups. In a fourth step (iv), the reactive mixture thus obtained is disperged in water.
摘要翻译：本发明涉及含水辐射可硬化环氧丙烯酸酯分散体，其包含（a）每分子具有至少两个丙烯酸酯基团的环氧丙烯酸酯树脂（P *），其中在25℃下所述环氧丙烯酸酯树脂在水中不自分散; 和（b）每分子具有至少一个丙烯酸酯基团的分散剂（D *），其中所述分散体可以通过在催化剂存在下，在第一步骤（i）中转化来制备，如果需要，可以使用一种或几种化合物（A），其选自HLB值小于12的非离子化合物，并且每分子含有至少两个环氧乙烷基团，其中一种或几种化合物（B）选自具有 HLB值为12〜20，每分子含有至少一个h酸基（ZH）。化合物（A）和（B）以当量比EpO（A）：ZH（B）在1.3:1至400:1的范围内使用，在第二步（ⅱ）中，由此得到的反应混合物在催化剂存在的情况下，如果需要，可以与一种或多种HLB值小于12的非离子化合物，每分子含有至少两个环氧乙烷基团（化合物A）和一种或多种化合物（C）选自HLB值小于12的非离子化合物，并含有至少两个H酸基团。化合物（A）和（C）以当量比EpO（A）：ZH（C）在1.1:1至20:1的范围内使用。在第三步骤（iii）中，如果需要的话，在催化剂存在下，如此得到的反应混合物通过所有环氧基的开环与丙烯酸一起转化。在第四步骤（iv）中，将由此获得的反应混合物分散在水中。

3. 发明申请

US20090099279A1 Acrylated Polyaminoamide (III) 审中-公开
标题翻译：丙烯酸聚氨基酰胺（III）
公开(公告)号：US20090099279A1
公开(公告)日：2009-04-16
申请号：US12252127
申请日：2008-10-15
申请人： Antoine Carroy , Jean-Marc Ballin , Laurence Druene , Morgan Garinet , Douglas Rhubright
发明人： Antoine Carroy , Jean-Marc Ballin , Laurence Druene , Morgan Garinet , Douglas Rhubright
IPC分类号： C08F2/46 , C08G63/91 , C08G73/06
CPC分类号： C08F290/06 , C08F283/04 , C08F290/061 , C09D11/101
摘要： Radiation-curable acrylated polyaminoamides obtainable by Michael addition of polyaminoamides containing terminal amine groups (A) and polyolester acrylates (B), the molar ratio of the acrylate groups in the polyolester acrylates (B) to the aminohydrogen groups in the polyaminoamides (A) being at least 1:1, characterized in that polyolester acrylates (B) are acrylated addition products of propylene oxide onto trimethylol propane, are suitable as radiation-curable compounds for the production of coatings.
摘要翻译：可通过迈克尔加入含有末端胺基（A）和多酯酯丙烯酸酯（B）的聚氨基酰胺获得的可辐射固化的丙烯酸酯化聚氨基酰胺，多胺酯丙烯酸酯（B）中的丙烯酸酯基与聚氨基酰胺（A）中的氨基氢的摩尔比为至少1：1，其特征在于多醇酯丙烯酸酯（B）是环氧丙烷在三羟甲基丙烷上的丙烯酸酯化加成产物，适合作为用于制备涂料的可辐射固化化合物。

4. 发明申请

US20120059081A1 RESINS COMPRISING ACRYLATE GROUPS 审中-公开
标题翻译：包含丙烯酸酯树脂的树脂
公开(公告)号：US20120059081A1
公开(公告)日：2012-03-08
申请号：US13320336
申请日：2010-04-30
申请人： Stefan Busch , Juergen Baro , Laurence Druene , Jean-Marc Ballin
发明人： Stefan Busch , Juergen Baro , Laurence Druene , Jean-Marc Ballin
IPC分类号： C09D177/06 , C09D11/10 , C08J3/28 , C08G69/48
CPC分类号： C08G69/26 , C08G69/28 , C08G69/34 , C08G69/48 , C08L77/06 , C08L77/08 , C09D11/101 , C09D177/08
摘要： The invention relates to resins comprising acrylate groups that are liquid at 25° C., obtained in that polycarboxylic acids (a) comprising at least 2 carboxyl groups and at least 2 C atoms per molecule are converted in a first stage with polyamines (b) comprising at least 2 amino groups and at least 2 C atoms per molecule, such that an intermediate compound (z) results, said compound being terminated by carboxyl groups, and said compound (z) being functionalized in a second stage, such that the free carboxyl groups thereof are provided with one or more (meth)acrylate groups in one or more stages, said resins being suitable as radiation-curing compounds for producing coatings.
摘要翻译：本发明涉及包含在25℃下为液体的丙烯酸酯基团的树脂，其获得方法是在第一阶段用多胺（b）将每分子中含有至少2个羧基和至少2个C原子的多元羧酸（a）每个分子包含至少2个氨基和至少2个C原子，使得得到中间体化合物（z），所述化合物被羧基封端，所述化合物（z）在第二阶段中被官能化，其羧基在一个或多个阶段中具有一个或多个（甲基）丙烯酸酯基，所述树脂适用于制备涂料的辐射固化化合物。

5. 发明申请

US20090099278A1 Acrylated Polyaminoamide (II) 审中-公开
标题翻译：丙烯酸聚氨基酰胺（II）
公开(公告)号：US20090099278A1
公开(公告)日：2009-04-16
申请号：US12252113
申请日：2008-10-15
申请人： Antoine Carroy , Jean-Marc Ballin , Laurence Druene , Morgan Garinet , Douglas Rhubright , Stefan Busch
发明人： Antoine Carroy , Jean-Marc Ballin , Laurence Druene , Morgan Garinet , Douglas Rhubright , Stefan Busch
IPC分类号： C09D11/02 , C08F283/04 , C09D177/06
CPC分类号： C08F283/04 , C08G69/26 , C08G69/34 , C08G73/028 , C08G81/00 , C08L79/02 , C09D11/101
摘要： Radiation-curable acrylated polyaminoamides obtainable by Michael addition of polyaminoamides containing terminal amine groups (A) and polyolester acrylates (B), the molar ratio of the acrylate groups in the polyolester acrylates (B) to the aminohydrogen groups in the polyaminoamides (A) being at least 1:1, characterized in that the polyaminoamides have an amine value above 115, are suitable as radiation-curable compounds for the production of coatings.
摘要翻译：可通过迈克尔加入含有末端胺基（A）和多酯酯丙烯酸酯（B）的聚氨基酰胺获得的可辐射固化的丙烯酸酯化聚氨基酰胺，多胺酯丙烯酸酯（B）中的丙烯酸酯基与聚氨基酰胺（A）中的氨基氢的摩尔比为至少1：1，其特征在于聚氨基酰胺具有高于115的胺值，适合作为用于制备涂料的可辐射固化化合物。

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