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    • 3. 发明授权
    • Method for preparing polyacrylonitrile-based polymer for preparation of carbon fiber using microwave and method for preparing carbon fiber using the same
    • 使用微波制备用于制备碳纤维的聚丙烯腈类聚合物的方法及使用其制备碳纤维的方法
    • US08685361B2
    • 2014-04-01
    • US13461241
    • 2012-05-01
    • Kap-Seung YangSung-Ho LeeHyang-Hoon ChaeDong-Hun Lee
    • Kap-Seung YangSung-Ho LeeHyang-Hoon ChaeDong-Hun Lee
    • D01F9/12
    • D01F9/225C08L33/18C08L2203/12
    • Disclosed therein is a method for preparing a polyacrylonitrile-based polymer for preparation of carbon fiber having a melting point controlled by selecting an optimal energy of microwave, and a method for preparing a carbon fiber through melt spinning using the preparation method for polyacrylonitrile-based polymer. The present invention uses microwave to control the properties of the polyacrylonitrile-based polymer in a simplified way and prepare the polymer optimized for preparation of carbon fiber precursor through melt spinning for a short polymerization time, and provides a means for mass production of the polyacrylonitrile-based polymer being suitable for melt spinning at a temperature lower than the stabilization temperature and acquiring properties adequate to preparation of carbon fiber through stabilization. Hence, the present invention is expected to contribute to mass production of high-performance carbon fibers at reduced cost.
    • 本发明公开了一种制备通过选择微波最佳能量来控制熔点的碳纤维的聚丙烯腈系聚合物的制造方法以及使用聚丙烯腈类聚合物的制备方法通过熔融纺丝制备碳纤维的方法 。 本发明使用微波以简单的方式控制聚丙烯腈类聚合物的性能,并通过熔融纺丝制备优化用于制备碳纤维前体的聚合物,聚合时间短,并提供了用于大量生产聚丙烯腈 - 基于聚合物适合于在低于稳定温度的温度下熔融纺丝,并通过稳定性获得足以制备碳纤维的性能。 因此,本发明预期有助于以低成本大量生产高性能碳纤维。