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1. 发明授权

US4006274A 2,4,6-Tris(carbamoylmethylamino)-1,3,5,-s-triazine 失效
标题翻译： 2,4,6-三（氨基甲酰基甲基氨基）-1,3,5，-s-三嗪
公开(公告)号：US4006274A
公开(公告)日：1977-02-01
申请号：US615015
申请日：1975-09-19
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： C07D251/70 , B05D3/02
CPC分类号： C07D251/70
摘要： 2,4,6-Tris(carbamoylmethylamino)-1,3,5-s-triazine, abbreviated TCMT, is prepared by the reaction of 2,4,6-tris(carbethoxymethylamino)-1,3,5-s-triazine with ammonia. The methylol derivative of TCMT is prepared and applied to cotton textiles and blends of cotton and polyester to impart wrinkle recovery thereto.
摘要翻译：通过2,4,6-三（乙酰氧基甲基氨基）-1,3,5-s-三嗪的反应制备2,4,6-三（氨基甲酰基甲基氨基）-1,3,5-s-三嗪，缩写为TCMT 与氨。制备TCMT的羟甲基衍生物，并应用于棉纺织物和棉和聚酯的共混物以赋予皱纹恢复性。

2. 发明授权

US4055720A Diaminotrihalopropyl triazines: and their methylol derivatives 失效
标题翻译：二氨基三卤丙基三嗪：及其羟甲基衍生物
公开(公告)号：US4055720A
公开(公告)日：1977-10-25
申请号：US689771
申请日：1976-05-25
申请人： Leon H. Chance , Judy D. Timpa
发明人： Leon H. Chance , Judy D. Timpa
IPC分类号： C07D251/18 , D06M13/358 , C07D251/48
CPC分类号： C07D251/18 , D06M13/358 , Y10S428/921
摘要： 2,4-Diamino-6(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-diamino-6(3,3,3-trichloro-1-propyl)-1,3,5-triazine were prepared by the reaction of the corresponding methyl or ethyl .gamma.-tribromo-butyrate or methyl or ethyl .gamma.-trichlorobutyrate with biguanide. The N-methylol derivatives of the diaminotrihalopropyl triazines were prepared by the reaction of the triazines with aqueous formaldehyde. Two pure tetramethylol derivatives were prepared, namely: 2,4-bis[bis(hydroxymethyl)amino]-6-(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-bis[bis(hydroxymethyl)amino]-6-(3,3,3-trichloro-1-propyl)-1,3,5-triazine. The tetramethylol derivatives were used to impart durable flame retardancy and wrinkle recovery to cellulosic textiles, particularly to cotton. Flame-retardancy was also imparted to wool and to blends of cotton and polyester.
摘要翻译： 2,4-二氨基-6（3,3,3-三溴-1-丙基）-1,3,5-三嗪和2,4-二氨基-6（3,3,3-三氯-1-丙基） - 通过相应的甲基或乙基γ-三溴丁酸酯或γ-三氯丁酸乙酯与双胍反应制备1,3,5-三嗪。二氨基三卤代丙基三嗪的N-羟甲基衍生物通过三嗪与甲醛水溶液的反应来制备。制备两种纯的四羟甲基衍生物，即2,4-双[双（羟甲基）氨基] -6-（3,3,3-三溴-1-丙基）-1,3,5-三氮杂和2,4 双[双（羟甲基）氨基] -6-（3,3,3-三氯-1-丙基）-1,3,5-三嗪。使用四羟甲基衍生物赋予纤维素纺织品特别是棉花持久的阻燃性和皱纹恢复性。还赋予了羊毛和棉和聚酯的混合物的阻燃性。

3. 发明授权

UST100601I4 Compositions and processes for producing flame retardant textile materials based on methylolaminotrihalopropyl triazines and antimony oxides 失效
标题翻译：基于甲基丙烯酰氧基丙烯酸酯和抗氧化剂生产阻燃纺织材料的组合物和方法
公开(公告)号：UST100601I4
公开(公告)日：1981-05-05
申请号：US134014
申请日：1980-03-26
申请人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
发明人： Leon H. Chance , Judy D. Timpa , George L. Drake, Jr.
IPC分类号： D06M11/47 , D06M13/358 , D06M13/44 , D06M9/00 , D06M13/34
CPC分类号： D06M11/47 , D06M13/358
摘要： The tetramethylol derivatives of 2,4-diamino-6(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-diamino-6(3,3,3-trichloro-1-propyl)-1,3,5-triazine, namely: 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-tribromo-1-propyl)-1,3,5-triazine and 2,4-bis[di(hydroxymethyl)amino]-6-(3,3,3-trichloro-1-propyl)-1,3,5-triazine, respectively, were used in combination with colloidal antimony oxides and or water emulsifying agents and suitable solvent to impart durable flame-retardancy to cellulosic materials, protein fibers such as wool, and to blends of cellulosic materials and synthetic fibers, particularly to cotton textiles or textiles composed of blends of cotton and polyester. Afterglow was eliminated by the use of small amounts of reactive phosphorus compounds.

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