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1. 发明申请

US20120283337A1 INORGANIC POROUS PARTICLES WITH STABILIZED MICROPORES 审中-公开
标题翻译：无机多孔微粒与稳定的微孔
公开(公告)号：US20120283337A1
公开(公告)日：2012-11-08
申请号：US13101178
申请日：2011-05-05
申请人： Mary Christine Brick , Joseph Salvatore Sedita , Mridula Nair
发明人： Mary Christine Brick , Joseph Salvatore Sedita , Mridula Nair
IPC分类号： C08K7/24 , B01J21/08 , B01J21/06 , B01J21/18 , C01F7/02 , A01P15/00 , C01G23/047 , C01G25/02 , C01B31/00 , C07F19/00 , A61K47/32 , A01N25/10 , B01J21/04 , C01B33/12
CPC分类号： C01G23/053 , B01J13/0056 , C01B13/32 , C01B33/18 , C01F7/36 , C01G25/02 , C01P2004/61 , C01P2006/16 , C01P2006/17 , C09C1/30 , C09C1/3607 , C09C1/407
摘要： Sol-gel inorganic porous particles can be formed with two set of pores with different average sizes. These inorganic porous particles are composed of an inorganic compound that provides an inorganic solid phase including an external particle surface. They also have a first set of pores wherein the pores have an average diameter of less than 100 nm and a second set of pores wherein the pores have an average diameter of at least 100 nm. The second set of pores contains stabilizing organic microgel particles. The first and second sets of pores are isolated from each other within the inorganic solid phase.
摘要翻译：溶胶 - 凝胶无机多孔颗粒可以用两组不同平均尺寸的孔形成。这些无机多孔颗粒由提供包含外部颗粒表面的无机固相的无机化合物组成。它们还具有第一组孔，其中孔具有小于100nm的平均直径和第二组孔，其中孔具有至少100nm的平均直径。第二组孔包含稳定的有机微粒凝胶颗粒。第一组和第二组孔隙在无机固相中彼此分离。

2. 发明申请

US20150111144A1 POLYMERIC COMPOSITE MATERIALS, MANUFACTURE, AND USES 有权
标题翻译：聚合物复合材料，制造和用途
公开(公告)号：US20150111144A1
公开(公告)日：2015-04-23
申请号：US14057251
申请日：2013-10-18
申请人： Mridula Nair , Joseph Salvatore Sedita , Peter David Rollinson
发明人： Mridula Nair , Joseph Salvatore Sedita , Peter David Rollinson
IPC分类号： G03G9/08
CPC分类号： G03G9/081 , C08J3/20 , C09D11/54 , G03G9/08 , G03G9/0819 , G03G9/0821 , G03G9/0825 , G03G9/087 , G03G9/08711 , G03G9/08755 , G03G9/08766 , G03G9/08777 , G03G9/08795 , G03G9/08797 , G03G9/093 , G03G9/09385 , G03G13/013 , G03G15/08
摘要： Composite materials such as composite particles have a solid non-elastomeric continuous phase made of an organic polymer having a glass transition temperature of at least 25° C. Dispersed within this solid non-elastomeric continuous phase are many multi-compartment porous chemically crosslinked elastomeric particles that have a mode particle size of at least 1 μm and up to and including 10 μm. The composite particles can be used as toner particles in electrophotographic imaging methods to provide fused toner images and especially stacked fused toner images.
摘要翻译：复合材料如复合颗粒具有由具有至少25℃的玻璃化转变温度的有机聚合物制成的固体非弹性连续相。在该固体非弹性体连续相中分散有许多多室多孔化学交联弹性体颗粒其模式粒度为至少1μm并且至多并包括10μm。复合颗粒可用作电子照相成像方法中的调色剂颗粒，以提供熔融的调色剂图像，特别是堆叠的熔融调色剂图像。

3. 发明申请

US20120282316A1 METHOD OF MAKING INORGANIC POROUS PARTICLES 有权
标题翻译：制造无机多孔颗粒的方法
公开(公告)号：US20120282316A1
公开(公告)日：2012-11-08
申请号：US13101185
申请日：2011-05-05
申请人： Mary Christine Brick , Joseph Salvatore Sedita , Joan Kay Williams , Mridula Nair
发明人： Mary Christine Brick , Joseph Salvatore Sedita , Joan Kay Williams , Mridula Nair
IPC分类号： A01N25/08 , B01J31/02 , A01P1/00 , B01J37/06 , C01B13/14 , A61K9/14 , B01J37/02
CPC分类号： C01B13/328 , A61K47/02 , C01B33/18 , C01F7/36 , C01G1/02 , C01G23/053 , C01G25/02 , C01P2004/61 , C01P2006/16 , C01P2006/17
摘要： Sol-gel inorganic porous particles are composed of an inorganic compound that provides an inorganic solid phase including an external particle surface. They also have a first set of pores wherein the pores have an average diameter of less than 100 nm and a second set of pores wherein the pores have an average diameter of at least 100 nm, which second set of pores contains stabilizing organic microgel particles. These inorganic porous particles are prepared using a first oil phase comprising a first water-immiscible aprotic solvent having a dielectric constant of less than 10 and having dissolved therein organic microgel particles. An aqueous phase comprising a polar solvent, an inorganic gel precursor, a catalyst, and a dispersing surfactant is neutralized to initiate condensation of the inorganic gel precursor. An oil-in-water emulsion is then formed with the organic microgel particles in the first oil phase, which is dispersed as first oil phase droplets in the aqueous phase. A second oil phase is combined with the oil-in-water emulsion with the second oil phase to form an oil-in-water-in-oil emulsion comprising the first oil phase droplets in the aqueous phase.
摘要翻译：溶胶凝胶无机多孔颗粒由提供包含外部颗粒表面的无机固相的无机化合物组成。它们还具有第一组孔，其中孔具有小于100nm的平均直径和第二组孔，其中孔具有至少100nm的平均直径，该第二组孔含有稳定的有机微粒凝胶颗粒。这些无机多孔颗粒使用第一油相制备，所述第一油相包含介电常数小于10并且溶解有机微粒凝胶颗粒的第一不溶于水的非质子传递溶剂。包含极性溶剂，无机凝胶前体，催化剂和分散表面活性剂的水相被中和以引发无机凝胶前体的缩合。然后与第一油相中的有机微粒凝胶颗粒形成水包油乳液，其作为第一油相液滴分散在水相中。将第二油相与水包油乳液与第二油相组合以形成包含在水相中的第一油相液滴的油包水包油乳液。

4. 发明授权

US09176405B2 Polymeric composite materials, manufacture, and uses 有权
标题翻译：聚合复合材料，制造和用途
公开(公告)号：US09176405B2
公开(公告)日：2015-11-03
申请号：US14057251
申请日：2013-10-18
申请人： Mridula Nair , Joseph Salvatore Sedita , Peter David Rollinson
发明人： Mridula Nair , Joseph Salvatore Sedita , Peter David Rollinson
IPC分类号： G03G9/00 , G03G9/097 , G03G9/087 , G03G9/08 , C08J3/20 , C09D11/54 , G03G9/093
CPC分类号： G03G9/081 , C08J3/20 , C09D11/54 , G03G9/08 , G03G9/0819 , G03G9/0821 , G03G9/0825 , G03G9/087 , G03G9/08711 , G03G9/08755 , G03G9/08766 , G03G9/08777 , G03G9/08795 , G03G9/08797 , G03G9/093 , G03G9/09385 , G03G13/013 , G03G15/08
摘要： Composite materials such as composite particles have a solid non-elastomeric continuous phase made of an organic polymer having a glass transition temperature of at least 25° C. Dispersed within this solid non-elastomeric continuous phase are many multi-compartment porous chemically crosslinked elastomeric particles that have a mode particle size of at least 1 μm and up to and including 10 μm. The composite particles can be used as toner particles in electrophotographic imaging methods to provide fused toner images and especially stacked fused toner images.
摘要翻译：复合材料如复合颗粒具有由具有至少25℃的玻璃化转变温度的有机聚合物制成的固体非弹性连续相。在该固体非弹性体连续相中分散有许多多室多孔化学交联弹性体颗粒其模式粒度为至少1μm并且至多并包括10μm。复合颗粒可用作电子照相成像方法中的调色剂颗粒，以提供熔融的调色剂图像，特别是堆叠的熔融调色剂图像。

5. 发明授权

US08394396B2 Method of making inorganic porous particles 有权
标题翻译：无机多孔颗粒的制备方法
公开(公告)号：US08394396B2
公开(公告)日：2013-03-12
申请号：US13101185
申请日：2011-05-05
申请人： Mary Christine Brick , Joseph Salvatore Sedita , Joan Kay Williams , Mridula Nair
发明人： Mary Christine Brick , Joseph Salvatore Sedita , Joan Kay Williams , Mridula Nair
IPC分类号： A01N25/26
CPC分类号： C01B13/328 , A61K47/02 , C01B33/18 , C01F7/36 , C01G1/02 , C01G23/053 , C01G25/02 , C01P2004/61 , C01P2006/16 , C01P2006/17
摘要： Sol-gel inorganic porous particles are composed of an inorganic compound that provides an inorganic solid phase including an external particle surface. They also have a first set of pores wherein the pores have an average diameter of less than 100 nm and a second set of pores wherein the pores have an average diameter of at least 100 nm, which second set of pores contains stabilizing organic microgel particles. These inorganic porous particles are prepared using a first oil phase comprising a first water-immiscible aprotic solvent having a dielectric constant of less than 10 and having dissolved therein organic microgel particles. An aqueous phase comprising a polar solvent, an inorganic gel precursor, a catalyst, and a dispersing surfactant is neutralized to initiate condensation of the inorganic gel precursor. An oil-in-water emulsion is then formed with the organic microgel particles in the first oil phase, which is dispersed as first oil phase droplets in the aqueous phase. A second oil phase is combined with the oil-in-water emulsion with the second oil phase to form an oil-in-water-in-oil emulsion comprising the first oil phase droplets in the aqueous phase.
摘要翻译：溶胶凝胶无机多孔颗粒由提供包含外部颗粒表面的无机固相的无机化合物组成。它们还具有第一组孔，其中孔具有小于100nm的平均直径和第二组孔，其中孔具有至少100nm的平均直径，该第二组孔含有稳定的有机微粒凝胶颗粒。这些无机多孔颗粒使用第一油相制备，所述第一油相包含介电常数小于10并且溶解有机微粒凝胶颗粒的第一不溶于水的非质子传递溶剂。包含极性溶剂，无机凝胶前体，催化剂和分散表面活性剂的水相被中和以引发无机凝胶前体的缩合。然后与第一油相中的有机微粒凝胶颗粒形成水包油乳液，其作为第一油相液滴分散在水相中。将第二油相与水包油乳液与第二油相组合以形成包含在水相中的第一油相液滴的油包水包油乳液。

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