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1. 发明申请

US20090042314A1 LANTHANIDE-DOPED NAYF4 NANOCRYSTALS, METHOD OF PREPARING AND USES THEREOF 有权
标题翻译：纳米DADED NAYF4纳米晶体，其制备方法及其用途
公开(公告)号：US20090042314A1
公开(公告)日：2009-02-12
申请号：US12125201
申请日：2008-05-22
申请人： John A. Capobianco , John-Christopher Boyer , Louis A. Cuccia , Fiorenzo Vetrone
发明人： John A. Capobianco , John-Christopher Boyer , Louis A. Cuccia , Fiorenzo Vetrone
IPC分类号： G01N33/53
CPC分类号： C01F17/0031 , B82Y15/00 , B82Y30/00 , C01P2002/52 , C01P2002/72 , C01P2002/77 , C01P2002/84 , C01P2002/86 , C01P2004/04 , C01P2004/22 , C01P2004/52 , C01P2004/64 , C09D11/037 , G01N33/588
摘要： The present invention relates to a method of preparing lanthanide-doped NaYF4 nanocrystals, the method comprising: (A) providing a first solution comprising a non-coordinating solvent, a fatty acid coordinating ligand, sodium trifluoroacetate, yttrium trifluoroacetate, a first doping lanthanide trifluoroacetate and a second doping lanthanide trifluoroacetate, and a second solution comprising the non-coordinating solvent and the fatty acid coordinating ligand, the first and second solutions being substantially free of water and oxygen; (B) in an inert atmosphere, slowly adding the first solution heated at a temperature between about 100° C. and about 150° C. to the second solution heated at temperature between about 290° C. and about 330° C., thereby producing a reaction mixture containing the nanocrystals; and (C) recovering the nanocrystals from the reaction mixture. The invention also relates to lanthanide-doped uniformly shaped cubic NaYF4 nanocrystals having an average particle size of at most about 50 nm with a standard deviation of at most about 15%. Finally, the invention also relates to methods of (A) identifying or authenticating a product, (B) labelling an analyte, (C) detecting an analyte, and (D) producing a light source for the telecommunication industry using the above nanocrystals.
摘要翻译：本发明涉及一种制备镧系元素掺杂的NaYF4纳米晶体的方法，所述方法包括：（A）提供包含非配位溶剂，脂肪酸配位配体，三氟乙酸钠，三氟乙酸钇，第一掺杂镧系元素三氟乙酸盐和第二掺杂镧系元素三氟乙酸盐，以及包含所述非配位溶剂和所述脂肪酸配位配体的第二溶液，所述第一和第二溶液基本上不含水和氧; （B）在惰性气氛中，将在约100℃至约150℃的温度下加热的第一溶液缓慢加入到在约290℃至约330℃之间的温度下加热的第二溶液，由此产生含有纳米晶体的反应混合物; 和（C）从反应混合物中回收纳米晶体。本发明还涉及平均粒度为至多约50nm的标准偏差至多约15％的镧系元素掺杂均匀形状的立方晶NaYF4纳米晶体。最后，本发明还涉及（A）鉴定或认证产品的方法，（B）标记分析物，（C）检测分析物，和（D）使用上述纳米晶体生产电信工业的光源。

2. 发明授权

US08088631B2 Lanthanide-doped NaYF4 nanocrystals, method of preparing and uses thereof 有权
标题翻译：掺杂镧系元素的NaYF4纳米晶体，其制备方法和用途
公开(公告)号：US08088631B2
公开(公告)日：2012-01-03
申请号：US12125201
申请日：2008-05-22
申请人： John A. Capobianco , John-Christopher Boyer , Louis A. Cuccia , Fiorenzo Vetrone
发明人： John A. Capobianco , John-Christopher Boyer , Louis A. Cuccia , Fiorenzo Vetrone
IPC分类号： G01N33/553
CPC分类号： C01F17/0031 , B82Y15/00 , B82Y30/00 , C01P2002/52 , C01P2002/72 , C01P2002/77 , C01P2002/84 , C01P2002/86 , C01P2004/04 , C01P2004/22 , C01P2004/52 , C01P2004/64 , C09D11/037 , G01N33/588
摘要： The present invention relates to a method of preparing lanthanide-doped NaYF4 nanocrystals, the method comprising: (A) providing a first solution comprising a non-coordinating solvent, a fatty acid coordinating ligand, sodium trifluoroacetate, yttrium trifluoroacetate, a first doping lanthanide trifluoroacetate and a second doping lanthanide trifluoroacetate, and a second solution comprising the non-coordinating solvent and the fatty acid coordinating ligand, the first and second solutions being substantially free of water and oxygen; (B) in an inert atmosphere, slowly adding the first solution heated at a temperature between about 100° C. and about 150° C. to the second solution heated at temperature between about 290° C. and about 330° C., thereby producing a reaction mixture containing the nanocrystals; and (C) recovering the nanocrystals from the reaction mixture. The invention also relates to lanthanide-doped uniformly shaped cubic NaYF4 nanocrystals having an average particle size of at most about 50 nm with a standard deviation of at most about 15%. Finally, the invention also relates to methods of (A) identifying or authenticating a product, (B) labelling an analyte, (C) detecting an analyte, and (D) producing a light source for the telecommunication industry using the above nanocrystals.
摘要翻译：本发明涉及一种制备镧系元素掺杂的NaYF4纳米晶体的方法，所述方法包括：（A）提供包含非配位溶剂，脂肪酸配位配体，三氟乙酸钠，三氟乙酸钇，第一掺杂镧系元素三氟乙酸盐和第二掺杂镧系元素三氟乙酸盐，以及包含所述非配位溶剂和所述脂肪酸配位配体的第二溶液，所述第一和第二溶液基本上不含水和氧; （B）在惰性气氛中，将在约100℃至约150℃的温度下加热的第一溶液缓慢加入到在约290℃至约330℃之间的温度下加热的第二溶液，由此产生含有纳米晶体的反应混合物; 和（C）从反应混合物中回收纳米晶体。本发明还涉及平均粒度为至多约50nm的标准偏差至多约15％的镧系元素掺杂均匀形状的立方晶NaYF4纳米晶体。最后，本发明还涉及（A）鉴定或认证产品的方法，（B）标记分析物，（C）检测分析物，和（D）使用上述纳米晶体生产电信工业的光源。

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