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1. 发明授权

US4416971A Novel xanthene compounds and their photographic use 失效
公开(公告)号：US4416971A
公开(公告)日：1983-11-22
申请号：US454092
申请日：1982-12-28
申请人： Alan L. Borror , Louis Cincotta , John W. Lee, Jr.
发明人： Alan L. Borror , Louis Cincotta , John W. Lee, Jr.
IPC分类号： C09B11/00 , C09B11/28 , G03C1/83 , G03C8/10 , G03C8/14 , G03C8/24 , G03C8/48 , G03C7/00 , G03C1/40 , G03C1/84 , G03C5/54
CPC分类号： G03C8/48 , C09B11/28 , G03C1/83
摘要： In one embodiment, the present invention is concerned with novel xanthene compounds of the formula ##STR1## wherein each R.sup.1 is the same and is selected from ##STR2## R.sup.2 is alkyl, R.sup.3 is an electron-withdrawing group positioned ortho, meta or para to said N atom, R.sup.4 is hydrogen, alkyl or an electron-withdrawing group positioned ortho, meta or para to said N atom; R.sup.5 is alkyl; X is hydrogen, an electron-withdrawing group or an electron-donating group; and A is an anion. In another embodiment, the present invention is concerned with photographic products and processes employing these xanthene compounds, e.g., as photographic light-screening dyes.

2. 发明授权

US4140689A 3-(Julolidinyl)-benz[d]isothiazole-1,1-dioxide 失效
标题翻译： 3-（月桂烷基） - 苯并[d] {9异噻唑-1,1-二氧化物
公开(公告)号：US4140689A
公开(公告)日：1979-02-20
申请号：US836023
申请日：1977-09-23
申请人： James W. Foley , John W. Lee, Jr.
发明人： James W. Foley , John W. Lee, Jr.
IPC分类号： C07D455/04 , G03C1/83 , G03C8/48 , C07D491/06 , C07D513/06
CPC分类号： G03C1/83 , C07D455/04 , G03C8/48
摘要： This invention relates to 3-(julolidinyl)-benz[d]-isothiazole-1,1-dioxide useful as an intermediate in the synthesis of certain 3,3-disubstituted-2,3-dihydrobenz[d]-isothiazole-1,1-dioxide dyes which find utility as, for example, photographic optical filter agents and filter agent precursors.
摘要翻译：本发明涉及可用作合成某些3,3-二取代-2,3-二氢苯并[d] - 异噻唑-1的中间体的3-（三环素基） - 苯并[d] - 异噻唑-1,1-二氧化物，可用作例如照相光学过滤剂和过滤剂前体的二氧化氯染料。

3. 发明授权

US4139704A Cyclic amino containing benzisothiazoles 失效
标题翻译：环状氨基苯并异噻唑
公开(公告)号：US4139704A
公开(公告)日：1979-02-13
申请号：US836022
申请日：1977-09-23
申请人： Alan L. Borror , James W. Foley , John W. Lee, Jr.
发明人： Alan L. Borror , James W. Foley , John W. Lee, Jr.
IPC分类号： C07D275/06 , C07D417/10
CPC分类号： C07D275/06
摘要： This invention relates to 3-(phenyl/naphthyl)benz[d]isothiazole-1,1-dioxides wherein the phenyl or naphthyl substituent possesses an N-heterocyclic moiety in the para position. These compounds are useful as intermediates in the synthesis of certain 3,3-disubstituted-2,3-dihydrobenz[d]isothiazole-1,1-dioxide dyes which find utility as, for example, photographic optical filter agents and filter agent precursors.
摘要翻译：本发明涉及3-（苯基/萘基）苯并[d]异噻唑-1,1-二氧化物，其中苯基或萘基取代基在对位具有N-杂环部分。这些化合物可用作合成某些3,3-二取代-2,3-二氢苯并[d]异噻唑-1,1-二氧化物染料的中间体，其可用作例如照相光学过滤剂和过滤剂前体。

4. 发明授权

US06905600B2 Method and apparatus for the treatment of particulate biodegradable organic waste 有权
标题翻译：用于处理颗粒状可生物降解有机废物的方法和设备
公开(公告)号：US06905600B2
公开(公告)日：2005-06-14
申请号：US10286454
申请日：2002-10-31
申请人： John W. Lee, Jr.
发明人： John W. Lee, Jr.
IPC分类号： B09B3/00 , C02F1/02 , C02F3/28 , C02F9/00 , C02F11/18 , C05F5/00 , C05F17/00 , C02F11/04
CPC分类号： C05F17/0045 , B09B3/00 , C02F1/025 , C02F1/66 , C02F3/28 , C02F3/286 , C02F9/00 , C02F11/18 , C05F5/00 , C05F17/0027 , C12M21/04 , C12M45/02 , C12M45/04 , C12M45/06 , C12M45/20 , Y02A40/209 , Y02E50/343 , Y02P20/145 , Y02W30/43 , Y02W30/47 , C05F7/00 , C05F11/00
摘要： A method for treating particulate biodegradable organic waste includes sizing the waste and adding a base prior to introducing the waste to a thermal hydrolysis reactor and hydrolyzing the waste at a temperature of about 130° C. or greater and a pressure greater than the saturated water vapor pressure to produce a slurry including solubilized organic material and residual solids. The solubilized organic material is separated from the residual solids using a liquid/solid separator and the solubilized organics are subjected to anaerobic digestion to produce a methane gas. The base is preferably potassium hydroxide (KOH) at a concentration of about 1%. The method may further include preheating the particulate biodegradable organic waste with latent heat of the separated solubilized organic material prior to thermal hydrolysis.
摘要翻译：用于处理颗粒状可生物降解的有机废物的方法包括在将废物引入热水解反应器之前对废物进行尺寸调整和添加碱，并在大约130℃或更高的温度和大于饱和水蒸气的压力下水解废物产生包括溶解的有机材料和残余固体的浆料的压力。使用液体/固体分离器将溶解的有机材料与残余固体分离，并将溶解的有机物进行厌氧消化以产生甲烷气体。碱的优选浓度为约1％的氢氧化钾（KOH）。该方法可以进一步包括在热水解之前用分离的溶解有机材料的潜热来预热颗粒状可生物降解的有机废物。

5. 发明授权

US4178447A Novel synthesis of 3,3-substituted dihydrobenzisothiazole-1,1-dioxides and -2,3-dihydronaphtho-1,2-thiazine-1,1-dioxides 失效
标题翻译： 3,3-取代二氢苯并异噻唑-1,1-二氧化物和2,3-二氢萘并-1,2-噻嗪-1,1-二氧化物的新合成
公开(公告)号：US4178447A
公开(公告)日：1979-12-11
申请号：US836025
申请日：1977-09-23
申请人： Alan L. Borror , James W. Foley , Marcis M. Kampe , John W. Lee, Jr.
发明人： Alan L. Borror , James W. Foley , Marcis M. Kampe , John W. Lee, Jr.
IPC分类号： C07C43/225 , C07D275/06 , C07D309/12 , C07D455/04 , C07F7/18 , G03C1/83 , G03C8/48
CPC分类号： C07D275/06 , C07C43/225 , C07D309/12 , C07D455/04 , C07F7/1852 , G03C1/83 , G03C8/48 , Y02P20/55
摘要： This invention relates to a method of synthesizing certain 3-(carbocyclic aryl)-3-(4'-OP-carbocyclic aryl)-2,3-dihydrobenz[d]isothiazole-1,1-dioxides (and -2,3-dihydronaphtho[1,8-de]-1,2-thiazine-1,1-dioxides) by reacting (a) a 4-OP-carbocyclic aryllithium compound wherein P is a protecting group and (b) a 3-(carbocyclic aryl)benz[d]isothiazole-1,1-dioxide wherein said 3-(carbocyclic aryl) moiety is other than a 3-(4'-OP-carbocyclic aryl) moiety to give (c) the corresponding 3-carbocyclic aryl)-3-(4'-OP-carbocyclic aryl)-2,3-dihydrobenz[d]isothiazole-1,1-dioxide. The -2,3-dihydronaphtho[1,8-de]-1,2-thiazine-1,1-dioxides are prepared in the same manner by reacting a 3-(carbocyclic aryl)naphtho[1,8-de]-1,2-thiazine-1,1-dioxide with said 4'-OP-carbocyclic aryllithium compound.In a further embodiment, the compounds synthesized according to the foregoing method are reacted with a carboxylic acid halide to give the corresponding 2-carbonyl-substituted 2,3-dihydrobenz[d]isothiazole-1,1-dioxide (or -2,3-dihydronaphtho[1,8-de]-1,2-thiazine-1,1-dioxides) followed by removing the protecting group, P, with weak acid to yield certain phenol and 1-naphthol sulfam(na)phthaleins useful, e.g., as optical filter agents and filter agent precursors in photography.
摘要翻译：本发明涉及合成某些3-（碳环芳基）-3-（4'-OP-碳环芳基）-2,3-二氢苯并[d]异噻唑-1,1-二氧化物（和-2,3-二（a）4-OP-碳环芳基锂化合物，其中P是保护基，和（b）3-（碳环基））苯并[d]异噻唑-1,1-二氧化物，其中所述3-（碳环芳基）部分不是3-（4'-OP-碳环芳基）部分，得到（c）相应的3-碳环芳基） 3-（4'-OP-碳环芳基）-2,3-二氢苯并[d]异噻唑-1,1-二氧化物。 2,3-二氢萘并[1,8-de] -1,2-噻嗪-1,1-二氧化物以相同的方式通过使3-（碳环芳基）萘并[1,8-de] 与所述4'-OP-碳环芳基锂化合物的1,2-噻嗪-1,1-二氧化物。在另一个实施方案中，将根据前述方法合成的化合物与羧酸卤化物反应，得到相应的2-羰基取代的2,3-二氢苯并[d]异噻唑-1,1-二氧化物（或-2,3 - 二氢萘并[1,8-de] -1,2-噻嗪-1,1-二氧化物），然后用弱酸除去保护基团P，得到某些苯酚和1-萘酚磺酰胺（na）酞类，例如，作为摄影中的滤光剂和滤光剂前体。

6. 发明授权

US07311834B2 Apparatus for the treatment of particulate biodegradable organic waste 有权
标题翻译：用于处理颗粒状可生物降解有机废物的设备
公开(公告)号：US07311834B2
公开(公告)日：2007-12-25
申请号：US11586343
申请日：2006-10-25
申请人： John W Lee, Jr.
发明人： John W Lee, Jr.
IPC分类号： C02F3/28
CPC分类号： C05F17/0045 , B09B3/00 , C02F1/025 , C02F1/66 , C02F3/28 , C02F3/286 , C02F9/00 , C02F11/18 , C05F5/00 , C05F17/0027 , C12M21/04 , C12M45/02 , C12M45/04 , C12M45/06 , C12M45/20 , Y02A40/209 , Y02E50/343 , Y02P20/145 , Y02W30/43 , Y02W30/47 , C05F7/00 , C05F11/00
摘要： An apparatus for treating particulate biodegradable organic waste includes a thermal hydrolysis reactor receiving the particulate biodegradable organic waste for performing thermal hydrolysis at a temperature of about 130° C. at a pressure at or above the saturated water vapor pressure of the organic waste to produce a slurry including solubilized organic material and residual solids. A pH adjustment means for adjusting the pH of the particulate biodegradable organic waste as necessary to provide an acidic pH of greater than about 3.15 before thermo hydrolysis of the particulate biodegradable organic waste is provided. Separating means receive the solubilized organic material and residual solids for separating solubilized organic material from the residual solids. An anaerobic reactor is configured to receive the solubilized organic material.
摘要翻译：用于处理颗粒状可生物降解的有机废物的装置包括热水解反应器，其接收颗粒状可生物降解的有机废物，用于在等于或高于有机废物的饱和水蒸汽压力的压力下在约130℃的温度下进行热水解，以产生包括溶解的有机材料和残留固体的浆料。 pH调节装置，用于在提供颗粒状可生物降解的有机废物的热水解之前根据需要调节颗粒状可生物降解的有机废物的pH以提供大于约3.15的酸性pH。分离装置接收溶解的有机材料和残余固体，用于从残留固体中分离溶解的有机材料。厌氧反应器被配置成接收溶解的有机材料。

7. 发明授权

US07968760B2 Treatment of particulate biodegradable organic waste by thermal hydrolysis using condensate recycle 有权
标题翻译：通过使用冷凝物回收的热水解处理颗粒可生物降解的有机废物
公开(公告)号：US07968760B2
公开(公告)日：2011-06-28
申请号：US12048423
申请日：2008-03-14
申请人： John W Lee, Jr.
发明人： John W Lee, Jr.
IPC分类号： A62D3/20
CPC分类号： C02F11/18 , B09B3/00 , B09B3/0083 , C02F1/66 , C02F2209/02 , C02F2209/03
摘要： A method of treating particulate biodegradable organic waste by thermal hydrolysis. The method includes subjecting a quantity of the particulate biodegradable waste to thermal hydrolysis at a temperature above about 130° C. and a pressure at or above the saturated water vapor pressure to produce a slurry. The slurry will include solubilized organic material and unhydrolyzed residual solids. The method further includes decreasing the pressure at which the slurry is maintained. Typically, the step of decreasing slurry pressure will occur in a flash tank, which allows the separation of an organic acid-rich steam from other hydrolysis products. The method further includes capturing the steam or other condensable gases released when pressure is decreased and condensing the steam or other condensable gases into a condensate. The captured condensate may then be added to a quantity of particulate biodegradable waste prior to thermal hydrolysis. Also disclosed is an apparatus for practicing the method described above.
摘要翻译：通过热水解处理颗粒生物降解有机废物的方法。该方法包括使一定量的颗粒生物可降解废物在高于约130℃的温度和等于或高于饱和水蒸气压的压力下进行热水解以产生浆料。浆料将包括溶解的有机材料和未水解的残留固体。该方法还包括降低保持浆料的压力。通常，降低浆料压力的步骤将发生在闪蒸罐中，其允许有机酸富含蒸汽与其它水解产物分离。该方法还包括捕获当压力降低时释放的蒸汽或其它可冷凝气体，并将蒸汽或其它可冷凝气体冷凝成冷凝物。然后在热水解之前将捕获的冷凝物加入到一定量的可生物降解的颗粒物中。还公开了用于实施上述方法的装置。

8. 发明授权

US4617402A Novel xanthene compounds and their photographic use 失效
标题翻译：新型呫吨化合物及其摄影用途
公开(公告)号：US4617402A
公开(公告)日：1986-10-14
申请号：US528454
申请日：1983-09-01
申请人： Alan L. Borror , Louis Cincotta , John W. Lee, Jr.
发明人： Alan L. Borror , Louis Cincotta , John W. Lee, Jr.
IPC分类号： C09B11/28 , G03C1/83 , G03C8/48 , C07D405/14 , C07D311/82
CPC分类号： G03C1/83 , C09B11/28 , G03C8/48
摘要： In one embodiment, the present invention is concerned with novel xanthene compounds of the formula ##STR1## wherein each R.sup.1 is the same and is selected from ##STR2## R.sup.2 is alkyl, R.sup.3 is an electron-withdrawing group positioned ortho, meta or para to said N atom, R.sup.4 is hydrogen, alkyl or an electron-withdrawing group positioned ortho, meta or para to said N atom; R.sup.5 is alkyl; X is hydrogen, an electron-withdrawing group or an electron-donating group; and A is an anion. In another embodiment, the present invention is concerned with photographic products and processes employing these xanthene compounds, e.g., as photographic light-screening dyes.
摘要翻译：在一个实施方案中，本发明涉及式（IMAGE）的新颖的呫吨化合物，其中每个R 1相同并且选自R 2是烷基，R 3是位于邻位，间或对位的吸电子基团所述N原子，R 4为氢，烷基或吸电子基团，位于所述N原子的邻位，间位或对位; R5是烷基; X是氢，吸电子基团或给电子基团; 而A是阴离子。在另一个实施方案中，本发明涉及使用这些呫吨化合物的照相产品和方法，例如作为照相照相染色剂。

9. 发明授权

US988917A Air-pressure indicator. 失效
标题翻译：空气压力指示器
公开(公告)号：US988917A
公开(公告)日：1911-04-04
申请号：US1910564265
申请日：1910-05-31
申请人： JOHN W LEE JR
发明人： WALKER HENRY W
CPC分类号： G01L19/0007

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