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1. 发明授权

US4911986A Curable silicone compositions comprising vinyl monomer 失效
标题翻译：包含乙烯基单体的可固化硅氧烷组合物
公开(公告)号：US4911986A
公开(公告)日：1990-03-27
申请号：US12475
申请日：1987-02-09
申请人： John R. Keryk , Padmakumari J. Varaprath , Antony P. Wright
发明人： John R. Keryk , Padmakumari J. Varaprath , Antony P. Wright
IPC分类号： C08F299/08 , C08F230/08 , C08F283/12 , C08F290/00 , C08F290/06 , C08F290/14 , C09D183/04 , C09D183/07 , C09D183/10
CPC分类号： C08F230/08 , C08F290/148 , Y10T428/31663
摘要： Curable organosilicon compounds which contain (meth)acryl-amido-substituted hydrocarbon radicals have their viscosities greatly reduced by the addition of a small amount of a vinyl monomer compound. Advantageously, the resulting compositions are more easily applied to a substrate, such as paper, in fast-paced coating operations without the significant loss of useful properties, such as the cure rate of the curable composition and the adhesive release behavior of the cured composition.

2. 发明授权

US06596821B1 Hydrosilyation cured silicone resins obtained by fractionation 失效
$Hydrosilyation cured silicone resins obtained by fractionation$
标题翻译：通过分级得到的水解固化的硅氧烷树脂
公开(公告)号：US06596821B1
公开(公告)日：2003-07-22
申请号：US10091678
申请日：2002-03-05
申请人： Dimitris E. Katsoulis , Bizhong Zhu , John R. Keryk , Frederick J. McGarry , Zhongtao Li
发明人： Dimitris E. Katsoulis , Bizhong Zhu , John R. Keryk , Frederick J. McGarry , Zhongtao Li
IPC分类号： C08G7704
CPC分类号： C08G77/04 , C08G77/36 , C08K5/0025
摘要： A process for producing a cured silsesquioxane resin. The process includes fractionating the silsesquioxane resin a plurality of times utilizing an organic solvent in combination with an organic non-solvent. The fractionated resin is then stripped of excess solvent. The stripped resin is then mixed with a cross-linking compound to form a curable composition. The curable composition is cured to form a cured resin having high fracture toughness and strength without the loss of elastic modulus.
摘要翻译：固化倍半硅氧烷树脂的制造方法。该方法包括使用有机溶剂与有机非溶剂组合多次分级倍半硅氧烷树脂。然后将分馏的树脂汽提出过量的溶剂。然后将剥离的树脂与交联化合物混合以形成可固化组合物。可固化组合物固化以形成具有高断裂韧性和强度的固化树脂，而不损失弹性模量。

3. 发明授权

US5608096A Method of forming siloxane polymers using a heteropoly catalyst having a keggin structure 失效
标题翻译：使用具有keggin结构的杂多酸催化剂形成硅氧烷聚合物的方法
公开(公告)号：US5608096A
公开(公告)日：1997-03-04
申请号：US580417
申请日：1995-12-28
申请人： Dimitris E. Katsoulis , John R. Keryk
发明人： Dimitris E. Katsoulis , John R. Keryk
IPC分类号： C07F7/08 , C08G77/08
CPC分类号： C07F7/0874 , C08G77/08
摘要： The invention relates to a method of forming siloxane polymers using a heteropoly catalyst having a Keggin structure. The method comprises contacting a fluid comprising at least one siloxane polymer precursor selected from the group consisting of cyclic siloxanes (I) having the formula (RR'SiO).sub.a and linear siloxanes (II) having the formula ##STR1## where R is a substituted or unsubstituted monovalent hydrocarbon having from 1 to 6 carbon atoms, R' is hydrogen or a substituted or unsubstituted monovalent hydrocarbon having from 1 to 6 carbon atoms, a is at least 3 and b is at least 1; with an effective amount of a heteropoly catalyst having a Keggin structure, selected from the group consisting of heteropoly acids (III) having the formula H.sub.n XM.sub.12 O.sub.40, salts thereof and mixed acid-salts thereof, where X is B.sup.+3, Si.sup.+4, Ge .sup.+4, p.sup.+5, M is Mo.sup.+6 and n is 3, 4 or 5, as required for the valence of the heteropoly acid to equal 0, at a temperature ranging from about 23.degree. C. to the boiling point of the siloxane polymer precursor.
摘要翻译：本发明涉及使用具有Keggin结构的杂多酸催化剂形成硅氧烷聚合物的方法。该方法包括使包含至少一种选自具有式（RR'SiO）a的环状硅氧烷（I）和具有式“IMAGE”的线性硅氧烷（II））的硅氧烷聚合物前体的流体接触，其中R是取代的或未取代的具有1至6个碳原子的一价烃，R'是氢或具有1至6个碳原子的取代或未取代的一价烃，a至少为3，b为至少1; 与有效量的具有Keggin结构的杂多酸催化剂，其选自具有式H n X M 12 O 40的杂多酸（III），其盐和其混合的酸盐，其中X是B + 3，Si + 4，Ge +4，p + 5，M为Mo + 6，n为3,4或5，如杂多酸的化合价等于0所需，在约23℃至沸点硅氧烷聚合物前体。

4. 发明授权

US07514148B2 Hybrid composite of silicone and organic resins 失效
标题翻译：硅胶和有机树脂的混合复合材料
公开(公告)号：US07514148B2
公开(公告)日：2009-04-07
申请号：US11337270
申请日：2006-01-20
申请人： Bizhong Zhu , Herschel H. Reese , Dimitris E. Katsoulis , John R. Keryk , Yuhong Wu , Frederick J. McGarry
发明人： Bizhong Zhu , Herschel H. Reese , Dimitris E. Katsoulis , John R. Keryk , Yuhong Wu , Frederick J. McGarry
IPC分类号： B32B13/12
CPC分类号： B32B5/26 , B32B3/12 , B32B5/022 , B32B5/024 , B32B27/04 , B32B27/08 , B32B2260/021 , B32B2260/046 , B32B2262/0261 , B32B2262/0269 , B32B2262/0276 , B32B2262/101 , B32B2262/106 , B32B2305/024 , B32B2305/076 , B32B2307/3065 , B32B2315/085 , H05K1/036 , H05K1/0366 , H05K2201/0162 , Y10T428/31511 , Y10T428/31663 , Y10T428/31667 , Y10T428/31855 , Y10T428/31935 , Y10T428/31942
摘要： A fiber reinforced composite including layers of fibers, each layer being impregnated with a resin. The layers include in combination a layer of an addition cured silicone resin and a layer of an organic resin. The layers form a hybrid composite having a higher modulus retention at elevated temperatures than the addition cured silicone resin alone. The hybrid composite's mechanical properties are similar to the organic resin composite, but demonstrate enhanced thermal resistance and reduced flammability.
摘要翻译：一种纤维增强复合材料，包括纤维层，每层用树脂浸渍。这些层包括加成固化的硅树脂层和有机树脂层的组合。这些层形成在高于仅加入固化的硅氧烷树脂的高温下具有更高模量保留性的混合复合材料。混合复合材料的机械性能类似于有机树脂复合材料，但表现出增强的耐热性和降低的可燃性。

5. 发明授权

US4596720A Radiation-curable organopolysiloxane coating composition 失效
标题翻译：可辐射固化的有机聚硅氧烷涂料组合物
公开(公告)号：US4596720A
公开(公告)日：1986-06-24
申请号：US783714
申请日：1985-10-03
申请人： John R. Keryk , Peter Y. Kwai Lo
发明人： John R. Keryk , Peter Y. Kwai Lo
IPC分类号： C09J7/02 , B05D3/06 , B05D5/08 , C08G77/20 , C08L83/04 , C08L83/07 , C08L83/08 , C09D5/00 , C09D183/04 , C09D183/07 , C09D183/08
CPC分类号： C08L83/08 , C08G77/20 , Y10T428/31663
摘要： Compositions curable by exposure to UV or electron beam are disclosed which contain mercapto functional organosiloxanes and organosiloxanes bearing alkenyl groups with 6 or more carbon atoms. The compositions cure upon irradiation without the emission of obnoxious odor which characterizes the analogous composition of the art containing olefinic siloxanes having only vinyl unsaturation. Also disclosed is a method of treating a substrate with the coating composition to improve the release of adhesive materials therefrom.
摘要翻译：公开了通过暴露于UV或电子束可固化的组合物，其含有巯基官能的有机硅氧烷和带有6个或更多个碳原子的烯基的有机硅氧烷。组合物在照射时固化而不发出令人讨厌的气味，其特征在于包含仅具有乙烯基不饱和度的烯属硅氧烷的本领域的类似组成。还公开了一种用涂料组合物处理基材以改善其粘合剂材料的释放的方法。

6. 发明授权

US07037592B2 Hybrid composite of silicone and organic resins 失效
公开(公告)号：US07037592B2
公开(公告)日：2006-05-02
申请号：US10374802
申请日：2003-02-25
申请人： Bizhong Zhu , Herschel H. Reese , Dimitris E. Katsoulis , John R. Keryk , Yuhong Wu , Frederick J. McGarry
发明人： Bizhong Zhu , Herschel H. Reese , Dimitris E. Katsoulis , John R. Keryk , Yuhong Wu , Frederick J. McGarry
IPC分类号： B32B13/12
CPC分类号： B32B5/26 , B32B3/12 , B32B5/022 , B32B5/024 , B32B27/04 , B32B27/08 , B32B2260/021 , B32B2260/046 , B32B2262/0261 , B32B2262/0269 , B32B2262/0276 , B32B2262/101 , B32B2262/106 , B32B2305/024 , B32B2305/076 , B32B2307/3065 , B32B2315/085 , H05K1/036 , H05K1/0366 , H05K2201/0162 , Y10T428/31511 , Y10T428/31663 , Y10T428/31667 , Y10T428/31855 , Y10T428/31935 , Y10T428/31942
摘要： A fiber reinforced composite including layers of fibers, each layer being impregnated with a resin. The layers include in combination a layer of an addition cured silicone resin and a layer of an organic resin. The layers form a hybrid composite having a higher modulus retention at elevated temperatures than the addition cured silicone resin alone. The hybrid composite's mechanical properties are similar to the organic resin composite, but demonstrate enhanced thermal resistance and reduced flammability.

7. 发明授权

US06646039B2 Hydrosilyation cured silicone resin containing colloidal silica and a process for producing the same 有权
标题翻译：含有胶体二氧化硅的含水溶性固化的硅氧烷树脂及其制备方法
公开(公告)号：US06646039B2
公开(公告)日：2003-11-11
申请号：US10091685
申请日：2002-03-05
申请人： Zhongtao Li , Frederick J. McGarry , Dimitris E. Katsoulis , John R. Keryk , Debora F. Bergstrom , Kermit S. Kwan , Bizhong Zhu
发明人： Zhongtao Li , Frederick J. McGarry , Dimitris E. Katsoulis , John R. Keryk , Debora F. Bergstrom , Kermit S. Kwan , Bizhong Zhu
IPC分类号： C08K336
CPC分类号： C08K9/06 , C08G77/12 , C08G77/20 , C08G77/70 , C08K3/36 , C08K5/5403 , C08L83/04 , C08L83/00
摘要： A hydrosilylation reaction curable composition including a silsesquioxane polymer, a cross-linking compound, a hydrosilylation reaction catalyst and colloidal silica having a surface coating formed thereon. The curable composition is cured to form a cured resin having high fracture toughness and strength without the loss of elastic modulus and glass transition temperature.
摘要翻译：包含倍半硅氧烷聚合物，交联化合物，氢化硅烷化反应催化剂和其上形成有表面涂层的胶体二氧化硅的氢化硅烷化反应固化性组合物。可固化组合物固化以形成具有高断裂韧性和强度的固化树脂，而不损失弹性模量和玻璃化转变温度。

8. 发明授权

US5371128A Hot-melt silicone pressure sensitive adhesive with siloxylated allyloxypropane diol copolymers as additives 失效
标题翻译：具有硅氧烷基化烯丙氧基丙烷二醇共聚物的热熔硅胶压敏粘合剂作为添加剂
公开(公告)号：US5371128A
公开(公告)日：1994-12-06
申请号：US181505
申请日：1994-01-14
申请人： Katherine L. Ulman , William J. Schulz, Jr. , John R. Keryk
发明人： Katherine L. Ulman , William J. Schulz, Jr. , John R. Keryk
IPC分类号： C09J5/06 , A61K9/70 , C09J183/00 , C09J183/04 , C08L83/04
CPC分类号： A61K9/7069 , C09J183/04
摘要： The instant invention pertains to a hot-melt pressure sensitive adhesive composition wherein the composition is comprised of a mixture of (i) a silicone resin and (ii) a silicone fluid, the mixture exhibiting tackiness and adhesiveness, the mixture being blended with (B) from about 1.0 to 20 weight percent, based on the total weight of the mixture of (i) and (ii), of a siloxylated allyloxypropane diol copolymer. The instant invention also encompasses method of using the composition, methods of making hot-melt silicone pressure sensitive adhesive-coated substrates, and devices made using the composition.
摘要翻译：本发明涉及一种热熔压敏粘合剂组合物，其中组合物由（i）硅树脂和（ii）硅氧烷流体的混合物组成，该混合物显示粘性和粘合性，该混合物与（B ）为约1.0至20重量％，基于（i）和（ii）的混合物的总重量，酯化烯丙氧基丙烷二醇共聚物。本发明还包括使用该组合物的方法，制备热熔性硅氧烷压敏粘合剂涂覆的基材的方法，以及使用该组合物制备的装置。

9. 发明授权

US06689859B2 High fracture toughness hydrosilyation cured silicone resin 失效
$High fracture toughness hydrosilyation cured silicone resin$
标题翻译：高断裂韧性硅烷化固化硅树脂
公开(公告)号：US06689859B2
公开(公告)日：2004-02-10
申请号：US10092055
申请日：2002-03-05
申请人： Zhongtao Li , Frederick J. McGarry , John R. Keryk , Bizhong Zhu , Dimitris E. Katsoulis
发明人： Zhongtao Li , Frederick J. McGarry , John R. Keryk , Bizhong Zhu , Dimitris E. Katsoulis
IPC分类号： C08G7706
CPC分类号： C08K5/54 , C08G77/12 , C08G77/20 , C08G77/70 , C08K5/5403 , C08K5/5419 , C08L83/04 , C08L83/00
摘要： A hydrosilylation reaction curable composition that includes a silsesquioxane polymer, a mixture of silanes or siloxanes as a cross-linking compound and a hydrosilylation reaction catalyst. The curable composition is cured to form a cured resin having high fracture toughness and strength without the loss of elastic modulus.
摘要翻译：一种氢化硅烷化反应可固化组合物，其包含倍半硅氧烷聚合物，作为交联化合物的硅烷或硅氧烷的混合物和氢化硅烷化反应催化剂。可固化组合物固化以形成具有高断裂韧性和强度的固化树脂，而不损失弹性模量。

10. 发明授权

US5548052A Silane modified polyoxometalate anions 失效
标题翻译：硅烷改性多金属氧酸盐阴离子
公开(公告)号：US5548052A
公开(公告)日：1996-08-20
申请号：US364336
申请日：1994-12-27
申请人： Dimitris E. Katsoulis , John R. Keryk
发明人： Dimitris E. Katsoulis , John R. Keryk
IPC分类号： C07F7/02 , C07F11/00 , C08G77/22 , C08G77/398
CPC分类号： C07F11/005
摘要： Silane modified polyoxometalate anions represented by the formula YZ(SiRR').sub.n were prepared by reacting a silane having two hydrolyzable groups with a lacunary polyoxometalate anion. In the formula YZ(SiRR').sub.n, Z is M.sub.11 O.sub.39.sup.-12, M.sub.9 O.sub.34.sup.-14 or M.sub.17 O.sub.61.sup.-20, where M is tungsten or molybdenum; Y is As.sup.+5, Si.sup.+4, B.sup.+3, Ge.sup.+4, P.sup.+5 or Fe.sup.+5 when Z is M.sub.11 O.sub.39.sup.-12, Y is Si.sup.+4, Ge.sup.+4, or P.sup.+5 when Z is M.sub.9 O.sub.34.sup.-14 and Y is As.sub.2.sup.+10 or P.sub.2.sup.+10 when Z is M.sub.17 O.sub.61.sup.-20 ; R is selected from the group consisting of monovalent hydrocarbon radicals having from 1 to 24 carbon atoms, monovalent halogenated hydrocarbon or carbon radicals having from 1 to 24 carbon atoms and monovalent hydrocarbon radicals having from 1 to 24 carbon atoms substituted with an epoxy group, an amino group, a mercapto group or a methacrylo group; R' is a hydrogen atom or R and n represents the number of (.dbd.SiRR').sup.+2 groups bonding to the polyoxometalate anion and has a value from 1 to 3.
摘要翻译：通过使具有两个可水解基团的硅烷与空隙多金属氧酸盐阴离子反应制备由式YZ（SiRR'）n表示的硅烷改性的多金属氧酸盐阴离子。在式YZ（SiRR'）n中，Z是M11O39-12，M9O34-14或M17O61-20，其中M是钨或钼; 当Z为M11O39-12时，Y为As + 5，Si + 4，B + 3，Ge + 4，P + 5或Fe + 5，当Z为M9O34时，Y为Si + 4，Ge + 4或P + -14，当Z为M17O61-20时，Y为As2 + 10或P2 + 10; R选自具有1至24个碳原子的一价烃基，一价卤代烃或具有1至24个碳原子的碳基和具有1至24个碳原子的被环氧基取代的一价烃基，氨基，巯基或甲基丙烯酰基; R'是氢原子或R，n表示与多金属氧酸盐阴离子结合的（= SiRR'）+ 2基团的数目，并且具有1至3的值。

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