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1. 发明授权

US07541479B1 Direct epoxidation process 失效
标题翻译：直接环氧化工艺
公开(公告)号：US07541479B1
公开(公告)日：2009-06-02
申请号：US12154730
申请日：2008-05-27
申请人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr. , Patrick N. Crowe
发明人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr. , Patrick N. Crowe
IPC分类号： C07D301/10
CPC分类号： C07D301/10
摘要： A process is disclosed for reacting an olefin, hydrogen, and oxygen in a slurry comprising a catalyst and a solvent in a reactor having a column and at least one side arm. The column is operated in a churn-turbulent flow regime. The slurry is circulated through the side arm, filtered, and exits the reactor.
摘要翻译：公开了一种在具有柱和至少一个侧臂的反应器中使烯烃，氢和氧在包含催化剂和溶剂的浆料中反应的方法。该柱以搅动 - 湍流流动方式操作。浆料通过侧臂循环，过滤并离开反应器。

2. 发明授权

US08124797B2 Epoxidation process 有权
标题翻译：环氧化工艺
公开(公告)号：US08124797B2
公开(公告)日：2012-02-28
申请号：US12459065
申请日：2009-06-26
申请人： Jay F. Miller , John H. Speidel, Jr.
发明人： Jay F. Miller , John H. Speidel, Jr.
IPC分类号： C07D301/12 , C07D301/06
CPC分类号： C07D301/12 , C07D301/32
摘要： This invention is a process for producing propylene oxide. The process comprises first contacting a titanium zeolite with a reaction feed comprising propylene, hydrogen peroxide, tertiary butyl alcohol, and water to produce a product stream comprising propylene, propylene oxide, propylene glycol, tertiary butyl alcohol, and water. The product stream is distilled to produce a first overhead stream comprising propylene and a first bottoms stream comprising propylene oxide, propylene glycol, tertiary butyl alcohol, and water. The first bottoms stream is distilled to produce a second overhead stream comprising propylene oxide and a second bottoms product stream comprising propylene glycol, tertiary butyl alcohol, and water. The second bottoms stream is distilled to produce a third overhead stream comprising an azeotrope of tertiary butyl alcohol and water and a third bottoms stream comprising propylene glycol and water.
摘要翻译：本发明是一种生产环氧丙烷的方法。该方法包括首先使钛沸石与包含丙烯，过氧化氢，叔丁醇和水的反应进料接触，以产生包含丙烯，环氧丙烷，丙二醇，叔丁醇和水的产物流。将产物流蒸馏以产生包含丙烯的第一塔顶物流和包含环氧丙烷，丙二醇，叔丁醇和水的第一塔底物流。将第一塔底物流蒸馏以产生包含环氧丙烷的第二塔顶物流和包含丙二醇，叔丁醇和水的第二塔底物产物流。蒸馏第二塔底物流以产生包含叔丁醇和水的共沸物的第三塔顶物流和包含丙二醇和水的第三塔底物流。

3. 发明授权

US07138535B1 Direct epoxidation process 失效
标题翻译：直接环氧化工艺
公开(公告)号：US07138535B1
公开(公告)日：2006-11-21
申请号：US11141962
申请日：2005-06-01
申请人： Peter J. Whitman , Jay F. Miller , John H. Speidel, Jr. , Robert N. Cochran
发明人： Peter J. Whitman , Jay F. Miller , John H. Speidel, Jr. , Robert N. Cochran
IPC分类号： C07D301/06 , C07D301/12
CPC分类号： C07D301/06
摘要： The invention is a process for epoxidizing an olefin with hydrogen and oxygen in the presence of a catalyst comprising a noble metal and a titanium or vanadium zeolite in a solvent mixture comprising water, methanol, and a C3–C6 aliphatic ketone. This process surprisingly gives significantly reduced by-product glycol and glycol ethers formed by the unwanted ring-opening of epoxides.
摘要翻译：本发明是一种在包含贵金属和钛或钒沸石的催化剂存在下，用氢和氧环氧化烯烃的方法，所述催化剂包含水，甲醇和C 3 - C 6脂族酮。该方法令人惊奇地得到由环氧化物不需要的开环形成的显着减少的副产物二醇和二醇醚。

4. 发明申请

US20100331556A1 Epoxidation process 有权
标题翻译：环氧化工艺
公开(公告)号：US20100331556A1
公开(公告)日：2010-12-30
申请号：US12459065
申请日：2009-06-26
申请人： Jay F. Miller , John H. Speidel, JR.
发明人： Jay F. Miller , John H. Speidel, JR.
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , C07D301/32
摘要： This invention is a process for producing propylene oxide. The process comprises first contacting a titanium zeolite with a reaction feed comprising propylene, hydrogen peroxide, tertiary butyl alcohol, and water to produce a product stream comprising propylene, propylene oxide, propylene glycol, tertiary butyl alcohol, and water. The product stream is distilled to produce a first overhead stream comprising propylene and a first bottoms stream comprising propylene oxide, propylene glycol, tertiary butyl alcohol, and water. The first bottoms stream is distilled to produce a second overhead stream comprising propylene oxide and a second bottoms product stream comprising propylene glycol, tertiary butyl alcohol, and water. The second bottoms stream is distilled to produce a third overhead stream comprising an azeotrope of tertiary butyl alcohol and water and a third bottoms stream comprising propylene glycol and water.
摘要翻译：本发明是一种生产环氧丙烷的方法。该方法包括首先使钛沸石与包含丙烯，过氧化氢，叔丁醇和水的反应进料接触，以产生包含丙烯，环氧丙烷，丙二醇，叔丁醇和水的产物流。将产物流蒸馏以产生包含丙烯的第一塔顶物流和包含环氧丙烷，丙二醇，叔丁醇和水的第一塔底物流。将第一塔底物流蒸馏以产生包含环氧丙烷的第二塔顶物流和包含丙二醇，叔丁醇和水的第二塔底物产物流。蒸馏第二塔底物流以产生包含叔丁醇和水的共沸物的第三塔顶物流和包含丙二醇和水的第三塔底物流。

5. 发明申请

US20090247773A1 Propylene oxide process 有权
标题翻译：环氧丙烷工艺
公开(公告)号：US20090247773A1
公开(公告)日：2009-10-01
申请号：US12079823
申请日：2008-03-28
申请人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, JR.
发明人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, JR.
IPC分类号： C07D301/06
CPC分类号： C07D301/06 , C07D301/10 , Y02P20/52
摘要： A process for making propylene oxide from propylene is disclosed. Propylene, hydrogen, and oxygen are reacted in a slurry comprising a catalyst and a solvent to produce a gaseous product stream and a liquid product stream. The gaseous product stream is contacted with an absorbent to produce a gas effluent and a liquid effluent. The gas effluent is recycled to the reaction step.
摘要翻译：公开了一种从丙烯制备环氧丙烷的方法。丙烯，氢和氧在包含催化剂和溶剂的浆料中反应以产生气态产物流和液体产物流。气态产物流与吸收剂接触以产生气体流出物和液体流出物。气体流出物再循环到反应步骤。

6. 发明申请

US20100174099A1 Propylene oxide reactor gas distribution system 审中-公开
标题翻译：环氧丙烷反应器气体分配系统
公开(公告)号：US20100174099A1
公开(公告)日：2010-07-08
申请号：US12319247
申请日：2009-01-05
申请人： Arsam Behkish , Rafael Espinoza , John H. Speidel, JR.
发明人： Arsam Behkish , Rafael Espinoza , John H. Speidel, JR.
IPC分类号： C07D301/02 , B01J19/00
CPC分类号： C07D301/02 , B01J8/006 , B01J8/22 , B01J2208/00132
摘要： A device for reacting fluids comprising: a reactor; a first inlet for transporting a first fluid into the reactor; a first tube system contained within the reactor and connected to and communicating with the first inlet for receiving the first fluid from the first inlet, the first tube system comprising at least one first tube in the form of a ring, the at least one first tube comprising outlets for releasing the first fluid into the reactor; a second inlet for transporting a second fluid into the reactor; and a second tube system contained within the reactor and connected to and communicating with the second inlet for receiving the second fluid from the second inlet, the second tube system comprising at least one second tube in the form of a ring, the at least one second tube comprising outlets for releasing the second fluid into the reactor; wherein at least one first tube and at least one second tube are concentric, and the outlets for releasing the first fluid from the at least one first tube and the outlets for releasing the second fluid from the at least one second tube are positioned so that, upon release of the first and second fluids, the first and second fluids are directed towards each other.
摘要翻译：一种用于使流体反应的装置，包括：反应器; 用于将第一流体输送到反应器中的第一入口; 第一管系统，其包含在所述反应器内并连接到所述第一入口并与所述第一入口连通，用于从所述第一入口接收所述第一流体，所述第一管系统包括至少一个呈环形的第一管，所述至少一个第一管包括用于将第一流体释放到反应器中的出口; 用于将第二流体输送到反应器中的第二入口; 以及第二管系统，其包含在所述反应器内并且连接到所述第二入口并与所述第二入口连通，用于从所述第二入口接收所述第二流体，所述第二管系统包括环形形式的至少一个第二管，所述至少一个第二管管包括用于将第二流体释放到反应器中的出口; 其中至少一个第一管和至少一个第二管是同心的，并且用于从所述至少一个第一管释放第一流体的出口和用于将第二流体从所述至少一个第二管释放的出口被定位成使得，在释放第一和第二流体时，第一和第二流体彼此指向。

7. 发明授权

US07649102B2 Propylene oxide process 有权
标题翻译：环氧丙烷工艺
公开(公告)号：US07649102B2
公开(公告)日：2010-01-19
申请号：US12079823
申请日：2008-03-28
申请人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr.
发明人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr.
IPC分类号： C07D301/06
CPC分类号： C07D301/06 , C07D301/10 , Y02P20/52
摘要： A process for making propylene oxide from propylene is disclosed. Propylene, hydrogen, and oxygen are reacted in a slurry comprising a catalyst and a solvent to produce a gaseous product stream and a liquid product stream. The gaseous product stream is contacted with an absorbent to produce a gas effluent and a liquid effluent. The gas effluent is recycled to the reaction step.
摘要翻译：公开了一种从丙烯制备环氧丙烷的方法。丙烯，氢和氧在包含催化剂和溶剂的浆料中反应以产生气态产物流和液体产物流。气态产物流与吸收剂接触以产生气体流出物和液体流出物。气体流出物再循环到反应步骤。

8. 发明授权

US07550610B1 Direct epoxidation process 失效
标题翻译：直接环氧化工艺
公开(公告)号：US07550610B1
公开(公告)日：2009-06-23
申请号：US12079796
申请日：2008-03-28
申请人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr.
发明人： Te Chang , Arsam Behkish , Jude T. Ruszkay , John H. Speidel, Jr.
IPC分类号： C07D301/10
CPC分类号： B01J8/22 , B01J8/006 , B01J8/228
摘要： A process is disclosed for reacting an olefin, hydrogen, and oxygen in a slurry comprising a catalyst and a solvent in a reactor. The gas bubbles in the slurry are in a churn-turbulent flow regime. The process gives improved yield and operational and maintenance advantages.
摘要翻译：公开了用于使反应器中包含催化剂和溶剂的浆料中的烯烃，氢和氧反应的方法。浆料中的气泡呈搅动流动状态。该方法提高了产量和操作和维护的优点。

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