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1. 发明授权

US5003104A Carbonylation process and catalyst 失效
标题翻译：羰基化过程和催化剂
公开(公告)号：US5003104A
公开(公告)日：1991-03-26
申请号：US265234
申请日：1988-10-31
申请人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , Robert G. Schultz , James F. Roth
发明人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , Robert G. Schultz , James F. Roth
IPC分类号： B01J31/20 , C07C51/10 , C07C51/12 , C07C51/14
CPC分类号： B01J31/26 , B01J31/0231 , B01J31/1895 , B01J31/20 , B01J31/2404 , C07C51/10 , C07C51/12 , C07C51/14 , C07C67/36 , B01J2231/321 , B01J2231/34 , B01J2531/822
摘要： This invention involves a process for the carbonylation of a carbonylatable reactant, e.g., an alkyl ester, a dialkyl ether or mixtures thereof by reacting the same with carbon monoxide. The process comprises effecting the carbonylation in the presence of a solution of a catalyst system containing a rhodium compound, an iodide and a lithium component at a temperature of from 50.degree. C. to 400.degree. C. at a carbon monoxide partial pressure of 1 psig to 15,000 psig. Hydrogen may also be present. The invention also concerns a carbonylation catalyst system effective for the addition of carbon monoxide to a carbonylatable reactant which comprises a solution containing as essential components a rhodium containing active component, an iodide and a lithium component.
摘要翻译：本发明涉及通过使其与一氧化碳反应来羰基化可羰基化反应物，例如烷基酯，二烷基醚或其混合物的方法。该方法包括在含有铑化合物，碘化物和锂组分的催化剂体系的溶液存在下，在50℃至400℃的温度下，在1psig的一氧化碳分压下进行羰基化至15,000 psig。氢也可能存在。本发明还涉及一种有效地将一氧化碳加入到可羰基化反应物中的羰基化催化剂体系，其包含含有铑的活性组分，碘化物和锂组分作为主要成分的溶液。

2. 发明授权

US4690912A Rhodium-containing carbonylation catalysts with halogen-containing promoter 失效
标题翻译：含铑羰基化催化剂与含卤素促进剂
公开(公告)号：US4690912A
公开(公告)日：1987-09-01
申请号：US541845
申请日：1983-10-14
申请人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
发明人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
IPC分类号： B01J27/08 , B01J31/02 , B01J31/20 , B01J31/24 , C07C51/12 , B01J31/18
CPC分类号： B01J31/2404 , B01J27/08 , B01J31/0231 , B01J31/20 , C07C51/12 , B01J2231/34 , B01J2531/822
摘要： A catalyst system having high activity and selectivity to carbonylation products comprises a rhodium-containing catalytically active component and a halogen-containing promoter component, the halogen being selected from the group consisting of bromine, iodine, bromide compounds, and iodide compounds.
摘要翻译：对羰基化产物具有高活性和选择性的催化剂体系包括含铑催化活性组分和含卤素促进剂组分，卤素选自溴，碘，溴化物和碘化合物。

3. 发明授权

US4060547A Production of dicarboxylic acids 失效
标题翻译：生产二羧酸
公开(公告)号：US4060547A
公开(公告)日：1977-11-29
申请号：US325291
申请日：1973-01-22
申请人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
发明人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
IPC分类号： C07C51/12 , C07C51/14
CPC分类号： C07C51/12
摘要： The present invention relates to a process for the preparation of dicarboxylic acids, specifically by the reaction of non-vicinal glycols; halogen containing derivatives in which the OH radical of the glycol is substituted by Cl, Br, or I; ester derivatives of glycols; and cyclic ether derivatives of glycols; with carbon monoxide in the presence of catalyst compositions essentially comprising rhodium or iridium compounds and complexes, together with a halide promoter.
摘要翻译：本发明涉及二羧酸的制备方法，特别是非邻位二醇的反应。含有卤素的衍生物，其中二醇的OH基被Cl，Br或I取代; 二醇的酯衍生物; 和二醇的环醚衍生物; 在催化剂组合物存在下，一氧化碳基本上包含铑或铱化合物和络合物，以及卤化物促进剂。

4. 发明授权

US6098557A High speed method for producing pant-like garments 失效
标题翻译：制作短裤样服装的高速方法
公开(公告)号：US6098557A
公开(公告)日：2000-08-08
申请号：US338898
申请日：1999-06-23
申请人： Jack L. Couillard , Laurie Couture-Dorschner , Gregory J. Rajala , James F. Roth
发明人： Jack L. Couillard , Laurie Couture-Dorschner , Gregory J. Rajala , James F. Roth
IPC分类号： A41H42/00 , A61F13/15 , A61B9/00 , B32B31/08
CPC分类号： A61F13/15804 , A41H42/00 , Y10T156/1015 , Y10T156/1084
摘要： A method for producing a pant-type garment in which a first substantially rectangular fabric layer is placed on top of a second substantially rectangular fabric layer. The first substantially rectangular fabric layer is joined to the second substantially rectangular fabric layer, forming a multi-layer fabric. A crescent-shaped cutout section is cutout from the opposed multi-layer fabric edges of the multi-layer fabric, forming opposed tabs at each end of the opposed multi-layer fabric having a first tab and a second tab. The multi-layer fabric is cut transversely in half, forming two multi-layer fabric halves. Each of the multi-layer halves is folded longitudinally and the first tab and the second tab on one side of each of the multi-layer fabric halves is joined to the corresponding first tab and second tab on the opposed side of each respective multi-layer fabric half, forming two outside-in pant-like garments.
摘要翻译：一种短裤型服装的制造方法，其中将第一基本上矩形的织物层放置在第二基本矩形的织物层的顶部上。第一基本上矩形的织物层与第二基本上矩形的织物层接合，形成多层织物。从多层织物的相对的多层织物边缘切出新月形的切口部分，在相对的多层织物的每个端部处形成具有第一突片和第二突片的相对的突片。将多层织物横向切成两半，形成两层多层织物。每个多层半部被纵向折叠，并且每个多层织物半部的一侧上的第一突片和第二突片连接到相应的第一突片和在相应的每个相应的多层的第二突出部织物一半，形成两个外在裤子般的衣服。

5. 发明授权

US4792620A Carbonylation catalysts 失效
标题翻译：羰基化催化剂
公开(公告)号：US4792620A
公开(公告)日：1988-12-20
申请号：US21384
申请日：1987-03-03
申请人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
发明人： Frank E. Paulik , Arnold Hershman , Walter R. Knox , James F. Roth
IPC分类号： B01J31/20 , C07C51/10 , C07C51/12 , C07C51/14 , C07C67/36
CPC分类号： B01J31/0231 , B01J31/1895 , B01J31/20 , B01J31/2409 , C07C51/10 , C07C51/12 , C07C51/14 , C07C67/36 , B01J2231/34 , B01J2531/822
摘要： A catalyst system having high activity and selectivity to carbonylation products comprises a rhodium-containing catalytically active component and a halogen-containing promoter component, the halogen being selected from the group consisting of bromine, iodine, bromide compounds, and iodide compounds.
摘要翻译：对羰基化产物具有高活性和选择性的催化剂体系包括含铑催化活性组分和含卤素促进剂组分，卤素选自溴，碘，溴化物和碘化合物。

6. 发明授权

US3989747A Production of propionic acid 失效
标题翻译：丙酸的生产
公开(公告)号：US3989747A
公开(公告)日：1976-11-02
申请号：US473464
申请日：1974-05-28
申请人： John H. Craddock , James F. Roth , Arnold Hershman , Frank E. Paulik
发明人： John H. Craddock , James F. Roth , Arnold Hershman , Frank E. Paulik
IPC分类号： C07C51/14
CPC分类号： C07C51/14
摘要： The present invention relates to an improved one-step process for the preparation of propionic acid, specifically by the reaction of ethylene with carbon monoxide and water at mild pressure, in the presence of catalyst compositions essentially comprising critical proportions of rhodium components with a bromide promoter. Under these reaction conditions, the process is catalytic both with respect to the rhodium and the bromide components.
摘要翻译：本发明涉及一种用于制备丙酸的改进的一步法，特别是在温和压力下乙烯与一氧化碳和水的反应，在催化剂组合物存在下，基本上包含临界比例的铑组分与溴化促进剂。在这些反应条件下，相对于铑和溴化物组分，该方法是催化的。

7. 发明授权

US3989748A Production of propionic acid 失效
标题翻译：丙酸的生产
公开(公告)号：US3989748A
公开(公告)日：1976-11-02
申请号：US473527
申请日：1974-05-28
申请人： Frank E. Paulik , Arnold Hershman , James F. Roth , John H. Craddock
发明人： Frank E. Paulik , Arnold Hershman , James F. Roth , John H. Craddock
IPC分类号： C07C51/14
CPC分类号： C07C51/14
摘要： The present invention relates to an improved one-step process for the preparation of propionic acid, specifically by the reaction of ethylene with carbon monoxide and water at mild pressure, in the presence of catalyst compositions essentially comprising critical proportions of iridium components with a bromide promoter. Under these reaction conditions, the process is catalytic both with respect to the iridium and the bromide components.
摘要翻译：本发明涉及一种用于制备丙酸的改进的一步法，特别是在温和压力下乙烯与一氧化碳和水的反应，在催化剂组合物的存在下，基本上包括临界比例的铱组分与溴化促进剂。在这些反应条件下，相对于铱和溴化物组分，该方法是催化的。

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