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1. 发明授权

US08278237B2 Catalyst for aromatization of lower hydrocarbons and process for production of aromatic compounds 有权
标题翻译：用于低级烃芳构化的催化剂和用于生产芳族化合物的方法
公开(公告)号：US08278237B2
公开(公告)日：2012-10-02
申请号：US12524029
申请日：2008-02-13
申请人： Shinichi Yamada , Tomohiro Yamada , Yuji Ogawa , Hirokazu Akiyama , Takuya Hatagishi
发明人： Shinichi Yamada , Tomohiro Yamada , Yuji Ogawa , Hirokazu Akiyama , Takuya Hatagishi
IPC分类号： B01J29/06 , C07C2/52 , C07C15/00
CPC分类号： C10G45/68 , B01J21/16 , B01J23/885 , B01J29/0308 , B01J29/041 , B01J29/076 , B01J29/40 , B01J29/48 , B01J29/7876 , B01J35/023 , B01J37/0201 , B01J37/088 , B01J37/18 , B01J2229/12 , B01J2229/123 , B01J2229/32 , B01J2229/40 , C01B3/40 , C01B2203/02 , C01B2203/1241 , C07C2/76 , C10G2400/30 , Y02P20/52 , C07C15/02
摘要： A catalyst for producing aromatic compounds from lower hydrocarbons while improving activity life stability of methane conversion rate; benzene formation rate; naphthalene formation rate; and total formation rate of benzene, toluene and xylene is formed by loading molybdenum and copper on metallo-silicate serving as a substrate and then calcining the metallo-silicate. When the catalyst is reacted with a reaction gas containing lower hydrocarbons and carbonic acid gas, aromatic compounds are produced. In order to obtain the catalyst, it is preferable that molybdenum and copper are loaded on zeolite formed of metallo-silicate after the zeolite is treated with a silane compound larger than a pore of the zeolite in diameter and having an amino group and a straight-chain hydrocarbon group, the amino group being able to selectively react with the zeolite at a Bronsted acid point of the zeolite. It is preferable that a loaded amount of molybdenum is within a range of from 2 to 12 wt. % based on total amount of the calcined catalyst while copper is loaded at a copper to molybdenum molar ratio of 0.01 to 0.8.
摘要翻译：一种用于从低级烃生产芳族化合物的催化剂，同时提高甲烷转化率的活性寿命稳定性; 苯形成率; 萘形成率; 苯，甲苯和二甲苯的总形成速率是通过将钼和铜负载在作为基底的金属硅酸盐上，然后煅烧金属硅酸盐而形成的。当催化剂与含有低级烃和碳酸气体的反应气体反应时，产生芳族化合物。为了得到催化剂，优选在沸石用直径大于沸石孔的硅烷化合物进行处理并具有氨基和直链状烷基的情况下，将钼和铜负载在由金属硅酸盐形成的沸石上，链烷烃基，该氨基能够在沸石的布朗斯台德酸点处与沸石选择性反应。钼的负载量优选在2〜12重量％的范围内。基于煅烧催化剂的总量的％，而铜以铜与钼的摩尔比为0.01至0.8。

2. 发明申请

US20100016647A1 CATALYST FOR AROMATIZATION OF LOWER HYDROCARBONS AND PROCESS FOR PRODUCTION OF AROMATIC COMPOUNDS 有权
标题翻译：低碳氢化合物的芳构化催化剂和芳香族化合物的生产方法
公开(公告)号：US20100016647A1
公开(公告)日：2010-01-21
申请号：US12524029
申请日：2008-02-13
申请人： Shinichi Yamada , Tomohiro Yamada , Yuji Ogawa , Hirokazu Akiyama , Takuya Hatagishi
发明人： Shinichi Yamada , Tomohiro Yamada , Yuji Ogawa , Hirokazu Akiyama , Takuya Hatagishi
IPC分类号： C07C2/52 , B01J21/06
CPC分类号： C10G45/68 , B01J21/16 , B01J23/885 , B01J29/0308 , B01J29/041 , B01J29/076 , B01J29/40 , B01J29/48 , B01J29/7876 , B01J35/023 , B01J37/0201 , B01J37/088 , B01J37/18 , B01J2229/12 , B01J2229/123 , B01J2229/32 , B01J2229/40 , C01B3/40 , C01B2203/02 , C01B2203/1241 , C07C2/76 , C10G2400/30 , Y02P20/52 , C07C15/02
摘要： A catalyst for producing aromatic compounds from lower hydrocarbons while improving activity life stability of methane conversion rate; benzene formation rate; naphthalene formation rate; and total formation rate of benzene, toluene and xylene is formed by loading molybdenum and copper on metallo-silicate serving as a substrate and then calcining the metallo-silicate. When the catalyst is reacted with a reaction gas containing lower hydrocarbons and carbonic acid gas, aromatic compounds are produced. In order to obtain the catalyst, it is preferable that molybdenum and copper are loaded on zeolite formed of metallo-silicate after the zeolite is treated with a silane compound larger than a pore of the zeolite in diameter and having an amino group and a straight-chain hydrocarbon group, the amino group being able to selectively react with the zeolite at a Bronsted acid point of the zeolite. It is preferable that a loaded amount of molybdenum is within a range of from 2 to 12 wt. % based on total amount of the calcined catalyst while copper is loaded at a copper to molybdenum molar ratio of 0.01 to 0.8.
摘要翻译：一种用于从低级烃生产芳族化合物的催化剂，同时提高甲烷转化率的活性寿命稳定性; 苯形成率; 萘形成率; 苯，甲苯和二甲苯的总形成速率是通过将钼和铜负载在作为基底的金属硅酸盐上，然后煅烧金属硅酸盐而形成的。当催化剂与含有低级烃和碳酸气体的反应气体反应时，产生芳族化合物。为了得到催化剂，优选在沸石用直径大于沸石孔的硅烷化合物进行处理并具有氨基和直链状烷基的情况下，将钼和铜负载在由金属硅酸盐形成的沸石上，链烷烃基，该氨基能够在沸石的布朗斯台德酸点处与沸石选择性反应。钼的负载量优选在2〜12重量％的范围内。基于煅烧催化剂的总量的％，而铜以铜与钼的摩尔比为0.01至0.8。

3. 发明授权

US4622469A Method for detecting rotten albumen and apparatus therefor 失效
标题翻译：检测烂蛋白的方法及其设备
公开(公告)号：US4622469A
公开(公告)日：1986-11-11
申请号：US706425
申请日：1985-02-27
申请人： Hirokazu Akiyama
发明人： Hirokazu Akiyama
IPC分类号： G01N21/64
CPC分类号： G01N21/6486 , Y10S250/91
摘要： A method and an apparatus for detecting rotten albumen in broken raw eggs which may include sound yolk are disclosed. The apparatus includes a device for casting ultraviolet light onto the albumen, an optical filter system filtering a complex of fluorescence of the albumen and the yolk and an ultraviolet light reflected from or transmitted through the albumen so as to transmit only the components due to fluorescence of the albumen, and a discriminator which compares the level of a signal corresponding to the fluorescence of the albumen to a threshold level corresponding to the fluorescence of the sound albumen. The method and the apparatus are applicable to both separating-type and nonseparating-type automatic egg breakers.
摘要翻译：公开了一种用于检测破碎的生蛋中可能含有蛋黄的烂蛋白的方法和装置。该装置包括用于将紫外光投射到白蛋白上的装置，过滤蛋白和蛋黄的荧光复合物的滤光器系统以及从白蛋白反射或透过白蛋白的紫外线，以便只透过由蛋白和鉴别器，其将与白蛋白的荧光相对应的信号的水平与对应于声音蛋白的荧光的阈值水平进行比较。该方法和装置适用于分离式和非分离式自动蛋清机。

4. 发明授权

US4591723A Optical egg inspecting apparatus 失效
标题翻译：光蛋检测仪器
公开(公告)号：US4591723A
公开(公告)日：1986-05-27
申请号：US706366
申请日：1985-02-27
申请人： Hirokazu Akiyama
发明人： Hirokazu Akiyama
IPC分类号： G01N21/31 , G01N33/08 , G01N21/64
CPC分类号： G01N33/08 , G01N21/314 , Y10S250/91
摘要： An optical egg inspecting apparatus includes a first transducer unit having a first sensitivity range of 400 to 500 nm in wavelength which corresponds to the absorption spectrum range of yolk (the yellow) and a second transducer unit having a second sensitivity range of 500 to 700 nm in wavelength which corresponds to the visual range excluding the first range. Therefore, the first transducer unit can detect eggshells but cannot detect the yolk, while the second transducer unit can detect both shells or yolk. When the first unit does not detect shells and additionally the second unit detects yolk, the presence of yolk included in egg white is decided even where the egg white includes shells. Further, the two transducer units cannot detect the presence of egg white because a polarized beam projected onto and reflected from egg white to be inspected is shut off by an analyzer having polarization axes arranged perpendicular to those of the polarized beam.
摘要翻译：光学蛋检查装置包括第一传感器单元，其具有对应于蛋黄（黄色）的吸收光谱范围的波长为400至500nm的第一灵敏度范围和具有500至700nm的第二灵敏度范围的第二换能器单元其对应于除了第一范围之外的视觉范围。因此，第一传感器单元可以检测蛋壳，但不能检测蛋黄，而第二传感器单元可检测壳或蛋黄。当第一单元不检测贝壳，另外单元检测蛋黄时，蛋清中包含的蛋黄的存在即使蛋白包括壳也是决定的。此外，两个换能器单元不能检测到蛋清的存在，因为投射到蛋清上并被反射的被检查的偏振光束被具有垂直于偏振光束的偏振轴的分析器切断。

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