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1. 发明授权

US4431565A Surface-active compounds, a process for their preparation and their use 失效
标题翻译：表面活性化合物，其制备方法及其用途
公开(公告)号：US4431565A
公开(公告)日：1984-02-14
申请号：US436329
申请日：1982-10-25
申请人： Siegfried Billenstein , Hildegard Freundl , Ignaz Wimmer , Fritz J. Gohlke , Johannes Macenka
发明人： Siegfried Billenstein , Hildegard Freundl , Ignaz Wimmer , Fritz J. Gohlke , Johannes Macenka
IPC分类号： C11D1/72 , B01D17/04 , B01D17/05 , B01F17/00 , B01F17/42 , B01F17/52 , C08G4/00 , C08G8/00 , C08G8/12 , C08G8/28 , C08G8/36 , C08G65/26 , C08L7/00 , C08L21/00 , C08L61/00 , C08L61/04 , C08L61/14 , C10G33/04 , C10L1/192 , C10L1/195 , C10L1/198
CPC分类号： C08G8/36 , B01D17/047 , B01F17/0028 , C08G4/00 , C08G65/2612 , C10G33/04
摘要： The new compounds consist essentially of ethylene oxide/propylene oxide block polymer units and oxyalkyleneated alkylphenol/aldehyde resin units, which are linked by methylene groups. They are prepared by reacting a block polymer of ethylene oxide and propylene oxide and an oxyalkyleneated alkylphenol/aldehyde resin with formaldehyde. The new compounds constitute especially advantageous breaking agents for petroleum.
摘要翻译：新化合物基本上由环氧乙烷/环氧丙烷嵌段聚合物单元和氧亚烷基化的烷基酚/醛树脂单元组成，它们通过亚甲基连接。它们通过使环氧乙烷和环氧丙烷的嵌段聚合物和氧化亚烷基化的烷基酚/醛树脂与甲醛反应来制备。新化合物构成了特别有利的石油破碎剂。

2. 发明申请

US20070027040A1 Mineral oils with improved conductivity and cold flowability 失效
标题翻译：具有改善导电性和冷流动性的矿物油
公开(公告)号：US20070027040A1
公开(公告)日：2007-02-01
申请号：US11494931
申请日：2006-07-28
申请人： Matthias Krull , Klaus Mikulecky , Carsten Cohrs , Hildegard Freundl
发明人： Matthias Krull , Klaus Mikulecky , Carsten Cohrs , Hildegard Freundl
IPC分类号： C07C309/62 , C09K15/08
CPC分类号： C10L1/143 , C10L1/1641 , C10L1/1963 , C10L1/1973 , C10L1/1981 , C10L1/1985 , C10L1/2222 , C10L1/223 , C10L1/224 , C10L1/232 , C10L1/233 , C10L1/238 , C10L10/02 , C10L10/16
摘要： The invention provides compositions comprising at least one alkylphenol resin (constituent I) and, based on the alkylphenol resin, from 0.05 to 10% by weight of at least one salt of an aromatic base and of a sulfonic acid (constituent II).
摘要翻译：本发明提供了包含至少一种烷基酚树脂（组分I）和基于烷基酚树脂的0.05至10重量％的至少一种芳族碱和磺酸盐（组分II）的组合物。

3. 发明申请

US20080045666A1 Process for preparing polyoxyalkylene glycol ethers using alkoxylated alkylphenol-aldehyde resins as demulsifiers 审中-公开
标题翻译：使用烷氧基化烷基酚醛树脂作为破乳剂制备聚氧亚烷基二醇醚的方法
公开(公告)号：US20080045666A1
公开(公告)日：2008-02-21
申请号：US11893900
申请日：2007-08-17
申请人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
发明人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
IPC分类号： C08F8/02
CPC分类号： C08G65/329
摘要： The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and a compound of the formula 1 in which R2 is a straight-chain or branched C1- to C20-alkyl radical, p is from 1 to 75, X is one 1,2-alkylene group or different 1,2-alkylene groups having from 2 to 4 carbon atoms, and k is from 1 to 200 to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.
摘要翻译：本发明提供了通过使烷氧基化物与烷基化剂反应制备聚氧亚烷基二醇单醚和/或二醚的方法，该方法包括加入水和其中R 2为直链的式1化合物或支链C 1至C 20 - 烷基，p为1至75，X为一个1,2-亚烷基或不同的1,2-亚烷基具有2至4个碳原子，并且k对于形成的醇盐，烷基化剂和聚氧亚烷基二醇醚的混合物为1至200。

4. 发明申请

US20080045652A1 Process for preparing polyoxyalkylene glycol ethers using alkoxylated oligo- or polyethyleneimines as demulsifiers 审中-公开
标题翻译：使用烷氧基化的寡聚或聚乙烯亚胺作为破乳剂制备聚氧亚烷基二醇醚的方法
公开(公告)号：US20080045652A1
公开(公告)日：2008-02-21
申请号：US11893923
申请日：2007-08-17
申请人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
发明人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
IPC分类号： C08G67/00
CPC分类号： C08G65/329
摘要： The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and oligo- or polyethyleneimines which have been alkoxylated with from 1 to 100 C2- to C4-alkylene oxide groups or a mixture of such alkylene oxide groups per free NH group to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.
摘要翻译：本发明提供了通过使烷氧基化物与烷基化剂反应来制备聚氧亚烷基二醇单醚和/或二醚的方法，该方法包括加入水和低聚或聚乙烯亚胺，所述低聚或聚乙烯亚胺在1至100℃2 - 至C 4 - 亚烷基氧基或每个游离NH基团的这种烯化氧基团的混合物与形成的醇盐，烷基化剂和聚氧亚烷基二醇醚的混合物。

5. 发明授权

US08133852B2 Mineral oils with improved conductivity and cold flowability 失效
标题翻译：具有改善导电性和冷流动性的矿物油
公开(公告)号：US08133852B2
公开(公告)日：2012-03-13
申请号：US11494931
申请日：2006-07-28
申请人： Matthias Krull , Klaus Mikulecky , Carsten Cohrs , Hildegard Freundl
发明人： Matthias Krull , Klaus Mikulecky , Carsten Cohrs , Hildegard Freundl
IPC分类号： C10M139/00 , C07C309/62
CPC分类号： C10L1/143 , C10L1/1641 , C10L1/1963 , C10L1/1973 , C10L1/1981 , C10L1/1985 , C10L1/2222 , C10L1/223 , C10L1/224 , C10L1/232 , C10L1/233 , C10L1/238 , C10L10/02 , C10L10/16
摘要： The invention provides compositions comprising at least one alkylphenol resin (constituent I) and, based on the alkylphenol resin, from 0.05 to 10% by weight of at least one salt of an aromatic base and of a sulfonic acid (constituent II).
摘要翻译：本发明提供了包含至少一种烷基酚树脂（组分I）和基于烷基酚树脂的0.05至10重量％的至少一种芳族碱和磺酸盐（组分II）的组合物。

6. 发明授权

US07776111B2 Mineral oils with improved conductivity and cold flowability 有权
标题翻译：具有改善导电性和冷流动性的矿物油
公开(公告)号：US07776111B2
公开(公告)日：2010-08-17
申请号：US11185387
申请日：2005-07-20
申请人： Matthias Krull , Carsten Cohrs , Hildegard Freundl , Stefan Lorenz
发明人： Matthias Krull , Carsten Cohrs , Hildegard Freundl , Stefan Lorenz
IPC分类号： C08K5/41
CPC分类号： C10L1/143 , C10L1/1641 , C10L1/195 , C10L1/1955 , C10L1/1963 , C10L1/1973 , C10L1/198 , C10L1/1981 , C10L1/1985 , C10L1/221 , C10L1/2222 , C10L1/2225 , C10L1/224 , C10L1/2364 , C10L1/2437 , C10L10/14
摘要： The invention provides compositions comprising at least one alkylphenol-aldehyde resin (constituent I) and, based on the alkylphenol resin, from 0.005 to 10% by weight of at least one oil-soluble organic ammonium sulfonate (constituent II).
摘要翻译：本发明提供包含至少一种烷基酚醛树脂（组分I）和基于烷基酚树脂0.005至10重量％的至少一种油溶性有机磺酸铵（组分II）的组合物。

7. 发明申请

US20080045667A1 Process for preparing polyoxyalkylene glycol ethers using block polymers as demulsifiers 审中-公开
标题翻译：使用嵌段聚合物作为破乳剂制备聚氧亚烷基二醇醚的方法
公开(公告)号：US20080045667A1
公开(公告)日：2008-02-21
申请号：US11894014
申请日：2007-08-17
申请人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
发明人： Alexander Snell , Carsten Cohrs , Gabriele Oberendfellner , Hildegard Freundl
IPC分类号： C08F8/02
CPC分类号： C08G65/329 , C08G65/2696
摘要： The invention provides a process for preparing polyoxyalkylene glycol monoethers and/or diethers by reacting an alkoxide with an alkylating agent, which comprises adding water and block polymers which are obtainable from a compound which comprises from 1 to 30 carbon atoms and from 1 to 25 hydroxyl groups, amino groups or both by its blockwise alkoxylation with at least 2 different blocks of in each case from 1 to 200 mol of C2- to C4-alkylene oxide to the mixture of alkoxide, alkylating agent and polyoxyalkylene glycol ether which has formed.
摘要翻译：本发明提供了一种通过使烷氧基化物与烷基化剂反应来制备聚氧亚烷基二醇单醚和/或二醚的方法，该方法包括加入水和嵌段聚合物，该聚合物可从含有1至30个碳原子的化合物和1至25个羟基基团，氨基或两者通过其阻断性烷氧基化与至少2个不同的嵌段在每种情况下为1至200摩尔C 2至C 4 - 亚烷基氧基至形成的醇盐，烷化剂和聚氧亚烷基二醇醚的混合物。

8. 发明申请

US20060020065A1 Mineral oils with improved conductivity and cold flowability 有权
标题翻译：具有改善导电性和冷流动性的矿物油
公开(公告)号：US20060020065A1
公开(公告)日：2006-01-26
申请号：US11185387
申请日：2005-07-20
申请人： Matthias Krull , Carsten Cohrs , Hildegard Freundl , Stefan Lorenz
发明人： Matthias Krull , Carsten Cohrs , Hildegard Freundl , Stefan Lorenz
IPC分类号： C08K5/41
CPC分类号： C10L1/143 , C10L1/1641 , C10L1/195 , C10L1/1955 , C10L1/1963 , C10L1/1973 , C10L1/198 , C10L1/1981 , C10L1/1985 , C10L1/221 , C10L1/2222 , C10L1/2225 , C10L1/224 , C10L1/2364 , C10L1/2437 , C10L10/14
摘要： The invention provides compositions comprising at least one alkylphenol-aldehyde resin (constituent I) and, based on the alkylphenol resin, from 0.005 to 10% by weight of at least one oil-soluble organic ammonium sulfonate (constituent II).
摘要翻译：本发明提供包含至少一种烷基酚醛树脂（组分I）和基于烷基酚树脂0.005至10重量％的至少一种油溶性有机磺酸铵（组分II）的组合物。

9. 发明申请

US20050203193A1 Demulsifiers 审中-公开
标题翻译：破乳剂
公开(公告)号：US20050203193A1
公开(公告)日：2005-09-15
申请号：US10515897
申请日：2003-05-16
申请人： Dirk Leinweber , Michael Feustel , Heidi Grundner , Hildegard Freundl
发明人： Dirk Leinweber , Michael Feustel , Heidi Grundner , Hildegard Freundl
IPC分类号： B01D17/04 , B01D17/05 , C08G59/14 , C08G59/34 , C08G65/26 , C10G33/04
CPC分类号： C08G59/027 , B01D17/047 , C08G59/1477 , C08G59/1494 , C08G65/2624 , C08G2650/34 , C10G33/04
摘要： The invention relates to polymers that can be obtained by: A) reacting an epoxidized ester, which is selected from one or more unsaturated fatty acids having 8 to 26 C atoms and a polyol having 2 to 6 OH groups, with a monoamine, diamine or polyamine; B) alkoxylating the polyamine obtained hereby with a C2 to C4 alkylene oxide in molar excess so that the average degree of alkoxylation per OH group ranges from 1 to 100. The polymers have a numerical average molecular weight ranging from 500 to 100,000 g/mol. The invention also relates to the use of these polymers in quantities ranging from 0.0001 to 5% by weight with regard to the oil as demulsifiers for oil-in-water emulsions.
摘要翻译：本发明涉及可以通过以下方法获得的聚合物：A）使选自具有8至26个C原子的一种或多种不饱和脂肪酸和具有2-6个OH基团的多元醇的环氧化酯与单胺，二胺或多胺 B）以C摩尔过量的方式将C 2 N 2 C 2 C 2 O 3烷氧基化，使得每OH基团的平均烷氧基化度在1至100范围内。聚合物的数均分子量为500〜100,000g / mol。本发明还涉及这些聚合物在0.0001至5重量％范围内的用途，作为油包水乳液的破乳剂。

10. 发明授权

US06365541B1 Alkoxylation catalyst 失效
标题翻译：烷氧基化催化剂
公开(公告)号：US06365541B1
公开(公告)日：2002-04-02
申请号：US09257630
申请日：1999-02-25
申请人： Ignaz Wimmer , Hildegard Freundl
发明人： Ignaz Wimmer , Hildegard Freundl
IPC分类号： B01J3100
CPC分类号： C08G65/2642 , B01J31/04 , B01J2231/4288 , C07C41/03 , C07C67/26 , C07C69/24 , C07C43/11 , C07C43/1785
摘要： An alkoxylation catalyst is prepared by a) reaction of one mol of a dicarboxylic acid with from 1.5 to 8 mol of an alkoxylated alcohol to form the corresponding dicarboxylic monoester, b) formation of an alkaline earth metal salt of the dicarboxylic monoester by addition of water and from 0.45 to 0.55 mol of a basic alkaline earth metal compound per mol of dicarboxylic acid originally used, c) partial neutralization of the alkaline earth metal salt by addition of from 0.25 to 0.7 mol of H2SO4 per mol of basic alkaline earth metal compound originally used and d) removal of the water present at a temperature of less than 100° C. The catalyst prepared in this way makes it possible to prepare colorless alkoxylates having a narrow homologue distribution.
摘要翻译：通过a）使一摩尔二羧酸与1.5至8摩尔烷氧基化醇反应形成相应的二羧酸单酯来制备烷氧基化催化剂，b）通过加入水形成二羧酸单酯的碱土金属盐;和原始使用的每摩尔二羧酸为0.45〜0.55摩尔的碱土金属化合物，c）通过加入0.25〜0.7摩尔H 2 SO 4 /摩尔碱性碱土金属化合物，最初使用的部分中和和d）去除在低于100℃的温度下存在的水。以这种方式制备的催化剂使得可以制备具有窄的同系物分布的无色烷氧基化物。

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