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1. 发明申请

US20080039642A1 Practical, Cost-Effective Synthesis of Chloromethylated 1, 4-Benzoquinones 审中-公开
标题翻译：氯甲基化1,4-苯醌的实用，经济有效的合成
公开(公告)号：US20080039642A1
公开(公告)日：2008-02-14
申请号：US11575749
申请日：2005-09-17
申请人： Volker Berl , Frank Wetterich , Hansgeorg Ernst , Karin Schein
发明人： Volker Berl , Frank Wetterich , Hansgeorg Ernst , Karin Schein
IPC分类号： C07C50/28
CPC分类号： C07C46/00 , C07C46/08 , C07C50/28
摘要： The present invention relates to a practical and cost-effective method for the synthesis of 5-chloromethylated 2,3-dialkoxy-6-alkyl-1,4-benzoquinones by direct chloromethylation of the corresponding 2,3-dialkoxy-6-alkyl-1,4-benzoquinones. The invention further relates to a method for the preparation of 5-chloromethylated 2,3-dialkoxy-6-alkyl-1,4-benzoquinones starting from a 3,4,5-trialkoxy-1-alkyl-benzene. The invention also relates to a method for the production of Coenzymes Qn, especially coenzyme Q10.
摘要翻译：本发明涉及通过相应的2,3-二烷氧基-6-烷基-1,4-苯醌的直接氯甲基化合成5-氯甲基化2,3-二烷氧基-6-烷基-1,4-苯醌的实用和成本有效的方法。 1,4-苯醌。本发明还涉及从3,4,5-三烷氧基-1-烷基 - 苯开始制备5-氯甲基化2,3-二烷氧基-6-烷基-1,4-苯醌的方法。本发明还涉及生产辅酶Q 1，特别是辅酶Q 10的方法。

2. 发明申请

US20050148675A1 Practical, cost-effective synthesis of ubiquinones 审中-公开
标题翻译：泛素的实用，经济有效的合成
公开(公告)号：US20050148675A1
公开(公告)日：2005-07-07
申请号：US11003544
申请日：2004-12-03
申请人： Bruce Lipshutz , Volker Berl , Karin Schein , Frank Wetterich
发明人： Bruce Lipshutz , Volker Berl , Karin Schein , Frank Wetterich
IPC分类号： A61K31/12 , A61K31/122 , C07C17/16 , C07C39/10 , C07C46/00 , C07C46/06 , C07C46/10 , C07C50/26 , C07C50/28 , C07C50/38 , C07F9/09 , C07F9/117 , C07F9/32 , C07F9/44 , C12Q20060101
CPC分类号： C07F9/094 , B01J31/2404 , B01J2231/4205 , B01J2531/847 , C07C17/16 , C07C39/10 , C07C46/00 , C07C46/06 , C07C46/10 , C07C50/28 , C07C50/38 , C07F9/117 , C07F9/3223 , C07F9/3241 , C07F9/4446 , C07F9/4453 , C07C21/04
摘要： The present invention provides a convergent method for the synthesis of ubiquinones and ubiquinone analogues. Also provided are precursors of ubiquinones and their analogues that are useful in the methods of the invention. The invention further provides an improved method for the carboalumination of alkyne substrates.
摘要翻译：本发明提供了一种用于合成泛醌和泛醌类似物的收敛方法。还提供了可用于本发明方法的泛醌及其类似物的前体。本发明进一步提供了一种用于炔底物的碳照射的改进方法。

3. 发明授权

US6124345A Carbamoyl carboxylic acid amide oximes 失效
标题翻译：氨基甲酰基羧酰胺肟
公开(公告)号：US6124345A
公开(公告)日：2000-09-26
申请号：US147305
申请日：1998-11-24
申请人： Frank Wetterich , Karl Eicken , Reinhard Kirstgen , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
发明人： Frank Wetterich , Karl Eicken , Reinhard Kirstgen , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
IPC分类号： A01N47/12 , C07C271/22 , C07D333/28 , A01N43/06 , A01N37/12 , A01N37/18 , A01N37/44 , A01N53/00
CPC分类号： C07C271/22 , A01N47/12 , C07D333/28
摘要： The present invention relates to carbomoylcarboxamide oximes of the formula (I): ##STR1## or salts thereof, processes for preparing the carbomoylcarboxamide oximes, compositions containing the carbomoylcarboxamide oximes and processes for controlling harmful fungi with an effective amount of the carbomoylcarboxamide oximes.
摘要翻译： PCT No.PCT / EP97 / 02687第 371日期：1998年11月24日 102（e）1998年11月24日PCT PCT 1997年5月26日PCT公布。第WO97 / 46518号公报日期：1997年12月11日本发明涉及式（I）的甲酰甲酰甲酰胺肟或其盐，制备羧甲酰甲酰胺肟的方法，含有甲酰甲酰甲脒肟的组合物和有效量的甲酰甲酰甲脒肟的有害真菌控制方法。

4. 发明申请

US20090131705A1 Practical, Cost-Effective Synthesis of Ubiquinones 审中-公开
标题翻译：实用，经济有效的泛醌的合成
公开(公告)号：US20090131705A1
公开(公告)日：2009-05-21
申请号：US12096372
申请日：2006-12-12
申请人： Bruce H. Lipshutz , Volker Berl , Karin Schein , Frank Wetterich
发明人： Bruce H. Lipshutz , Volker Berl , Karin Schein , Frank Wetterich
IPC分类号： C07F5/06 , C07C49/403
CPC分类号： C07C17/263 , C07C5/333 , C07C17/16 , C07C46/00 , C07C46/08 , C07C2531/14 , C07F5/062 , C07C15/46 , C07C21/04 , C07C25/24 , C07C50/28 , C07C50/38
摘要： The present invention provides a convergent method for the synthesis of ubiquinones and ubiquinone analogues. Also provided are precursors of ubiquinones and their analogues that are useful in the methods of the invention. The invention further provides an improved method for the carboalumination of alkyne substrates.
摘要翻译：本发明提供了一种用于合成泛醌和泛醌类似物的收敛方法。还提供了可用于本发明方法的泛醌及其类似物的前体。本发明进一步提供了一种用于炔底物的碳照射的改进方法。

5. 发明授权

US06680402B2 Benzamidoxime derivatives, intermediates and processes for their preparation, and their use as fungicides 失效
标题翻译：苯甲酰胺肟衍生物，中间体及其制备方法及其作为杀真菌剂的用途
公开(公告)号：US06680402B2
公开(公告)日：2004-01-20
申请号：US10261122
申请日：2002-10-01
申请人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
发明人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
IPC分类号： C07C25549
CPC分类号： C07D333/24 , A01N37/52 , A01N43/10 , A01N43/56 , C07C255/53 , C07C255/54 , C07C259/18
摘要： Benzamidoxime derivatives of the formula I: where R1 is difluoromethyl or trifluoromethyl R2 is hydrogen or fluorine R3 is C1-C4-alkyl which may be substituted by cyano, C1-C4-haloalkyl, C1-C4-alkoxy-C1-C4-alkyl, C3-C6-alkenyl, C3-C6-haloalkenyl, C3-C6-alkynyl, C3-C8-cycloalkyl-C1-C4-alkyl R4 is phenyl-C1-C6-alkyl which may carry one or more substitutents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the phenyl ring, or is thienyl-C1-C4-alkyl which may carry one or more substituents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the thienyl ring, or is pyrazolyl-C1-C4-alkyl which may carry one or more substituents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the pyrazole ring, are prepared, and intermediates for their preparation and their use as fungicides are described.
摘要翻译：式I的苯甲酰胺肟衍生物：其中R 1是二氟甲基或三氟甲基R 2是氢或氟，R 3是可以被氰基，C 1 -C 4卤代烷基，C 1 -C 4 - 烷氧基 - C 1 -C 4 - 烷基，C 3 -C 6 - 烯基，C 3 -C 6 - 卤代烯基，C 3 -C 6 - 炔基，C 3 -C 8 - 环烷基-C 1 -C 4 - 烷基R 4是苯基-C 1 -C 6 - 或更多的选自苯基环上的卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基的取代基，可以携带的噻吩基-C 1 -C 4烷基一个或多个选自噻吩基环上的卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基的取代基，其可以是吡唑基-C 1 -C 4烷基，在吡唑环上携带一个或多个选自卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基的取代基，制备中间体和描述了它们作为杀真菌剂的用途。

6. 发明申请

US20110137084A1 METHOD FOR PRODUCING PURE OR ENRICHED Q10 COENZYME 审中-公开
标题翻译：生产纯或Q10聚苯乙烯的方法
公开(公告)号：US20110137084A1
公开(公告)日：2011-06-09
申请号：US11722455
申请日：2005-12-17
申请人： Volker Berl , Karin Schein , Frank Wetterich
发明人： Volker Berl , Karin Schein , Frank Wetterich
IPC分类号： C07C46/10
CPC分类号： C07C46/10 , C07C50/28
摘要： The present invention relates to a method for isolating coenzyme Q10 of formula (I) by separating material mixtures containing coenzyme Q10 and the compound of formula (II)
摘要翻译：本发明涉及通过分离含有辅酶Q10的物质混合物和式（II）化合物来分离式（I）的辅酶Q10的方法，

7. 发明授权

US06509501B2 Benzamidoxime derivatives, intermediates and processes for their preparation, and their use as fungicides 失效
标题翻译：苯甲酰胺肟衍生物，中间体及其制备方法及其作为杀真菌剂的用途
公开(公告)号：US06509501B2
公开(公告)日：2003-01-21
申请号：US10093634
申请日：2002-03-11
申请人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
发明人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
IPC分类号： C07C25148
CPC分类号： C07D333/24 , A01N37/52 , A01N43/10 , A01N43/56 , C07C255/53 , C07C255/54 , C07C259/18
摘要： Benzamidoxime derivatives of the formula I where R1 is difluoromethyl or trifluoromethyl R2 is hydrogen or fluorine R3 is C1-C4-alkyl which may be substituted by cyano, C1-C4-haloalkyl, C1-C4-alkoxy-C1-C4-alkyl, C3-C6-alkenyl, C3-C6-haloalkenyl, C3-C6-alkynyl, C3-C8-cycloalkyl-C1-C4-alkyl R4 is phenyl-C1-C6-alkyl which may carry one or more substitutents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the phenyl ring, or is thienyl-C1-C4-alkyl which may carry one or more substituents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the thienyl ring, or is pyrazolyl-C1-C4-alkyl which may carry one or more substituents selected from the group consisting of halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy and C1-C4-haloalkoxy on the pyrazole ring, are prepared, and intermediates for their preparation and their use as fungicides are described.
摘要翻译：式I的苯甲酰胺肟衍生物，其中R 1是二氟甲基或三氟甲基，R 2是氢或氟，R 3是可被氰基，C 1 -C 4卤代烷基，C 1 -C 4 - 烷氧基-C 1 -C 4 - 烷基，C 3 -C 6 - 烯基，C 3 -C 6 - 卤代链烯基，C 3 -C 6 - 炔基，C 3 -C 8 - 环烷基-C 1 -C 4 - 烷基基团R 4是苯基-C 1 -C 6 - 烷基，其可以带有一个或多个选自卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基，可以带有一个或多个选自卤素，C 1 -C 4 - 在噻吩环上的C 1 -C 4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基，可以带有一个或多个选自卤素，C 1 -C 4 - C 1-4 - 烷基，C 1 -C 4 - 卤代烷基，C 1 -C 4 - 烷氧基和C 1 -C 4 - 卤代烷氧基，并且描述了制备中间体及其作为杀真菌剂的用途。

8. 发明授权

US06420605B1 Benzamidoxim derivatives, intermediate products and methods for preparing and using them as fungicides 失效
标题翻译：苯甲酰胺衍生物，中间产物和制备和使用它们作为杀真菌剂的方法
公开(公告)号：US06420605B1
公开(公告)日：2002-07-16
申请号：US09508597
申请日：2000-03-14
申请人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
发明人： Karl Eicken , Joachim Rheinheimer , Frank Wetterich , Eberhard Ammermann , Gisela Lorenz , Siegfried Strathmann
IPC分类号： C07C23304
CPC分类号： C07D333/24 , A01N37/52 , A01N43/10 , A01N43/56 , C07C255/53 , C07C255/54 , C07C259/18
摘要： The invention relates to benzamidoxim derivatives of formula (I) wherein the substituents have the following meanings: R1 represents difluoromethyl or trifluoromethyl, R2 represents hydrogen or fluorine, R3 represents C1-C4 alkyl optionally substituted with cyano, C1-C4 halogenalkyl, C1-C4 alkoxy-C1-C4 alkyl, C3-C6 alkenyl, C3-C6 halogenalkenyl, C3-C6 alkinyl, C3-C8 cycloalkyl-C1-C4 alkyl, R4 represents phenyl-C1-C6 alkyl, which can carry one or more substituents selected from the group composed of halogen, C1-C4 alkyl, C1-C4 halogenalkyl, C1-C4 alkoxy or C1-C4 halogenalkoxy on the phenyl ring, or thienyl-C1-C4 alkyl, which can carry one or more substituents selected from the group composed of halogen, C1-C4 alkyl, C1-C4 halogenalkyl, C1-C4 halogenalkoxy on the thienyl ring, or pyrazol-C1-C4 alkyl, which can carry one or more substituents selected from the group composed of halogen, C1-C4 alkyl, C1-C4 halogenalkyl, C1-C4 alkoxy or C1-C4 halogenalkoxy on the pyrazol ring. The invention also relates to intermediate products for the preparation of these derivatives and to their use as fungicides.
摘要翻译：本发明涉及式（I）的苯甲酰氨基亚胺衍生物，其中取代基具有以下含义：R 1表示二氟甲基或三氟甲基，R 2表示氢或氟，R 3表示任选被氰基，C 1 -C 4卤代烷基，C 1 -C 4 烷氧基-C 1 -C 4烷基，C 3 -C 6烯基，C 3 -C 6卤代链烯基，C 3 -C 6炔基，C 3 -C 8环烷基-C 1 -C 4烷基，R 4表示苯基-C 1 -C 6烷基，其可以携带一个或多个选自由苯基环上的卤素，C 1 -C 4烷基，C 1 -C 4卤代烷基，C 1 -C 4烷氧基或C 1 -C 4卤代烷氧基组成的基团，或可以携带一个或多个选自组成的基团的噻吩基-C 1 -C 4烷基卤素，C 1 -C 4烷基，C 1 -C 4卤代烷基，噻吩基上的C 1 -C 4卤代烷氧基或吡唑基-C 1 -C 4烷基，其可以携带一个或多个选自卤素，C 1 -C 4烷基，吡唑环上的C 1 -C 4卤代烷基，C 1 -C 4烷氧基或C 1 -C 4卤代烷氧基。本发明还涉及用于制备这些衍生物的中间产物及其作为杀真菌剂的用途。

9. 发明授权

US06265447B1 Cycloalkylalkanecarboxamides and the production and use thereof 失效
标题翻译：环烷基烷烃甲酰胺及其制备和应用
公开(公告)号：US06265447B1
公开(公告)日：2001-07-24
申请号：US09381050
申请日：1999-09-14
申请人： Frank Wetterich , Karl Eicken , Gisela Lorenz , Eberhard Ammermann , Siegfried Strathmann , Ingo Rose
发明人： Frank Wetterich , Karl Eicken , Gisela Lorenz , Eberhard Ammermann , Siegfried Strathmann , Ingo Rose
IPC分类号： A01N3718
CPC分类号： C07C255/58 , A01N37/34 , C07C255/31 , C07C2601/02 , C07C2601/08
摘要： The present invention relates to novel cycloalkylalkane-carboxamides of the formula I where the substituents have the following meanings: A is C3-C6-cycloalkyl; R1 is C1-C6-alkyl or C2-C6-alkenyl; R2, R3 and R4 are hydrogen or, independently of this meaning, have one of the meanings of the radical R1; n is 0 or 1; Y is cyano or halogen; w is phenyl, naphthyl or heteroaryl.
摘要翻译：本发明涉及式I的新的环烷基烷烃 - 甲酰胺，其中取代基具有以下含义：A为C 3 -C 6 - 环烷基; R 1为C 1 -C 6 - 烷基或C 2 -C 6 - 烯基; R 2，R 3和R 4为氢或独立于该含义，具有基团R 1的含义之一; n为0或1; Y为氰基或卤素; w为苯基，萘基或杂芳基。

10. 发明授权

US06090853A Fungicidally active carboxylic acid amides 失效
标题翻译：杀真菌活性羧酸酰胺
公开(公告)号：US06090853A
公开(公告)日：2000-07-18
申请号：US155099
申请日：1998-09-21
申请人： Frank Wetterich , Oliver Wagner , Karl Eicken , Eberhard Ammermann , Siegfried Strathmann , Gisela Lorenz , John-Bryan Speakman
发明人： Frank Wetterich , Oliver Wagner , Karl Eicken , Eberhard Ammermann , Siegfried Strathmann , Gisela Lorenz , John-Bryan Speakman
IPC分类号： C07C231/02 , A01N37/18 , A01N37/34 , C07C233/58 , C07C233/59 , C07C233/60 , C07C253/30 , C07C255/47 , C07C255/60
CPC分类号： C07C233/59 , C07C233/58 , C07C233/60 , C07C255/47 , C07C255/60 , C07C2102/42 , C07C2103/68 , C07C2103/74
摘要： Carboxamides of the formula I ##STR1## where the substituents have the following meanings: R.sup.1 is unsubstituted or substituted bicycloalkyl, tricycloalkyl or bicycloalkenyl;R.sup.2,R.sup.3 and R.sup.4 are each, independently of one another, hydrogen, or unsubstituted or substituted: alkyl, cycloalkyl, cycloalkenyl or heterocyclyl;Ar is unsubstituted or substituted aryl or hetaryl,but excluding 2-cyano-N-[1-(1-naphthyl)ethyl]-3-phenyl-bicyclo[2.2.1]hept-5-ene-2-carboxamide, a process for their preparation, compositions comprising compounds I and the use of compounds I for preparing the compositions, and further a process for controlling harmful fungi and the use of the compounds I for this purpose.
摘要翻译： PCT No.PCT / EP97 / 01161 Sec。 371日期：1998年9月21日 102（e）1998年9月21日PCT PCT 1997年3月7日PCT公布。公开号WO97 / 35838 日期1997年10月2日具有下列含义的式I的酰胺：R1是未取代的或取代的双环烷基，三环烷基或双环烯基; R2，R3和R4彼此独立地为氢，或未取代或取代的：烷基，环烷基，环烯基或杂环基; Ar是未取代或取代的芳基或杂芳基，但不包括2-氰基-N- [1-（1-萘基）乙基] -3-苯基 - 双环[2.2.1]庚-5-烯-2-甲酰胺，用于制备组合物，包含化合物I的组合物和化合物I用于制备组合物的用途，以及用于控制有害真菌的方法和用于该目的的化合物I的用途。

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