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1. 发明授权

US08921512B2 Process for forming an aramid copolymer 有权
标题翻译：形成芳族聚酰胺共聚物的方法
公开(公告)号：US08921512B2
公开(公告)日：2014-12-30
申请号：US13559659
申请日：2012-07-27
申请人： Frederick K Mallon
发明人： Frederick K Mallon
IPC分类号： C08G73/00 , C08G69/00 , C08G73/18 , C08G69/28 , C08G69/32
CPC分类号： C08G69/00 , C08G69/28 , C08G69/32 , C08G73/18
摘要： The invention concerns processes for forming polymer crumb comprising residues of 2-(4-amino phenyl)-5(6)amino benzimidazole (DAPBI), paraphenylene diamine (PPD), and terephthaloyl dichloride, comprising the steps of: (a) forming a slurry of b mole percent DAPBI and y mole percent PPD in a solvent system comprising organic solvent and c weight percent of an inorganic salt, wherein the inorganic salt is present in an amount of at least 5 weight percent of the organic solvent, DAPBI and PPD being present in an amount sufficient for providing a polymer solution having a weight percent solids of 12 percent or greater on a polymer basis; and (b) contacting the slurry of step a) with a stoichiometric amount of terephthaloyl dichloride to form a product comprising the polymer; wherein the sum of y+b is 100 and the product of b×c is 225 or greater.
摘要翻译：本发明涉及形成包含2-（4-氨基苯基）-5（6）氨基苯并咪唑（DAPBI），对苯二胺（PPD）和对苯二酰氯的残留物的聚合物碎屑的方法，包括以下步骤：（a）在含有机溶剂和c％重量百分比的无机盐的溶剂体系中，B摩尔％DAPBI和y摩尔％PPD的浆料，其中无机盐以有机溶剂DAPBI和PPD的至少5重量％的量存在以足够的量存在，以提供基于聚合物的重量百分比固体含量为12％或更高的聚合物溶液; 和（b）使步骤a）的浆料与化学计量的对苯二酰氯接触以形成包含聚合物的产物; 其中y + b的和为100，b×c的乘积为225以上。

2. 发明授权

US08716430B2 Aramid copolymer 有权
标题翻译：芳族聚酰胺共聚物
公开(公告)号：US08716430B2
公开(公告)日：2014-05-06
申请号：US13559657
申请日：2012-07-27
申请人： Frederick K Mallon
发明人： Frederick K Mallon
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G69/00 , C08G69/28 , C08G69/32 , C08G73/18
摘要： The invention concerns polymer comprising residues of 2-(4-amino phenyl)-5 (6) amino benzimidazole (DAPBI), paraphenylene diamine (PPD), and terephthaloyl dichloride, made by a process comprising the steps of: (a) forming a slurry of b mole percent DAPBI and y mole percent PPD in a solvent system comprising organic solvent and c weight percent of an inorganic salt, wherein the inorganic salt is present in an amount of at least 5 weight percent of the organic solvent, DAPBI and PPD being present in an amount sufficient for providing a polymer solution having a weight percent solids of 12 percent or greater on a polymer basis; and (b) contacting the slurry of step a) with a stoichiometric amount of terephthaloyl dichloride to form a product comprising the polymer; wherein the sum of y+b is 100 and the product of b×c is 225 or greater.
摘要翻译：本发明涉及包含2-（4-氨基苯基）-5（6）氨基苯并咪唑（DAPBI），对苯二胺（PPD）和对苯二酰氯的残基的聚合物，该方法包括以下步骤：（a）在含有机溶剂和c％重量百分比的无机盐的溶剂体系中，B摩尔％DAPBI和y摩尔％PPD的浆料，其中无机盐以有机溶剂DAPBI和PPD的至少5重量％的量存在以足够的量存在，以提供基于聚合物的重量百分比固体含量为12％或更高的聚合物溶液; 和（b）使步骤a）的浆料与化学计量的对苯二酰氯接触以形成包含聚合物的产物; 其中y + b的和为100，b×c的乘积为225以上。

3. 发明申请

US20130197147A1 PROCESS FOR FORMING AN ARAMID COPOLYMER 有权
标题翻译：形成芳香族共聚物的方法
公开(公告)号：US20130197147A1
公开(公告)日：2013-08-01
申请号：US13559659
申请日：2012-07-27
申请人： FREDERICK K. MALLON
发明人： FREDERICK K. MALLON
IPC分类号： C08G69/28
CPC分类号： C08G69/00 , C08G69/28 , C08G69/32 , C08G73/18
摘要： The invention concerns processes for forming polymer crumb comprising residues of 2- (4-amino phenyl)-5 (6) amino phenyl benzimidazole (DAPBI), paraphenylene diamine (PPD), and terephthaloyl dichloride, comprising the steps of: (a) forming a slurry of b mole percent DAPBI and y mole percent PPD in a solvent system comprising organic solvent and c weight percent of an inorganic salt, wherein the inorganic salt is present in an amount of at least 5 weight percent of the organic solvent, DAPBI and PPD being present in an amount sufficient for providing a polymer solution having a weight percent solids of 12 percent or greater on a polymer basis; and (b) contacting the slurry of step a) with a stoichiometric amount of terephthaloyl dichloride to form a product comprising the polymer; wherein the sum of y+b is 100 and the product of b×c is 225 or greater.
摘要翻译：本发明涉及形成包含2-（4-氨基苯基）-5（6）氨基苯基苯并咪唑（DAPBI），对苯二胺（PPD）和对苯二酰氯的残留物的聚合物碎屑的方法，包括以下步骤：（a）在包含有机溶剂和c％重量百分比的无机盐的溶剂体系中，b摩尔％DAPBI和y摩尔％PPD的浆料，其中无机盐的存在量为有机溶剂DAPBI的至少5重量％ PPD存在的量足以提供聚合物基础上具有12％或更高的重量百分比固体的聚合物溶液; 和（b）使步骤a）的浆料与化学计量的对苯二酰氯接触以形成包含聚合物的产物; 其中y + b的和为100，b×c的乘积为225以上。

4. 发明申请

US20130018138A1 NEUTRALIZED COPOLYMER CRUMB AND PROCESSES FOR MAKING SAME 审中-公开
标题翻译：中和共聚物和其制备方法
公开(公告)号：US20130018138A1
公开(公告)日：2013-01-17
申请号：US13349642
申请日：2012-01-13
申请人： KIU-SEUNG LEE , FREDERICK K. MALLON , CHRISTOPHER WILLIAM NEWTON
发明人： KIU-SEUNG LEE , FREDERICK K. MALLON , CHRISTOPHER WILLIAM NEWTON
IPC分类号： C08G73/10 , C08K3/30
CPC分类号： C08G69/32 , C08L77/10 , D01F6/605
摘要： The invention concerns copolymer crumb derived from the copolymerization of para-phenylenediamine, 5(6)-amino-2-(p-aminophenyl)benzimidazole, and terephthaloyl dichloride having an inherent viscosity of at least 3 dl/g having less than 0.4 mol/Kg of titrate-able acid. In addition, the invention concerns filaments and yarn formed from such polymer crumb and processes for forming the filaments and yarn.
摘要翻译：本发明涉及衍生自对苯二胺，5（6） - 氨基-2-（对氨基苯基）苯并咪唑和对苯二酰氯的对苯二甲酰氯的共聚物碎屑，其特性粘度为至少3dl / g，具有小于0.4mol / Kg的可滴定酸。此外，本发明涉及由这种聚合物碎屑形成的长丝和纱线以及用于形成长丝和纱线的方法。

5. 发明授权

US07009028B2 Continuous process for the production of polyamides 有权
标题翻译：生产聚酰胺的连续工艺
公开(公告)号：US07009028B2
公开(公告)日：2006-03-07
申请号：US10439463
申请日：2003-05-16
申请人： Arthur William Etchells, III , Frederick K. Mallon
发明人： Arthur William Etchells, III , Frederick K. Mallon
IPC分类号： C08G69/26 , C08G69/08 , C08G73/10
CPC分类号： C08G69/28 , C08G69/04
摘要： In a two-step precondensate process for preparing polyamides diamines are reacted with dicarboxylic acid dihalides in a polar, non-basic, inert organic liquid medium under conditions such that a condensation product having a low degree of polymerization is formed. The resulting condensation then is contacted with an aqueous solution of a water-soluble acid acceptor by continuously feeding the components into a reactor system having a total residence time from about 2 seconds to about 2 minutes, and having a Peclet number greater than about 3.5 to form a polyamide product having a high degree of polymerization.
摘要翻译：在两步预缩合方法中，制备聚酰胺二胺与二羧酸二卤化物在极性非碱性惰性有机液体介质中反应，使得形成低聚合度的缩合产物。然后通过将组分连续地供入到具有约2秒至约2分钟的总停留时间的反应器系统中，然后使所得缩合物与水溶性酸受体的水溶液接触，并且具有大于约3.5至约3.5的佩佩克数形成具有高聚合度的聚酰胺产品。

6. 发明授权

US06541598B2 Composition comprising titanium and process therewith 失效
标题翻译：含钛的组合物及其处理
公开(公告)号：US06541598B2
公开(公告)日：2003-04-01
申请号：US10196065
申请日：2002-07-16
申请人： Jiwen F. Duan , Donald E. Putzig , Frederick K. Mallon , Timothy M. Davis
发明人： Jiwen F. Duan , Donald E. Putzig , Frederick K. Mallon , Timothy M. Davis
IPC分类号： C08G6378
CPC分类号： B01J31/0258 , B01J27/1806 , B01J31/0212 , B01J31/04 , B01J31/1845 , B01J31/2208 , B01J2231/14 , B01J2231/40 , B01J2531/46 , B01J2531/48 , C08G63/06 , C08G63/82 , C08G63/85 , C08G63/87
摘要： A composition that can be used as catalyst is disclosed. The composition comprises, or is produced by combining, (A) a titanium compound; (B) either (i) a complexing agent, (ii) a combination of a complexing agent, hypophosphorous acid or a salt thereof, and optionally a solvent, a zirconium compound, or both, (iii) combinations thereof; (C) a phosphorus compound; and optionally a solvent. Also disclosed is a process that can be used for producing a polyester. The process comprises contacting, in the presence of an esterification or transesterification or polycondensation catalyst composition and a phosphorus compound, a carbonyl compound and an alcohol under a condition suitable for esterification, transesterification, or polymerization. Further disclosed is a process to make polyester with reduced insoluble particles or solids using a phosphorus compound other than the commonly used phosphoric acid.
摘要翻译：公开了可用作催化剂的组合物。组合物包含或通过组合（A）钛化合物或（B）（i）络合剂，（ii）络合剂，次磷酸或其盐和任选的溶剂，锆化合物或二者的组合，（iii）它们的组合; （C）磷化合物; 和任选的溶剂。还公开了可用于生产聚酯的方法。该方法包括在适于酯化，酯交换或聚合的条件下，在酯化或酯交换或缩聚催化剂组合物与磷化合物，羰基化合物和醇的存在下接触。进一步公开的是使用除普通磷酸以外的磷化合物制备具有降低的不溶性颗粒或固体的聚酯的方法。

7. 发明申请

US20130012679A1 2,4,5-TRIAMINOPHENOLS AND RELATED COMPOUNDS 失效
公开(公告)号：US20130012679A1
公开(公告)日：2013-01-10
申请号：US13516755
申请日：2010-12-21
申请人： Rajiv Dhawan , Joachim C. Ritter , Frederick K. Mallon , Steven R. Allen , David J. Rodini , Roger K. Siamionko
发明人： Rajiv Dhawan , Joachim C. Ritter , Frederick K. Mallon , Steven R. Allen , David J. Rodini , Roger K. Siamionko
IPC分类号： C08G65/38
CPC分类号： C08G73/18 , C08G61/123 , C08G73/22
摘要： New triaminophenol compositions and related compounds are disclosed, as are processes for their preparation and for the preparation of novel salts and diacid complexes from such compounds. Polymers prepared from these compositions can be made into high strength fiber, film, and tape and are useful in applications such as protective apparel, aircraft, automotive components, personal electronics, and sports equipment.

8. 发明授权

US06489433B2 Metal-containing composition and process therewith 失效
标题翻译：含金属的组合物及其工艺
公开(公告)号：US06489433B2
公开(公告)日：2002-12-03
申请号：US09792182
申请日：2001-02-23
申请人： Jiwen F. Duan , Donald E. Putzig , Frederick K. Mallon , Timothy M. Davis
发明人： Jiwen F. Duan , Donald E. Putzig , Frederick K. Mallon , Timothy M. Davis
IPC分类号： C08G6378
CPC分类号： B01J31/0258 , B01J27/1806 , B01J31/0212 , B01J31/04 , B01J31/1845 , B01J31/2208 , B01J2231/14 , B01J2231/40 , B01J2531/46 , B01J2531/48 , C08G63/06 , C08G63/82 , C08G63/85 , C08G63/87
摘要： A composition that can be used as catalyst is disclosed. The composition comprises, or is produced by combining, (A) a titanium compound; (B) either (i) a complexing agent, (ii) a combination of a complexing agent, hypophosphorous acid or a salt thereof, and optionally a solvent, a zirconium compound, or both, (iii) combinations thereof; (C) a phosphorus compound; and optionally a solvent. Also disclosed is a process that can be used for producing a polyester. The process comprises contacting, in the presence of an esterification or transesterification or polycondensation catalyst composition and a phosphorus compound, a carbonyl compound and an alcohol under a condition suitable for esterification, transesterification, or polymerization. Further disclosed is a process to make polyester with reduced insoluble particles or solids using a phosphorus compound other than the commonly used phosphoric acid.
摘要翻译：公开了可用作催化剂的组合物。组合物包含或通过组合（A）钛化合物或（B）（i）络合剂，（ii）络合剂，次磷酸或其盐和任选的溶剂，锆化合物或二者的组合，（iii）它们的组合; （C）磷化合物; 和任选的溶剂。还公开了可用于生产聚酯的方法。该方法包括在适于酯化，酯交换或聚合的条件下，在酯化或酯交换或缩聚催化剂组合物与磷化合物，羰基化合物和醇的存在下接触。进一步公开的是使用除普通磷酸以外的磷化合物制备具有降低的不溶性颗粒或固体的聚酯的方法。

9. 发明授权

US08921511B2 Process for forming an aramid copolymer 有权
标题翻译：形成芳族聚酰胺共聚物的方法
公开(公告)号：US08921511B2
公开(公告)日：2014-12-30
申请号：US13559655
申请日：2012-07-27
申请人： Frederick K Mallon
发明人： Frederick K Mallon
IPC分类号： C08G73/00 , C08G69/28 , C08G73/18 , C08G69/32 , C08G69/00 , C08G69/26
CPC分类号： C08G69/00 , C08G69/265 , C08G69/28 , C08G69/32 , C08G73/18
摘要： The invention concerns processes for forming polymer crumb comprising residues of 2-(4-amino phenyl)-5 (6) amino benzimidazole (DAPBI), paraphenylene diamine (PPD), and terephthaloyl dichloride (TCl), comprising the steps of: i) forming a slurry of b mole percent DAPBI in a solvent system comprising organic solvent and c weight percent of an inorganic salt, wherein the inorganic salt is present in an amount of at least 5 weight present of the organic solvent; ii) contacting the slurry with a less than stoichiometric amount of terephthaloyl chloride to form an prepolymer solution; and iii) contacting the prepolymer solution with y mole percent of PPD and additional TCL to form a polymer solution; wherein the total amount of TCL added in steps ii) and iii) is a stoichiometric amount based on the total amount of DAPBI and PPD added in steps i) and iii); the DAPBI and PPD are added in an amount sufficient for providing a polymer solution having a weight percent solids of 12 percent or greater on a polymer basis; and wherein the sum of y+b is 100 and the product of b×c is 225 or greater.
摘要翻译：本发明涉及形成包含2-（4-氨基苯基）-5（6）氨基苯并咪唑（DAPBI），对苯二胺（PPD）和对苯二甲酰氯（TCl））残留物的聚合物碎屑的方法，包括以下步骤：i）在包含有机溶剂和c重量百分数的无机盐的溶剂体系中形成b摩尔％DAPBI的浆料，其中无机盐以至少5重量％存在的有机溶剂的量存在; ii）使所述浆料与少于化学计量的对苯二甲酰氯接触以形成预聚物溶液; 和iii）使预聚物溶液与γ-摩尔％的PPD和另外的TCL接触以形成聚合物溶液; 其中步骤ii）和iii）中加入的TCL的总量是基于在步骤i）和iii）中添加的DAPBI和PPD的总量的化学计量的量; 加入DAPBI和PPD的量足以提供基于聚合物的重量百分比固体含量为12％或更高的聚合物溶液; 并且其中y + b的和为100，并且b×c的乘积为225或更大。

10. 发明授权

US08664348B2 2,4,5-triaminophenols and related compounds 失效
标题翻译： 2,4,5-三氨基苯酚和相关化合物
公开(公告)号：US08664348B2
公开(公告)日：2014-03-04
申请号：US13516755
申请日：2010-12-21
申请人： Rajiv Dhawan , Joachim C Ritter , Frederick K Mallon , Steven R Allen , David J Rodini , Roger K Siemionko
发明人： Rajiv Dhawan , Joachim C Ritter , Frederick K Mallon , Steven R Allen , David J Rodini , Roger K Siemionko
IPC分类号： C08G63/02 , C08G64/00
CPC分类号： C08G73/18 , C08G61/123 , C08G73/22
摘要： New triaminophenol compositions and related compounds are disclosed, as are processes for their preparation and for the preparation of novel salts and diacid complexes from such compounds. Polymers prepared from these compositions can be made into high strength fiber, film, and tape and are useful in applications such as protective apparel, aircraft, automotive components, personal electronics, and sports equipment.
摘要翻译：公开了新的三氨基苯酚组合物和相关化合物，以及它们的制备方法以及从这些化合物制备新的盐和二酸配合物。由这些组合物制备的聚合物可以制成高强度纤维，薄膜和胶带，并且可用于诸如保护性服装，飞机，汽车部件，个人电子设备和运动器材的应用中。

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