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1. 发明申请

US20080108719A1 Phthalic Anhydride Based Polyester-Ether Polyols and Double Metal Cyanide Catalyst System for Preparing Same 审中-公开
标题翻译：邻苯二甲酸酐基聚酯 - 醚多元醇和双金属氰化物催化剂体系的制备
公开(公告)号：US20080108719A1
公开(公告)日：2008-05-08
申请号：US11876431
申请日：2007-10-22
申请人： Eric Geiger , Douglas Hillshafer
发明人： Eric Geiger , Douglas Hillshafer
IPC分类号： C08G18/00
CPC分类号： C08G18/10 , C08G18/4261 , C08G18/4866 , C08G18/4887 , C08G2101/00 , C08G2190/00 , C09J175/04 , C08G18/3206 , C08G18/302
摘要： Disclosed are polyester-ether polyols and their use in urethane prepolymers, urethane foams and non-foam urethane coatings, adhesives, sealants and/or elastomers. Methods for producing such polyester-ether polyols using double metal cyanide catalysts are disclosed, along with methods for producing urethane prepolymers. The polyester-ether polyols of the instant invention are preferably the reaction product of phthalic anhydride, diethylene glycol, and propylene oxide. These polyester-ether polyols are useful as either the primary polyol in urethane compositions or in combination with conventional auxiliary polyester- and/or polyether-based polyols. The polyester-ether polyols impart greatly improved solubility and compatibility to mixtures of either polyether and/or polyester polyols. The polyester-ether polyols of the instant invention are desirably of lower viscosity than their precursor intermediate polyester polyols and are generally soluble in either polyester- and/or polyether-based polyols. Additionally, the polyester-ether polyols generally provide improved hydrolytic stability to CASE materials in which they are utilized.
摘要翻译：公开了聚酯 - 醚多元醇及其在氨基甲酸酯预聚物，聚氨酯泡沫和非泡沫聚氨酯涂料，粘合剂，密封剂和/或弹性体中的用途。公开了使用双金属氰化物催化剂生产这种聚酯 - 醚多元醇的方法以及制备氨基甲酸酯预聚物的方法。本发明的聚酯 - 醚多元醇优选为邻苯二甲酸酐，二甘醇和环氧丙烷的反应产物。这些聚酯 - 醚多元醇可用作聚氨酯组合物中的主要多元醇或与常规辅助聚酯和/或聚醚基多元醇组合使用。聚酯 - 醚多元醇大大提高了聚醚和/或聚酯多元醇的混合物的溶解度和相容性。本发明的聚酯 - 醚多元醇理想地比其前体中间体聚酯多元醇具有更低的粘度，并且通常可溶于基于聚酯和/或聚醚的多元醇中。另外，聚醚醚多元醇通常提供改进的水解稳定性，其中使用它们的CASE材料。

2. 发明申请

US20070037953A1 Novel polyols derived from a vegetable oil using an oxidation process 失效
标题翻译：使用氧化法从植物油衍生的新型多元醇
公开(公告)号：US20070037953A1
公开(公告)日：2007-02-15
申请号：US11368159
申请日：2006-10-03
申请人： Eric Geiger , Nicole Becker , Lawrence Armbruster
发明人： Eric Geiger , Nicole Becker , Lawrence Armbruster
IPC分类号： C08G18/00
CPC分类号： C08G18/36 , C07D303/42 , C08G18/0885 , C08G18/14 , C08G18/4018 , C08G18/4081 , C08G18/4288 , C08G18/64 , C08G18/6696 , C08G2101/00 , C08G2125/00 , C11C3/006
摘要： A method for producing a vegetable oil-derived polyol having increased hydroxyl functionality by reacting a vegetable oil with an oxidizing agent in the presence of an organometallic catalyst is provided. The resulting higher functionality polyols derived from vegetable oil produced by the process are also provided. Also provided is a method for decreasing the acid value of a vegetable oil-derived polyol by reacting the vegetable oil-derived polyol with an epoxide component in the presence of a Lewis base catalyst. Urethane products produced using higher functional vegetable oil-derived polyols and/or lower acid vegetable oil-derived polyols are also provided.
摘要翻译：提供了通过在有机金属催化剂的存在下使植物油与氧化剂反应而生产具有增加的羟基官能度的植物油衍生的多元醇的方法。还提供了由该方法生产的得自植物油的更高官能度多元醇。还提供了一种通过在路易斯碱催化剂存在下使植物油衍生的多元醇与环氧化物组分反应来降低植物油衍生的多元醇的酸值的方法。还提供了使用更高功能的植物油衍生的多元醇和/或较低的酸性植物油衍生的多元醇制备的聚氨酯产品。

3. 发明申请

US20060135637A1 Phthalic anhydride based polyester-ether polyols and double metal cyanide catalyst system for preparing same 审中-公开
标题翻译：邻苯二甲酸酐基聚酯 - 醚多元醇和双金属氰化物催化剂体系制备
公开(公告)号：US20060135637A1
公开(公告)日：2006-06-22
申请号：US11286575
申请日：2005-11-22
申请人： Douglas Hillshafer , Warren Kaplan , Eric Geiger
发明人： Douglas Hillshafer , Warren Kaplan , Eric Geiger
IPC分类号： C08G18/00
CPC分类号： C08G18/4244 , C08G18/10 , C08G18/4261 , C08G18/4288 , C08G18/4866 , C08G18/4887 , C08G63/668 , C08G2101/00 , C08G2190/00 , C09J175/04 , C08G18/3206 , C08G18/302
摘要： Disclosed are polyester-ether polyols and their use in foams, in particular rigid or flexible foams. Methods for producing such polyester-ether polyols using potassium hydroxide or double metal cyanide catalysts are disclosed, along with methods for producing urethane prepolymers. The polyester-ether polyols of the instant invention are preferably the reaction product of phthalic anhydride, diethylene glycol, and propylene oxide. These polyester-ether polyols are useful as either the primary polyol in urethane compositions or in combination with conventional auxiliary polyester- and/or polyether-based polyols. The polyester-ether polyols impart greatly improved solubility and compatibility to mixtures of either polyether and/or polyester polyols. The polyester-ether polyols of the instant invention are desirably of lower viscosity than their precursor intermediate polyester polyols and are generally soluble in either polyester- and/or polyether-based polyols.
摘要翻译：公开了聚醚醚多元醇及其在泡沫中的用途，特别是刚性或柔性泡沫。公开了使用氢氧化钾或双金属氰化物催化剂生产这种聚酯 - 醚多元醇的方法，以及制备氨基甲酸酯预聚物的方法。本发明的聚酯 - 醚多元醇优选为邻苯二甲酸酐，二甘醇和环氧丙烷的反应产物。这些聚酯 - 醚多元醇可用作聚氨酯组合物中的主要多元醇或与常规辅助聚酯和/或聚醚基多元醇组合使用。聚酯 - 醚多元醇大大提高了聚醚和/或聚酯多元醇的混合物的溶解度和相容性。本发明的聚酯 - 醚多元醇理想地比其前体中间体聚酯多元醇具有更低的粘度，并且通常可溶于基于聚酯和/或聚醚的多元醇中。

4. 发明申请

US20050085658A1 Phthalic anhydride based polyester-ether polyols and double metal cyanide catalyst system for preparing same 审中-公开
公开(公告)号：US20050085658A1
公开(公告)日：2005-04-21
申请号：US11000675
申请日：2004-11-30
申请人： Eric Geiger , Douglas Hillshafer
发明人： Eric Geiger , Douglas Hillshafer
IPC分类号： C08G18/10 , C08G18/42 , C08G63/668 , C08G18/00
CPC分类号： C08G18/4244 , C08G18/10 , C08G18/4261 , C08G18/4288 , C08G18/4866 , C08G18/4887 , C08G63/668 , C08G2101/00 , C08G2190/00 , C09J175/04 , C08G18/3206 , C08G18/302
摘要： Disclosed are polyester-ether polyols and their use in urethane prepolymers, urethane foams and non-foam urethane coatings, adhesives, sealants and/or elastomers. Methods for producing such polyester-ether polyols using double metal cyanide catalysts are disclosed, along with methods for producing urethane prepolymers. The polyester-ether polyols of the instant invention are preferably the reaction product of phthalic anhydride, diethylene glycol, and propylene oxide. These polyester-ether polyols are useful as either the primary polyol in urethane compositions or in combination with conventional auxiliary polyester- and/or polyether-based polyols. The polyester-ether polyols impart greatly improved solubility and compatibility to mixtures of either polyether and/or polyester polyols. The polyester-ether polyols of the instant invention are desirably of lower viscosity than their precursor intermediate polyester polyols and are generally soluble in either polyester- and/or polyether-based polyols. Additionally, the polyester-ether polyols generally provide improved hydrolytic stability to CASE materials in which they are utilized.

5. 发明授权

US07262311B2 Process for preparing blown vegetable oil 失效
标题翻译：吹制植物油的制备方法
公开(公告)号：US07262311B2
公开(公告)日：2007-08-28
申请号：US10835367
申请日：2004-04-29
申请人： Rodney Christianson , Michael Noble , Andrew Rourke , Eric Geiger , Larry Mahlum
发明人： Rodney Christianson , Michael Noble , Andrew Rourke , Eric Geiger , Larry Mahlum
IPC分类号： C11B7/00 , C11B3/00
CPC分类号： C11B3/00 , A23D9/00 , C11B3/16
摘要： A method for partially refining a crude vegetable oil utilizing physical refining techniques is described. The crude vegetable oil is first degummed by either (1) allowing the crude oil to settle over a period of time, such as twenty days, so that the oil becomes stratified into at least two layers, wherein one layer comprises gums with low oil content and a second layer comprises oil containing only a fraction of the gums originally present and then separating the oil layer from the gum layer, or (2) heating the crude oil to a temperature of about 270-300° F. with agitation and then allowing the crude oil to settle for a period of time until the oil becomes stratified into the at least two layers. The degummed oil is then aerated and agitated while being maintained at a temperature of 170-180° F. for a time period sufficient to obtain a desired oil viscosity. The resulting partially refined oil is suitable for use in industrial applications such as the preparation of urethane foams.
摘要翻译：描述了利用物理精制技术部分精炼粗植物油的方法。首先使原油植物油脱胶，（1）允许原油在一段时间如二十天内沉降，使得油分层成至少两层，其中一层包含油含量低的树胶并且第二层包含仅含有原始存在的一部分树胶的油，然后将油层与胶层分离，或（2）在搅拌下将原油加热至约270-300°F的温度，然后允许原油沉淀一段时间，直到油分层成至少两层。然后将脱胶油充气并搅拌，同时保持在170-180°F的温度下足够长的时间以获得所需的油粘度。所得到的部分精制油适用于工业应用，例如制备聚氨酯泡沫。

6. 发明申请

US20050065356A1 Process for preparing blown vegetable oil 失效
标题翻译：吹制植物油的制备方法
公开(公告)号：US20050065356A1
公开(公告)日：2005-03-24
申请号：US10835367
申请日：2004-04-29
申请人： Rodney Christianson , Michael Noble , Andrew Rourke , Eric Geiger , Larry Mahlum
发明人： Rodney Christianson , Michael Noble , Andrew Rourke , Eric Geiger , Larry Mahlum
IPC分类号： A23D9/00 , C11B3/00 , C11B3/16 , C07C51/43
CPC分类号： C11B3/00 , A23D9/00 , C11B3/16
摘要： A method for partially refining a crude vegetable oil utilizing physical refining techniques is described. The crude vegetable oil is first degummed by either (1) allowing the crude oil to settle over a period of time, such as twenty days, so that the oil becomes stratified into at least two layers, wherein one layer comprises gums with low oil content and a second layer comprises oil containing only a fraction of the gums originally present and then separating the oil layer from the gum layer, or (2) heating the crude oil to a temperature of about 270-300° F. with agitation and then allowing the crude oil to settle for a period of time until the oil becomes stratified into the at least two layers. The degummed oil is then aerated and agitated while being maintained at a temperature of 170-180° F. for a time period sufficient to obtain a desired oil viscosity. The resulting partially refined oil is suitable for use in industrial applications such as the preparation of urethane foams.
摘要翻译：描述了利用物理精制技术部分精炼粗植物油的方法。首先使原油植物油脱胶，（1）允许原油在一段时间如二十天内沉降，使得油分层成至少两层，其中一层包含油含量低的树胶并且第二层包含仅含有原始存在的一部分树胶的油，然后将油层与胶层分离，或（2）在搅拌下将原油加热至约270-300°F的温度，然后允许原油沉淀一段时间，直到油分层成至少两层。然后将脱胶油充气并搅拌，同时保持在170-180°F的温度下足够长的时间以获得所需的油粘度。所得到的部分精制油适用于工业应用，例如制备聚氨酯泡沫。

7. 发明申请

US20070173626A9 Novel polyols derived from a vegetable oil using an oxidation process 失效
公开(公告)号：US20070173626A9
公开(公告)日：2007-07-26
申请号：US11368159
申请日：2006-03-03
申请人： Eric Geiger , Nicole Becker , Lawrence Armbruster
发明人： Eric Geiger , Nicole Becker , Lawrence Armbruster
IPC分类号： C08G18/00
CPC分类号： C08G18/36 , C07D303/42 , C08G18/0885 , C08G18/14 , C08G18/4018 , C08G18/4081 , C08G18/4288 , C08G18/64 , C08G18/6696 , C08G2101/00 , C08G2125/00 , C11C3/006
摘要： A method for producing a vegetable oil-derived polyol having increased hydroxyl functionality by reacting a vegetable oil with an oxidizing agent in the presence of an organometallic catalyst is provided. The resulting higher functionality polyols derived from vegetable oil produced by the process are also provided. Also provided is a method for decreasing the acid value of a vegetable oil-derived polyol by reacting the vegetable oil-derived polyol with an epoxide component in the presence of a Lewis base catalyst. Urethane products produced using higher functional vegetable oil-derived polyols and/or lower acid vegetable oil-derived polyols are also provided.

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