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1. 发明授权

US5575954A Process for preparing conductive polymeric particles with linear and crosslinked portions 失效
标题翻译：制备具有直链和交联部分的导电聚合物颗粒的方法
公开(公告)号：US5575954A
公开(公告)日：1996-11-19
申请号：US546627
申请日：1995-10-23
申请人： Hadi K. Mahabadi , Denise Y. Wright , Michael F. Cunningham , John A. Creatura
发明人： Hadi K. Mahabadi , Denise Y. Wright , Michael F. Cunningham , John A. Creatura
IPC分类号： C08F2/44 , C08F292/00 , C08J3/03 , C08J3/12 , G03G9/113 , G03G5/00 , C08F2/14 , C08F2/32 , G03G9/10
CPC分类号： C08F292/00 , G03G9/1135
摘要： A process for the preparation of conductive polymeric particles with linear and crosslinked portions, which comprises mixing a monomer with at least one conductive filler, solvent, at least one polymerization initiator, and a chain transfer component; effecting solution polymerization by heating until from about 80 to about 100 weight percent of the monomer has been polymerized; drying the mixture by removing the solvent to yield an intimate blend of polymer with conductive filler; dispersing the aforementioned blend of polymer and conductive filler in at least one monomer with at least one polymerization initiator, a crosslinking agent and a chain transfer agent to form an organic phase; dispersing the resulting organic phase mixture in water containing a stabilizing component to obtain a suspension of particles with an average volume diameter of from about 0.05 to about 5 microns in water; polymerizing the resulting suspension by heating; and subsequently optionally washing and drying the polymeric product.
摘要翻译：一种用于制备具有线性和交联部分的导电聚合物颗粒的方法，其包括将单体与至少一种导电填料，溶剂，至少一种聚合引发剂和链转移组分混合; 通过加热进行溶液聚合直到约80至约100重量％的单体已经聚合; 通过除去溶剂干燥混合物，得到聚合物与导电填料的紧密混合物; 将上述聚合物和导电填料的共混物在至少一种单体中与至少一种聚合引发剂，交联剂和链转移剂分散以形成有机相; 将所得有机相混合物分散在含有稳定组分的水中，以获得平均体积直径为约0.05至约5微米的水悬浮液; 通过加热使得到的悬浮液聚合; 随后任选地洗涤和干燥聚合物。

2. 发明授权

US5330874A Dry carrier coating and processes 失效
标题翻译：干载体涂层和工艺
公开(公告)号：US5330874A
公开(公告)日：1994-07-19
申请号：US953382
申请日：1992-09-30
申请人： Hadi K. Mahabadi , Denise Y. Wright , T. Hwee Ng , Angelo J. Barbetta , John A. Creatura
发明人： Hadi K. Mahabadi , Denise Y. Wright , T. Hwee Ng , Angelo J. Barbetta , John A. Creatura
IPC分类号： G03G9/113 , G03G5/00
CPC分类号： G03G9/1139 , G03G9/1133
摘要： A process for the preparation of carrier particles which comprises the dry coating of a carrier or carrier cores with conductive submicron polymeric particles containing from about 1 to about 50 weight percent of conductive fillers, and wherein said conductive polymer particles are prepared by mixing at least one monomer with a polymerization initiator, a crosslinking component and a chain transfer component; effecting bulk polymerization until from about 5 to about 50 weight percent of the monomer has been polymerized; terminating polymerization by cooling the partially polymerized monomer; adding thereto from about 1 to about 50 weight percent of a conductive filler or conductive fillers, followed by mixing thereof; dispersing the aforementioned mixture of conductive filler or fillers, and partially polymerized product in water containing a stabilizing component to obtain a suspension of particles with an average diameter of from about 0.05 to about 1 micron in water; polymerizing the resulting suspension by heating; subsequently washing and drying the product; thereafter heating the carrier core or carrier cores and the resulting conductive polymer particles to enable fusing thereof to said core or cores; and cooling the carrier particles obtained, which particles have a conductivity of from between about 10.sup. -4 to about 10.sup.-10 mho-cm.sup.-1.
摘要翻译：一种用于制备载体颗粒的方法，其包括用包含约1-约50重量％的导电填料的导电亚微米聚合物颗粒干燥涂覆载体或载体芯，并且其中所述导电聚合物颗粒通过将至少一种具有聚合引发剂的单体，交联组分和链转移组分; 直到约5至约50重量％的单体已经聚合才能进行本体聚合; 通过冷却部分聚合的单体终止聚合; 加入约1至约50重量％的导电填料或导电填料，然后混合; 将上述导电填料或填料的混合物和部分聚合的产物分散在含有稳定组分的水中以获得在水中平均直径为约0.05至约1微米的颗粒的悬浮液; 通过加热使得到的悬浮液聚合; 随后洗涤和干燥产品; 然后加热载体芯或载体芯和所得导电聚合物颗粒以使其熔合到所述芯或芯上; 并冷却所获得的载体颗粒，该颗粒的导电率介于约10 -4至10 -10 mho-cm -1之间。

3. 发明授权

US5487847A Process for the preparation of conductive polymeric particles with linear and crosslinked portions 失效
标题翻译：用于制备具有线性和交联部分的导电聚合物颗粒的方法
公开(公告)号：US5487847A
公开(公告)日：1996-01-30
申请号：US225855
申请日：1994-04-11
申请人： Hadi K. Mahabadi , Denise Y. Wright , Michael F. Cunningham , John A. Creatura
发明人： Hadi K. Mahabadi , Denise Y. Wright , Michael F. Cunningham , John A. Creatura
IPC分类号： C08F2/44 , C08F292/00 , C08J3/03 , C08J3/12 , G03G9/113 , G03G5/00 , C08F2/14 , C08F2/32 , G03G9/10
CPC分类号： C08F292/00 , G03G9/1135
摘要： A process for the preparation of conductive polymeric particles with linear and crosslinked portions, which comprises mixing a monomer with at least one conductive filler, solvent, at least one polymerization initiator, and a chain transfer component; effecting solution polymerization by heating until from about 80 to about 100 weight percent of the monomer has been polymerized; drying the mixture by removing the solvent to yield an intimate blend of polymer with conductive filler; dispersing the aforementioned blend of polymer and conductive filler in at least one monomer with at least one polymerization initiator, a crosslinking agent and a chain transfer agent to form an organic phase; dispersing the resulting organic phase mixture in water containing a stabilizing component to obtain a suspension of particles with an average volume diameter of from about 0.05 to about 5 microns in water; polymerizing the resulting suspension by heating; and subsequently optionally washing and drying the polymeric product.
摘要翻译：一种用于制备具有线性和交联部分的导电聚合物颗粒的方法，其包括将单体与至少一种导电填料，溶剂，至少一种聚合引发剂和链转移组分混合; 通过加热进行溶液聚合直到约80至约100重量％的单体已经聚合; 通过除去溶剂干燥混合物，得到聚合物与导电填料的紧密混合物; 将上述聚合物和导电填料的共混物在至少一种单体中与至少一种聚合引发剂，交联剂和链转移剂分散以形成有机相; 将所得有机相混合物分散在含有稳定组分的水中，以获得平均体积直径为约0.05至约5微米的水悬浮液; 通过加热使得到的悬浮液聚合; 随后任选地洗涤和干燥聚合物。

4. 发明授权

US5288585A Processes for the preparation of polymers 失效
标题翻译：制备聚合物的方法
公开(公告)号：US5288585A
公开(公告)日：1994-02-22
申请号：US872197
申请日：1992-04-23
申请人： Hadi K. Mahabadi , Michael Cunningham , Denise Y. Wright
发明人： Hadi K. Mahabadi , Michael Cunningham , Denise Y. Wright
IPC分类号： G03G9/087 , C08L57/00 , G03G9/08
CPC分类号： G03G9/0812 , G03G9/0806
摘要： A process for the preparation of a toner composition which comprises (1) mixing a water soluble monomer or monomers, and an oil soluble monomer or monomers with polymerization initiators, a crosslinking component and a chain transfer component; (2) effecting bulk polymerization until from about 10 to about 40 weight percent of the water soluble and oil soluble monomer or monomers have been polymerized; (3) cooling the product obtained; (4) mixing with the aforesaid partially polymerized product components comprised of charge control agents, pigments, dyes, initiators, chain transfer agents and crosslinking agents to formulate a uniform organic phase; (5) dispersing the organic phase into from between about 2 to about 5 times its volume of water containing from between about 1 to about 5 weight percent of a stabilizing component to form a suspension with an average particle size of from between about 5 to about 25 microns and a particle size distribution of from about 1.1 to about; and (6) suspension polymerizing to complete the conversion of said monomer, or said monomers to polymer.
摘要翻译：一种制备调色剂组合物的方法，其包括（1）将水溶性单体或单体与油溶性单体或聚合引发剂，交联组分和链转移组分混合; （2）进行本体聚合，直到约10至约40重量％的水溶性和油溶性单体已经聚合; （3）冷却所得产品; （4）与由电荷控制剂，颜料，染料，引发剂，链转移剂和交联剂组成的上述部分聚合的产物组分混合以配制均匀的有机相; （5）将有机相分散在含有约1至约5重量％稳定组分的体积的约2至约5倍的水中，以形成平均粒度为约5至约5重量％的悬浮液 25微米，粒度分布为约1.1至约; 和（6）悬浮聚合以完成所述单体或所述单体转化为聚合物。

5. 发明授权

US5236629A Conductive composite particles and processes for the preparation thereof 失效
标题翻译：导电复合颗粒及其制备方法
公开(公告)号：US5236629A
公开(公告)日：1993-08-17
申请号：US792570
申请日：1991-11-15
申请人： Hadi K. Mahabadi , Denise Y. Wright , T. Hwee Ng , Angelo J. Barbetta , John A. Creatura
发明人： Hadi K. Mahabadi , Denise Y. Wright , T. Hwee Ng , Angelo J. Barbetta , John A. Creatura
IPC分类号： C08F2/18 , C08F2/02 , C08F2/24 , C08F2/44 , H01B1/00
CPC分类号： C08F2/44
摘要： A process for the preparation of conductive submicron polymeric particles which comprises mixing at least one monomer with a polymerization initiator, a crosslinking component and a chain transfer component; effecting bulk polymerization until from about 10 to about 50 weight percent of the monomer has been polymerized; terminating polymerization by cooling the partially polymerized monomer; adding thereto from about 1 to about 50 weight percent of a conductive filler, or conductive fillers, followed by mixing thereof; dispersing the aforementioned mixture of conductive filler or fillers, and partially polymerized product in water containing a stabilizing component to obtain a suspension of particles with an average diameter of from about 0.05 to about 1 micron in water; polymerizing the resulting suspension by heating; and subsequently washing and drying the product.
摘要翻译：一种制备导电亚微米聚合物颗粒的方法，其包括将至少一种单体与聚合引发剂，交联组分和链转移组分混合; 直到约10至约50重量％的单体已经聚合才能进行本体聚合; 通过冷却部分聚合的单体终止聚合; 加入约1至约50重量％的导电填料或导电填料，然后混合; 将上述导电填料或填料的混合物和部分聚合的产物分散在含有稳定组分的水中，得到平均直径为约0.05至约1微米的水悬浮液; 通过加热使得到的悬浮液聚合; 随后洗涤和干燥该产品。

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