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    • 1. 发明授权
    • Methods of forming polycrystalline compacts
    • 形成多晶压块的方法
    • US09067304B2
    • 2015-06-30
    • US13618927
    • 2012-09-14
    • Danny E. ScottAnthony A. DiGiovanni
    • Danny E. ScottAnthony A. DiGiovanni
    • B24D3/00B24D3/14B24D18/00B24D99/00
    • B24D18/0009B01J3/06B01J2203/062B01J2203/0645B24D3/06B24D3/14B24D99/005E21B10/55
    • Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high-pressure, high-temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.
    • 公开了用于形成切割元件的方法,用于形成多晶压块的方法和相关的多晶压块。 对硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间,将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态(例如,压力,温度)和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料,并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性,耐磨性,韧性和性能。
    • 5. 发明申请
    • METHODS OF FORMING POLYCRSTALLINE COMPACTS AND RESULTING COMPACTS
    • 形成聚合物复合物和结果综合的方法
    • US20130067825A1
    • 2013-03-21
    • US13618927
    • 2012-09-14
    • Danny E. ScottAnthony A. DiGiovanni
    • Danny E. ScottAnthony A. DiGiovanni
    • B24D3/04B24D18/00
    • B24D18/0009B01J3/06B01J2203/062B01J2203/0645B24D3/06B24D3/14B24D99/005E21B10/55
    • Methods for forming cutting elements, methods for forming polycrystalline compacts, and related polycrystalline compacts are disclosed. Grains of a hard material are subjected to a high pressure, high temperature process to form a polycrystalline compact. Inclusion of at least one relatively quick spike in system pressure or temperature during an otherwise plateaued temperature or pressure stage accommodates formation of inter-granular bonds between the grains. The brevity of the peak stage may avoid undesirable grain growth. Embodiments of the methods may also include at least one of oscillating at least one system condition (e.g., pressure, temperature) and subjecting the grains to ultrasonic or mechanical vibrations. A resulting polycrystalline compact may include a high density of inter-granularly bonded hard material with a minimized amount of catalyst material, and may provide improved thermal stability, wear resistance, toughness, and behavior during use of a cutting element incorporating the polycrystalline compact.
    • 公开了用于形成切割元件的方法,用于形成多晶压块的方法和相关的多晶压块。 将硬质材料的颗粒进行高压高温处理以形成多晶压块。 在另外的平稳温度或压力阶段期间,将系统压力或温度中的至少一个相对较快的尖峰包含在颗粒之间形成颗粒间结合。 高峰阶段的简洁可以避免不必要的晶粒生长。 方法的实施例还可以包括振荡至少一个系统状态(例如,压力,温度)和使晶粒经受超声或机械振动中的至少一个。 所得到的多晶压块可以包括具有最小量的催化剂材料的高密度颗粒间结合的硬质材料,并且可以在使用结合多晶压块的切割元件时提供改善的热稳定性,耐磨性,韧性和性能。
    • 6. 发明授权
    • Diamond-enhanced cutting elements, earth-boring tools employing diamond-enhanced cutting elements, and methods of making diamond-enhanced cutting elements
    • 钻石增强切割元件,采用钻石增强切割元素的钻孔工具,以及制作金刚石增强切割元件的方法
    • US08292006B2
    • 2012-10-23
    • US12508440
    • 2009-07-23
    • Danny E. ScottNicholas J. Lyons
    • Danny E. ScottNicholas J. Lyons
    • E21B10/46
    • E21B10/56B22F2999/00B24D3/10C22C26/00C22C2204/00B22F2207/03
    • Cutting elements for use in earth-boring applications include a substrate, a transition layer, and a working layer. The transition layer and the working layer comprise a continuous matrix phase and a discontinuous diamond phase dispersed throughout the matrix phase. The concentration of diamond in the working layer is higher than in the transition layer. Earth-boring tools include at least one such cutting element. Methods of making cutting elements and earth-boring tools include mixing diamond crystals with matrix particles to form a mixture. The mixture is formulated in such a manner as cause the diamond crystals to comprise about 50% or more by volume of the solid matter in the mixture. The mixture is sintered to form a working layer of a cutting element that is at least substantially free of polycrystalline diamond material and that includes the diamond crystals dispersed within a continuous matrix phase formed from the matrix particles.
    • 用于镗孔应用的切割元件包括基底,过渡层和工作层。 过渡层和工作层包括分散在整个基质相中的连续的基质相和不连续的金刚石相。 工作层中金刚石的浓度高于过渡层。 钻孔工具包括至少一个这样的切割元件。 制造切割元件和钻孔工具的方法包括将金刚石晶体与基质颗粒混合以形成混合物。 混合物配制成使金刚石晶体占混合物中固体物质的约50%或更多的体积。 混合物被烧结以形成至少基本上不含多晶金刚石材料的切割元件的工作层,并且包括分散在由基质颗粒形成的连续基质相中的金刚石晶体。