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1. 发明授权

US06699429B2 Method of making silicon nitride-bonded silicon carbide honeycomb filters 失效
标题翻译：制造氮化硅结合碳化硅蜂窝过滤器的方法
公开(公告)号：US06699429B2
公开(公告)日：2004-03-02
申请号：US10210308
申请日：2002-08-01
申请人： Yanxia Lu , Dale R. Wexell , Elizabeth M. Wheeler
发明人： Yanxia Lu , Dale R. Wexell , Elizabeth M. Wheeler
IPC分类号： C04B3332
CPC分类号： C04B38/0006 , C04B35/565 , C04B35/584 , C04B38/0022
摘要： A process for forming a silicon nitride-bonded silicon carbide honeycomb monolith by a) forming a plasticizable mixture which includes (1) about 60% to 85% by weight, powdered silicon carbide with a median particle size of about 10-40 micrometers; (2) about 15% to 40% by weight, powdered silicon metal with a median particle size of about 5-20 micrometers; and, (3) organic components; b) extruding the plasticizable mixture to form a green honeycomb monolith; c) drying the green honeycomb monolith; and, d) heating the honeycomb monolith to 1450° C. with a hold of 1 hour in an atmosphere of argon; and, e) nitriding the honeycomb monolith between 1450° C. to 1600° C. for a time sufficient to obtain a silicon nitride-bonded silicon carbide body.
摘要翻译：一种通过以下步骤形成氮化硅结合的碳化硅蜂窝体整体的方法：a）形成可塑化混合物，其包括（1）约60％至85％（重量）的中等颗粒尺寸为约10-40微米的粉末状碳化硅; （2）约15〜40重量％，中等粒度为约5-20微米的粉末状硅金属; 和（3）有机成分; b）挤出可塑化混合物以形成绿色蜂窝状整料; c）干燥绿色蜂窝状整料; 和d）在氩气气氛中保持1小时将蜂窝体整体加热至1450℃; 并且e）在1450℃至1600℃之间将蜂窝状整体氮化，达到足以获得氮化硅结合的碳化硅体的时间。

2. 发明授权

US5738955A Deep-discharge battery separator 失效
标题翻译：深放电电池分离器
公开(公告)号：US5738955A
公开(公告)日：1998-04-14
申请号：US679693
申请日：1996-07-11
申请人： Thomas N. Gardner , Alvin J. Salkind , John L. Stempin , Dale R. Wexell
发明人： Thomas N. Gardner , Alvin J. Salkind , John L. Stempin , Dale R. Wexell
IPC分类号： H01M2/16 , H01M2/18 , H01M4/16 , H01M10/12
CPC分类号： H01M2/1646 , H01M2/1653 , H01M4/16
摘要： A tubular, rigid, porous, ceramic separator for a rechargeable, deep-discharge battery assembly, the separator having a porosity greater than 40%. A plurality of battery cells, each embodying such separators, are assembled with a common terminal to form the positive electrode in a motive traction battery.
摘要翻译：用于可再充电的深放电电池组件的管状，刚性，多孔的陶瓷分离器，所述隔板具有大于40％的孔隙率。每个体现这种分离器的多个电池单元组装有公共端子，以在动力牵引电池中形成正电极。

3. 发明授权

US5427986A B-N-C.sub.x hydrid coatings for inorganic fiber reinforcement materials 失效
标题翻译： B-N-Cx无机纤维增强材料的水泥涂层
公开(公告)号：US5427986A
公开(公告)日：1995-06-27
申请号：US431161
申请日：1989-10-16
申请人： Kenneth Chyung , John L. Stempin , Dale R. Wexell
发明人： Kenneth Chyung , John L. Stempin , Dale R. Wexell
IPC分类号： C04B35/80 , C03C14/00 , C04B41/45 , C22C49/00 , C23C16/36 , D06M11/00 , D06M11/73 , D06M101/00 , D06M101/40 , C04B35/52
CPC分类号： C03C14/002 , C04B41/4584 , C22C49/00 , C23C16/36 , C03C2214/02 , C03C2214/03 , C03C2214/20 , Y10T428/2916
摘要： Inorganic reinforcing fibers comprising hybrid BN--C protective coatings containing up to 12% by weight of hexagonal (graphitic) carbon dissolved in the BN matrix but being essentially free of undissolved pyrolytic and graphitic carbon secondary phases, and fiber-reinforced ceramic matrix composite products incorporating the protectively-coated fibers, are disclosed. The fibers resist oxidation and provide good bonding interface characteristics when disposed in ceramic encapsulating materials, such that the composite products exhibit excellent resistance to high temperature embrittlement.
摘要翻译：无机增强纤维包含混合的BN-C保护涂层，其中含有高达12％（重量）的溶解在BN基体中的六方晶系（石墨）碳，但基本上不含未溶解的热解和石墨碳二次相，以及纤维增强陶瓷基复合材料公开了保护性涂布的纤维。纤维在陶瓷封装材料中的抗氧化作用下，具有良好的接合界面特性，因此复合产品具有优异的耐高温脆性。

4. 发明授权

US5132254A Coated fibers for ceramic matrix composites 失效
标题翻译：陶瓷基复合材料的涂层纤维
公开(公告)号：US5132254A
公开(公告)日：1992-07-21
申请号：US628624
申请日：1990-12-17
申请人： John L. Stempin , Dale R. Wexell
发明人： John L. Stempin , Dale R. Wexell
IPC分类号： C03C14/00
CPC分类号： C03C14/002 , C03C2214/02 , C03C2214/03 , C03C2214/20
摘要： Ceramic matrix composite articles comprising a matrix phase composed of a silicate glass or glass-ceramic and a matrix reinforcement material disposed within the matrix comprising carbon (e.g., graphite) fibers are described, wherein the fibers are provided with a protective boron nitride surface coating. The mechanical properties of the composites at high temperatures are substantially improved.
摘要翻译：描述了包括由硅酸盐玻璃或玻璃陶瓷构成的基体相和布置在包含碳（例如石墨）纤维的基体内的基质增强材料）的陶瓷基复合材料制品，其中纤维具有保护性氮化硼表面涂层。复合材料在高温下的机械性能大大提高。

5. 发明授权

US4298382A Method for producing large metallic glass bodies 失效
标题翻译：生产大型金属玻璃体的方法
公开(公告)号：US4298382A
公开(公告)日：1981-11-03
申请号：US55176
申请日：1979-07-06
申请人： John L. Stempin , Dale R. Wexell
发明人： John L. Stempin , Dale R. Wexell
IPC分类号： B22F3/00 , B22F3/14 , B22F9/00 , C22C45/00 , B22F1/00
CPC分类号： B22F9/008 , B22F3/006 , B22F3/14 , C22C45/008
摘要： This invention relates to the production of large shapes of metallic glasses from finely-dimensioned ribbons powders, flakes, wires, fibers, or filaments thereof. The inventive method contemplates placing the precursor finely-dimensioned articles of metallic glass into contact with one another and then hot pressing the mass at temperatures in the close vicinity of the glass transition temperature with applied forces of at least 1000 psi. One metallic glass, Fe.sub.58 Cr.sub.14 Cu.sub.6 Si.sub.6 B.sub.6, which is readily shaped into bulk bodies via the inventive method, exhibits excellent resistance to attack by sea water.
摘要翻译：本发明涉及从精细尺寸的带状粉末，薄片，线，纤维或其细丝生产大型金属玻璃。本发明的方法考虑将前体精细尺寸的金属玻璃制品彼此接触，然后在施加至少1000psi的力的玻璃化转变温度附近的温度下热压该物料。通过本发明的方法容易地成形为块体的一种金属玻璃Fe58Cr14Cu6Si6B6显示出优异的耐海水侵蚀性。

6. 发明授权

US4098610A Biocidal glass additive for marine paints 失效
标题翻译：杀虫剂玻璃添加剂用于海洋涂料
公开(公告)号：US4098610A
公开(公告)日：1978-07-04
申请号：US799189
申请日：1977-05-23
申请人： Dale R. Wexell
发明人： Dale R. Wexell
IPC分类号： C09D5/08 , C03C3/062 , C03C3/076 , C03C3/089 , C03C3/145 , C03C4/00 , C03C8/02 , C03C12/00 , C09D5/16 , C03C3/04 , C03C3/14 , C03C3/30 , C09D5/14
CPC分类号： C03C3/076 , C03C12/00 , C03C3/062 , C03C3/089 , C03C3/145 , C03C4/0035 , C09D5/1618 , C03C2204/02 , Y10T428/24421
摘要： This invention relates to the production of borate-based or silicate-based glasses containing copper which are operable as biocidal additives in marine anti-fouling coatings. Zinc and/or tin may be substituted for a portion of the copper or, if present in combination at high loadings, may be substituted in total for the copper. When dispersed in the standard film forming binders employed in marine paints, the rate of solution of the metal ion in salt water is in excess of 10 mg/m.sup.2 /day.
摘要翻译：本发明涉及生产可在海洋防污涂料中作为杀生物添加剂操作的含铜的硼酸盐基或硅酸盐系玻璃。锌和/或锡可以代替铜的一部分，或者如果以高负载组合存在，则可以总共代替铜。当分散在用于船用涂料的标准成膜粘合剂中时，金属离子在盐水中的溶解速度超过10mg / m 2 /天。

7. 发明授权

US5164341A Fiber reinforced ceramic matrix composites exhibiting improved high-temperature strength 失效
标题翻译：纤维增强陶瓷基复合材料具有改善的高温强度
公开(公告)号：US5164341A
公开(公告)日：1992-11-17
申请号：US266829
申请日：1988-11-03
申请人： Kenneth Chyung , John L. Stempin , Dale R. Wexell
发明人： Kenneth Chyung , John L. Stempin , Dale R. Wexell
IPC分类号： C03C10/06 , C03C14/00
CPC分类号： C03C14/002 , C03C2214/02 , C03C2214/03 , C03C2214/20 , C03C2214/30 , Y10S428/902 , Y10T428/2938
摘要： Fiber-reinforced ceramic matrix composite products comprising boron-nitride-coated reinforcing silicon carbide fibers disposed in a substantially non-porous alkaline earth aluminosilicate glass-ceramic matrix are disclosed, the matrix comprising triclinic anorthite (CaO,SrO.Al.sub.2 O.sub.3.2SiO.sub.2) as the principal crystal phase and the products exhibiting unexpectedly good resistance to high-temperature degradation.
摘要翻译：公开了包含设置在基本上无孔的碱土金属硅铝酸盐玻璃 - 陶瓷基体中的氮化硼涂覆的增强碳化硅纤维的纤维增强陶瓷基复合材料，所述基质包含三斜钙矾石（CaO，SrO.Al 2 O 3·2SiO 2）作为主要结晶相，并且产品具有出乎意料的良好的耐高温劣化性能。

8. 发明授权

US5039635A Carbon-coated reinforcing fibers and composite ceramics made therefrom 失效
标题翻译：碳涂层增强纤维和由其制成的复合陶瓷
公开(公告)号：US5039635A
公开(公告)日：1991-08-13
申请号：US314451
申请日：1989-02-23
申请人： John L. Stempin , Dale R. Wexell
发明人： John L. Stempin , Dale R. Wexell
IPC分类号： C03C14/00 , C04B35/80
CPC分类号： C03C14/002 , C04B35/803 , C03C2214/02 , C03C2214/03 , C03C2214/20
摘要： Fiber-reinforced ceramic matrix composite products are made by providing inorganic fiber reinforcement materials with pyrolytic carbon coatings, combining the carbon-coated fibers with a selected ceramic matrix material to make a composite preform, and consolidating the preform with heat and pressure to form the fiber-reinforced composite. Preferably, the peak consolidation temperature of the composite is moderated, with the retained pyrolytic carbon coating acting to preserve tough fracture behavior in the composite product notwithstanding the absence of the conventional graphitic fiber interface layer therefrom.
摘要翻译：纤维增强陶瓷基复合材料是通过提供无机纤维增强材料制成热解碳涂层，将碳涂层纤维与选定的陶瓷基体材料结合，制成复合预成型件，并用热和压力固化预制件以形成纤维 - 强化复合材料。优选地，复合材料的峰值固结温度缓和，保留的热解碳涂层用于在复合产品中保持韧性断裂行为，尽管不存在常规的石墨纤维界面层。

9. 发明授权

US4746632A Inorganic crystalline fibers 失效
标题翻译：无机结晶纤维
公开(公告)号：US4746632A
公开(公告)日：1988-05-24
申请号：US904663
申请日：1986-09-08
申请人： James E. Flannery , Dale R. Wexell
发明人： James E. Flannery , Dale R. Wexell
IPC分类号： C03C10/16 , C01B25/455 , C01B33/20 , C01B33/26 , C01B35/06 , C03B32/02 , C03C13/00 , D01F9/08
CPC分类号： C01B33/20 , C01B25/455 , C01B33/26 , C01B33/28 , C01B35/06 , D01F9/08
摘要： This invention is directed to the production of inorganic crystalline fibers containing a minor amount of Mo0.sub.3 and/or W0.sub.3 and/or As.sub.2 0.sub.3 and wherein the predominant crystal phase is selected from the group of a fluormica, a fluoramphibole, canasite, potassium and/or sodium fluorrichterite, fluorapatite, and a lithium-containing, beta-spodumene-type crystal.
摘要翻译：本发明涉及含有少量MoO 3和/或W 3 O和/或As 2 O 3的无机结晶纤维的制备，其中主要结晶相选自氟堇，氟phi石，堇青石，钾和/或钠氟锆石，氟磷灰石和含锂的β-锂辉石型晶体。

10. 发明授权

US4298390A Fluorophosphate opal glasses 失效
标题翻译：氟磷酸蛋白石眼镜
公开(公告)号：US4298390A
公开(公告)日：1981-11-03
申请号：US177627
申请日：1980-08-13
申请人： James E. Flannery , John L. Stempin , Dale R. Wexell
发明人： James E. Flannery , John L. Stempin , Dale R. Wexell
IPC分类号： C03C1/04 , C03C3/083 , C03C3/085 , C03C3/112 , C03C3/115 , C03C3/118 , C03C4/00 , C03C4/02 , C03C10/16 , C03C11/00 , C03C3/04 , C03C3/08
CPC分类号： C03C3/085 , C03C10/16 , C03C3/083 , C03C3/112 , C03C3/118 , C03C4/005
摘要： This invention is directed to spontaneous opal glasses wherein Ba.sub.2 F(PO.sub.4) constitutes the predominant crystalline opal phase. The glasses exhibit softening points in excess of 710.degree. C., excellent chemical durability, and consist essentially, in weight percent on the oxide basis, of 6-10% Na.sub.2 O, 1-6% K.sub.2 O, 4-11% BaO, 9-18% Al.sub.2 O.sub.3, 50-70% SiO.sub.2, 3.5-7% P.sub.2 O.sub.5, and 1-4% F.
摘要翻译：本发明涉及自发蛋白石玻璃，其中Ba2F（PO4）构成主要的结晶蛋白石相。玻璃的软化点超过710℃，优异的化学耐久性，基本上以氧化物的重量百分比计含有6-10％的Na2O，1-6％的K2O，4-11％的BaO，9- 18％Al2O3，50-70％SiO2，3.5-7％P2O5和1-4％F.

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