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1. 发明授权

US08393195B2 Method and apparatus for detecting and quantifying a chemical compound in a fluid flow 有权
标题翻译：用于检测和定量流体流中的化合物的方法和装置
公开(公告)号：US08393195B2
公开(公告)日：2013-03-12
申请号：US12669227
申请日：2008-06-24
申请人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
发明人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
IPC分类号： G01N1/00 , G01N30/96
CPC分类号： G01N1/4005 , G01N1/2214 , G01N1/2247 , G01N2001/4011
摘要： A method and apparatus for capturing a chemical compound, typically an impurity, and for accumulating said chemical compound on a capture mass CAPT included in at least one removable adsorbent cartridge MC over a period exceeding 2 days, with a view to the external chemical analysis thereof. The apparatus ST suitable for capturing at least one chemical compound in a fluid flow for its detection and/or quantification comprise, downstream of said cartridge or cartridges, at least one device for measuring the cumulative flow which has traversed the cartridge or cartridges over a set time period. In a preferred variation of the invention, the capture mass CAPT is fragmented into a plurality of elementary masses CAPTi which allows for the spread of an irreversible adsorption front or the displacement of a chromatographic zone.
摘要翻译：为了对其进行外部化学分析，本发明提供了一种用于捕获化合物（通常为杂质）的方法和装置，并且用于在超过2天的时间内将所述化合物累积在包含在至少一个可移除吸附剂盒MC中的捕获质量CAPT 。适于捕获流体流中的至少一种化学化合物用于其检测和/或定量的装置ST包括在所述药筒或药筒的下游的至少一个装置，用于测量已经穿过药筒或药筒的累积流量时间段。在本发明的优选变型中，捕获质量CAPT被分段成多个基本质量CAPTi，其允许不可逆吸附前沿的扩散或色谱区的移位。

2. 发明授权

US08361798B2 Process and installation for testing catalysts 有权
标题翻译：测试催化剂的工艺和安装
公开(公告)号：US08361798B2
公开(公告)日：2013-01-29
申请号：US12668992
申请日：2008-06-24
申请人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
发明人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
IPC分类号： G01N31/10
CPC分类号： B01J8/0285 , B01J8/008 , B01J8/0453 , B01J35/00 , B01J2208/00061 , B01J2208/00407 , B01J2208/00814 , B01J2208/00964 , B01J2208/00973 , B01J2219/00286 , B01J2219/00495 , B01J2219/00585 , B01J2219/00747 , G01N31/10
摘要： For testing performance levels and/ or changes over time of at least one catalyst (CAT) for a fixed-bed reactor: a device (CT) for a test, comprising at least one hollow metal cartridge (MC) containing the catalyst (CAT) is connected at a point A of an industrial chemical installation containing a reaction feedstock suitable for testing the catalyst (CAT); a liquid stream containing a fraction that is less than or equal to 1% of preheated reagents circulating in the industrial chemical installation is circulated in the cartridge (MC) through the catalyst (CAT) and sampled at a reaction temperature for a period (T), and returned to the industrial chemical installation at point B downstream of the device.
摘要翻译：用于测试用于固定床反应器的至少一种催化剂（CAT）的性能水平和/或随时间的变化：用于测试的装置（CT），包括至少一个含有催化剂（CAT）的空心金属盒（MC）在含有适用于测试催化剂（CAT）的反应原料的工业化学设备的A点连接; 含有小于或等于在工业化学设备中循环的预热试剂的1％的馏分的液体流在筒（MC）中通过催化剂（CAT）循环，并在反应温度下进行一段时间（T）采样，并返回设备下游B点的工业化学品安装。

3. 发明申请

US20110045596A1 PROCESS AND INSTALLATION FOR TESTING CATALYSTS 有权
标题翻译：过程和安装测试催化剂
公开(公告)号：US20110045596A1
公开(公告)日：2011-02-24
申请号：US12668992
申请日：2008-06-24
申请人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
发明人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
IPC分类号： G01N31/10
CPC分类号： B01J8/0285 , B01J8/008 , B01J8/0453 , B01J35/00 , B01J2208/00061 , B01J2208/00407 , B01J2208/00814 , B01J2208/00964 , B01J2208/00973 , B01J2219/00286 , B01J2219/00495 , B01J2219/00585 , B01J2219/00747 , G01N31/10
摘要： The invention relates to a process for testing performance levels and/or changes over time of at least one catalyst CAT for a fixed-bed reactor comprising at least the following stages: A device for a CT test, comprising at least one hollow metal cartridge MC that contains in particular the catalyst CAT, is connected at a point A of an industrial chemical installation that uses a reaction feedstock that is suitable for testing the catalyst CAT, At point A, a liquid stream that consists of a fraction that is less than or equal to 1% of the preheated reagents circulating in the industrial chemical installation that is circulated in the cartridge MC through the catalyst CAT is sampled at a reaction temperature for a period T, At least a fraction of the effluent of the cartridge MC is sampled for chemical analysis, Optionally, the device for the CT test of the industrial chemical installation is isolated without stopping its operation, and at least a fraction of the catalyst CAT is sampled for physical and/or chemical analysis. The invention also relates to an industrial chemical installation that comprises the device for the CT bypass test.
摘要翻译：本发明涉及一种用于测试至少一种用于固定床反应器的至少一种催化剂CAT的性能水平和/或随时间变化的方法，该固定床反应器至少包括以下阶段：用于CT测试的装置，包括至少一个中空金属盒MC 其特别包含催化剂CAT在工业化学设备的A点处连接，工业化学设备使用适合于测试催化剂CAT的反应原料。在A点，由低于或等于相当于在通过催化剂CAT循环在筒MC中的工业化学设备中循环的预热试剂的1％在反应温度下进行一段时间T的采样，对盒式MC的至少一部分流出物进行取样化学分析，任选地，用于工业化学设备的CT测试的装置被隔离而不停止其操作，并且至少一部分催化剂CAT被采样用于物理和/或化学分析。本发明还涉及一种工业化学设备，其包括用于CT旁路测试的装置。

4. 发明申请

US20110016950A1 METHOD AND APPARATUS FOR DETECTING AND QUANTIFYING A CHEMICAL COMPOUND IN A FLUID FLOW 有权
标题翻译：检测和定量流体化学化合物的方法和装置
公开(公告)号：US20110016950A1
公开(公告)日：2011-01-27
申请号：US12669227
申请日：2008-06-24
申请人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
发明人： Olivier Ducreux , Fabienne Le Peltier , Cyril Collado
IPC分类号： G01N30/02 , G01N21/33 , G01N21/35 , H01J49/26 , G01R33/44 , G01N25/00 , G01J3/46
CPC分类号： G01N1/4005 , G01N1/2214 , G01N1/2247 , G01N2001/4011
摘要： The invention concerns a method for capturing a chemical compound, typically an impurity, and for accumulating said chemical compound on a capture mass CAPT included in at least one removable adsorbant cartridge MC over a long period exceeding 2 days, with a view to the external chemical analysis thereof.The invention also concerns an apparatus ST suitable for capturing at least one chemical compound in a fluid flow for its detection and/or quantification comprising, downstream of said cartridge or cartridges, at least one means for measuring the cumulative flow which has traversed said cartridge or cartridges over a set time period. In a preferred variation of the invention, the capture mass CAPT is fragmented into a plurality of elementary masses CAPTi which allowing the spread of an irreversible adsorption front or the displacement of a chromatographic zone to be determined.
摘要翻译：本发明涉及一种用于捕获化合物（通常为杂质）的方法，并且用于在长时间超过2天的时间内将包含在至少一个可移除吸附剂盒MC中的捕获质量CAPT积聚在所述化学化合物上，分析。本发明还涉及适于捕获流体流中的至少一种化学化合物用于其检测和/或定量的装置ST，其包括在所述药筒或药筒的下游，至少一种用于测量已经穿过所述药筒的累积流量的装置墨盒在一段时间内。在本发明的优选变型中，捕获质量CAPT被分段成多个基本质量CAPTi，其允许确定不可逆吸附前沿的扩散或色谱区的位移。

5. 发明申请

US20060060501A1 Process for hydroconversion of a heavy feedstock with dispersed catalyst 审中-公开
标题翻译：用分散催化剂加氢转化重质原料的方法
公开(公告)号：US20060060501A1
公开(公告)日：2006-03-23
申请号：US11229706
申请日：2005-09-20
申请人： Thierry Gauthier , Cyril Collado , Alain Ranc , Stephane Kressmann
发明人： Thierry Gauthier , Cyril Collado , Alain Ranc , Stephane Kressmann
IPC分类号： C10G47/00 , C10G45/04 , C10G47/02 , B01J8/04
CPC分类号： C10G49/02
摘要： The invention relates to a process for hydroconversion in a reaction zone (preferably in a bubbling bed and/or in slurry) of liquid heavy hydrocarbon feedstocks containing sulphur, in the presence of hydrogen and a catalytic solid phase, said solid phase being obtained from a catalytic precursor, a process in which the catalytic precursor is injected into a part of the liquid conversion products which contain dissolved hydrogen sulphide, asphaltenes and/or resins, under temperature and pressure conditions close to those at which they leave the reaction zone, and the obtained mixture is injected into the reaction zone. Preferably, the catalytic precursor is injected into the part of the conversion effluents that is recycled to the reactor inlet. The invention also relates to a device that can be used for implementing this process.
摘要翻译：本发明涉及在氢和催化固相存在下，在含有硫的液体重烃原料的反应区（优选在鼓泡床中和/或浆料中）加氢转化的方法，所述固相由催化前体，其中将催化前体注入含有溶解硫化氢，沥青质和/或树脂的部分液体转化产物中，在接近离开反应区的温度和压力条件下，将所得混合物注入反应区。优选地，将催化前体注入到再循环到反应器入口的转化流出物的一部分中。本发明还涉及可用于实现该过程的装置。

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