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1. 发明授权

US4409092A Combination process for upgrading oil products of coal, shale oil and crude oil to produce jet fuels, diesel fuels and gasoline 失效
标题翻译：组合煤，油页岩油和原油石油产品，生产喷气燃料，柴油和汽油
公开(公告)号：US4409092A
公开(公告)日：1983-10-11
申请号：US307468
申请日：1981-10-01
申请人： Charles A. Johnson , Clifford Ward , Howard F. Moore , Jr.; William P. Hettinger
发明人： Charles A. Johnson , Clifford Ward , Howard F. Moore , Jr.; William P. Hettinger
IPC分类号： C10G11/05 , C10G17/04 , C10G21/08 , C10G35/04 , C10G67/08 , C10G69/08 , F02B3/06 , C10G45/00 , B07B1/06
CPC分类号： C10G35/04 , C10G11/05 , C10G17/04 , C10G21/08 , C10G67/08 , C10G69/08 , F02B3/06
摘要： A combination process for upgrading hydrocarbon fractions obtained from raw shale oil, oil products of coal processing and select fractions of crude oils comprising sulfur, nitrogen and metal contaminants to produce jet fuel product fractions such as JP4, JP5, JP8 and other turbine-type fuel materials provided. The combination of integrated processing steps involving hydrotreating, acid extraction of basic nitrogen compounds and hydrofining thereof to produce a feed composition suitable for catalytic reforming in the absence of significant hydrocracking whereby jet fuel boiling range material is produced significantly reduces by the combination the hydrogen requirements of the process. A further significant contribution to the combination operation resides in the utilization of a catalytic cracking operation of restricted severity to particularly convert high-boiling portions of the hydrocarbon feed fractions to product boiling in the jet fuel boiling range desired before acid extraction of basic nitrogen compounds and further refining thereof as above provided by hydrotreating, reforming and hydrofining of the select product of the reforming operation. Thus, the combination operation of the invention substantially maximizes the yield of desired jet fuel products under hydrogenating conditions particularly conserving the consumption of hydrogen.
摘要翻译：用于提高从原始页岩油获得的烃馏分，煤加工的油产品和包含硫，氮和金属污染物的原油的精馏馏分以产生喷气燃料产物馏分如JP4，JP5，JP8和其它涡轮型燃料的组合方法提供材料综合处理步骤包括加氢处理，碱性氮化合物的酸萃取和其加氢精制，以在不存在明显的加氢裂化的情况下生产适用于催化重整的进料组合物，从而通过组合氢气需求的过程。对组合操作的进一步的重要贡献在于利用限制严重性的催化裂化操作特别将烃进料馏分的高沸点部分转化成在酸性萃取碱性氮化合物之前所需的喷气燃料沸腾范围内沸腾的产物，以及如上所述，通过对重整操作的选择产物的加氢处理，重整和加氢精制提供上述方法。因此，本发明的组合操作在特别节省氢气消耗的氢化条件下基本上最大化了所需喷气燃料产物的产率。

2. 发明授权

US4120865A Metal complex and method for preparing 失效
标题翻译：金属络合物及其制备方法
公开(公告)号：US4120865A
公开(公告)日：1978-10-17
申请号：US830513
申请日：1977-09-06
申请人： Clifford Ward
发明人： Clifford Ward
IPC分类号： C10G27/10 , B01J31/00 , B01J31/16 , B01J31/18 , B01J31/22 , C02F1/74 , C07B61/00 , C07C67/00 , C07C313/00 , C07C319/24 , C07C321/14 , C07C321/28 , C07D487/22 , C07F9/00 , C07F15/06 , C09B47/04 , C09B47/06 , C10G27/06 , C10G45/04 , H01B5/16
CPC分类号： C07F15/065 , B01J31/1616 , B01J31/183 , C07C319/24 , C07F15/06 , C07F9/00 , C07F9/005 , B01J2531/025 , B01J2531/56 , B01J2531/845
摘要： Disclosed is a catalyst and method for converting mercaptans and mercaptide compounds in aqueous alkaline solution to disulfides. Catalytic agent is a metal complex synthesized from 3,3',4,4'-benzophenonetetracarboxylic dianhydride and converted to either the alkali metal salt or to the acid form. The method for oxidizing the mercaptide compounds comprises contacting mercaptans and mercaptide compounds in aqueous alkaline solution with air in the presence of the catalyst and subsequently separating alkaline solution from the resultant disulfide compounds.
摘要翻译：公开了一种在碱性水溶液中将硫醇和硫醇化合物转化为二硫化物的催化剂和方法。催化剂是由3,3'，4,4'-二苯甲酮四羧酸二酐合成的金属络合物，转化为碱金属盐或酸形式。用于氧化硫醇化合物的方法包括在碱性溶液中将硫醇和硫醇化合物与空气在催化剂存在下接触，随后从所得的二硫化物中分离出碱性溶液。

3. 发明授权

US4069138A Method and catalyst for removing mercaptans and mercaptide compounds from aqueous alkaline solutions and hydrocarbon distillates 失效
标题翻译：从碱性水溶液和烃馏分中除去硫醇和硫醇化合物的方法和催化剂
公开(公告)号：US4069138A
公开(公告)日：1978-01-17
申请号：US728041
申请日：1976-09-30
申请人： Clifford Ward
发明人： Clifford Ward
IPC分类号： B01J31/16 , B01J31/18 , C10G27/10 , C10G27/06 , C07C149/00 , C10G19/02
CPC分类号： C10G27/10 , B01J31/1616 , B01J31/183 , B01J2531/025 , B01J2531/56 , B01J2531/845
摘要： Disclosed is a catalyst and method for converting mercaptans and mercaptide compounds in aqueous alkaline solution to disulfides. Catalytic agent is metal compound of 3,4-tetrapyridinotetraazaporphine (3,4-TPTAP) preferably impregnated on an inert granular support. Method comprises contacting mercaptans and mercaptide compounds in aqueous alkaline solution with air in the presence of the catalyst and subsequently separating alkaline solution from the resultant disulfide compounds.
摘要翻译：公开了一种在碱性水溶液中将硫醇和硫醇化合物转化为二硫化物的催化剂和方法。催化剂是优选浸渍在惰性颗粒载体上的3,4-四吡啶四氮杂萘（3,4-TPTAP）的金属化合物。方法包括在碱性溶液水溶液中与催化剂存在下的空气接触硫醇和硫醇盐化合物，随后从所得的二硫化物中分离出碱性溶液。

4. 发明授权

US1342843A Washbasin for motor-propelled vehicles 失效
标题翻译：洗手盆用于电动车辆
公开(公告)号：US1342843A
公开(公告)日：1920-06-08
申请号：US14349717
申请日：1917-01-20
申请人： CLIFFORD WARD I
发明人： CLIFFORD WARD I
IPC分类号： B60R15/02
CPC分类号： B60R15/02

5. 发明授权

US4927620A Process for the manufacture of carbon fibers and feedstock therefor 失效
标题翻译：用于制造碳纤维及其原料的方法
公开(公告)号：US4927620A
公开(公告)日：1990-05-22
申请号：US789590
申请日：1985-10-21
申请人： Clifford Ward , Eugene Chao , Roy E. Booth , Frank H. Turrill , Robert H. Wombles , John W. Newman , William P. Hettinger, Jr.
发明人： Clifford Ward , Eugene Chao , Roy E. Booth , Frank H. Turrill , Robert H. Wombles , John W. Newman , William P. Hettinger, Jr.
IPC分类号： C10C3/00 , D01F9/155 , D01F9/32
CPC分类号： C10C3/002 , D01F9/155 , D01F9/322
摘要： Disclosed herein is an improved pitch for making readily stabilizable, substantially nonmesophasic carbon fibers. The pitch has a softening point of about 250.degree. C. (480.degree. F.) or above and is produced from an unoxidized thermal petroleum pitch by selectively reducing or eliminating a portion of the low molecular weight materials in a very short period of time so that the tendency to produce mesophase pitch is eliminated or reduced and so that the chemical integrity of the components of the higher molecular weight fractions is preserved as much as possible. Also disclosed is a method of producing carbon fibers therefrom and rovings or mats from such fibers.
摘要翻译：本文公开了用于制备容易稳定的，基本上非中性的碳纤维的改进沥青。沥青具有约250℃（480°F）或更高的软化点，并通过在非常短的时间内选择性还原或除去一部分低分子量材料而由未氧化的热石油沥青生产，因此消除或减少产生中间相沥青的趋势，并且尽可能地保持较高分子量级分的组分的化学完整性。还公开了从这种纤维生产碳纤维的方法和粗纱或垫子。

6. 发明授权

US4382855A Process for removal of hydroxy- and/or mercapto-substituted hydrocarbons from coal liquids 失效
标题翻译：从煤液中除去羟基和/或巯基取代的烃的方法
公开(公告)号：US4382855A
公开(公告)日：1983-05-10
申请号：US315823
申请日：1981-10-28
申请人： Clifford Ward , Charles A. Johnson, III
发明人： Clifford Ward , Charles A. Johnson, III
IPC分类号： C10G21/20 , C10G29/20 , C10G17/00
CPC分类号： C10G21/20 , C10G2400/02
摘要： Removal of hydroxy-substituted and/or mercapto-substituted-hydrocarbons from coal liquids which comprises contacting the coal liquids with an aqueous composition containing an alkanolamine, thereby providing a two-phase mixture, and then separating the mixture into an aqueous extract phase and a naphtha rich raffinate phase.
摘要翻译：从煤液中除去羟基取代和/或巯基取代的烃，其包括使煤液体与含有链烷醇胺的含水组合物接触，从而提供两相混合物，然后将混合物分离成水相萃取相和富含石脑油的萃余液相。

7. 发明授权

US3980582A Method and catalyst for removing mercaptans and mercaptide compounds from aqueous alkaline solutions 失效
标题翻译：从碱性水溶液中除去硫醇和硫醇化合物的方法和催化剂
公开(公告)号：US3980582A
公开(公告)日：1976-09-14
申请号：US554492
申请日：1975-03-03
申请人： Gilbert P. Anderson, Jr. , Clifford Ward
发明人： Gilbert P. Anderson, Jr. , Clifford Ward
IPC分类号： B01J31/16 , B01J31/18 , C10G27/10
CPC分类号： C10G27/10 , B01J31/1616 , B01J31/183 , B01J2531/025 , B01J2531/56 , B01J2531/845
摘要： Disclosed is a catalyst and method for converting mercaptans and mercaptide compounds in aqueous alkaline solution to disulfides. Catalytic agent is metal compound of tetrapyridinoporphyrazine (TPPA) preferably impregnated on an inert granular support. Method comprises contacting mercaptans and mercaptide compounds in aqueous alkaline solution with air in the presence of the catalyst and subsequently separating alkaline solution from the resultant disulfide compounds.
摘要翻译：公开了一种在碱性水溶液中将硫醇和硫醇化合物转化为二硫化物的催化剂和方法。催化剂是优选浸渍在惰性颗粒载体上的四吡啶并吡啶（TPPA）的金属化合物。方法包括在碱性溶液水溶液中与催化剂存在下的空气接触硫醇和硫醇盐化合物，随后从所得的二硫化物中分离出碱性溶液。

8. 发明授权

US4671864A Process for the manufacture of carbon fibers and feedstock therefor 失效
标题翻译：用于制造碳纤维及其原料的方法
公开(公告)号：US4671864A
公开(公告)日：1987-06-09
申请号：US693438
申请日：1985-01-22
申请人： William R. Sawran , Frank H. Turrill , John W. Newman , Norman W. Hall , Clifford Ward
发明人： William R. Sawran , Frank H. Turrill , John W. Newman , Norman W. Hall , Clifford Ward
IPC分类号： C10C3/00 , D01F9/155 , D01F9/32 , D01F9/12 , C10C3/02
CPC分类号： D01F9/322 , C10C3/002 , D01F9/155
摘要： Disclosed herein is an improved pitch for making readily stabilizable, substantially nonmesophasic carbon fibers. The pitch has a softening point of about 250.degree. C.(480.degree. F.) or above and is produced from an unoxidized thermal petroleum pitch by selectively reducing or eliminating a portion of the low molecular weight materials in a very short period of time so that the tendency to produce mesophase pitch is eliminated or reduced and so that the chemical integrity of the components of the higher molecular weight fractions is preserved as much as possible. Also disclosed is a method of producing carbon fibers therefrom and rovings or mats from such fibers.
摘要翻译：本文公开了用于制备容易稳定的，基本上非中性的碳纤维的改进沥青。沥青具有约250℃（480°F）或更高的软化点，并通过在非常短的时间内选择性还原或除去一部分低分子量材料而由未氧化的热石油沥青生产，因此消除或减少产生中间相沥青的趋势，并且尽可能地保持较高分子量级分的组分的化学完整性。还公开了从这种纤维生产碳纤维的方法和粗纱或垫子。

9. 发明授权

US4243551A Catalyst for oxidizing mercaptans and mercaptide compounds and method for preparing 失效
标题翻译：用于氧化硫醇和硫醇化合物的催化剂及其制备方法
公开(公告)号：US4243551A
公开(公告)日：1981-01-06
申请号：US966163
申请日：1978-12-04
申请人： Clifford Ward
发明人： Clifford Ward
IPC分类号： B01J31/16 , B01J31/18 , B01J31/34 , C10G27/10 , B01J31/22
CPC分类号： C10G27/10 , B01J31/1616 , B01J31/183 , C07C319/24 , B01J2231/4205 , B01J2531/025 , B01J2531/56 , B01J2531/845
摘要： Disclosed is a catalyst and method for converting mercaptans and mercaptide compounds in aqueous alkaline solution to disulfides. Catalytic agent is a metal complex synthesized from 3,3',4,4'-benzophenonetetracarboxylic dianhydride and converted to either the alkali metal salt or to the acid form. The method for oxidizing the mercaptide compounds comprises contacting mercaptans and mercaptide compounds in aqueous alkaline solution with air in the presence of the catalyst and subsequently separating alkaline solution from the resultant disulfide compounds.
摘要翻译：公开了一种在碱性水溶液中将硫醇和硫醇化合物转化为二硫化物的催化剂和方法。催化剂是由3,3'，4,4'-二苯甲酮四羧酸二酐合成的金属络合物，转化为碱金属盐或酸形式。用于氧化硫醇化合物的方法包括在碱性溶液中将硫醇和硫醇化合物与空气在催化剂存在下接触，随后从所得的二硫化物中分离出碱性溶液。

10. 发明授权

US4090954A Method for oxidizing mercaptans and mercaptide compounds from aqueous alkaline solutions and hydrocarbon distillates 失效
标题翻译：从碱性水溶液和烃馏分中氧化硫醇和硫醇化合物的方法
公开(公告)号：US4090954A
公开(公告)日：1978-05-23
申请号：US753400
申请日：1976-12-22
申请人： Clifford Ward
发明人： Clifford Ward
IPC分类号： C10G27/10 , B01J31/00 , B01J31/16 , B01J31/18 , B01J31/22 , C02F1/74 , C07B61/00 , C07C67/00 , C07C313/00 , C07C319/24 , C07C321/14 , C07C321/28 , C07D487/22 , C07F9/00 , C07F15/06 , C09B47/04 , C09B47/06 , C10G27/06 , C10G45/04 , H01B5/16
CPC分类号： C07F15/065 , B01J31/1616 , B01J31/183 , C07C319/24 , C07F15/06 , C07F9/00 , C07F9/005 , B01J2531/025 , B01J2531/56 , B01J2531/845
摘要： Disclosed is a catalyst and method for converting mercaptans and mercaptide compounds in aqueous alkaline solution to disulfides. Catalytic agent is a metal complex synthesized from 3,3',4,4'-benzophenonetetracarboxylic dianhydride and converted to either the alkali metal salt or to the acid form. The method for oxidizing the mercaptide compounds comprises contacting mercaptans and mercaptide compounds in aqueous alkaline solution with air in the presence of the catalyst and subsequently separating alkaline solution from the resultant disulfide compounds.
摘要翻译：公开了一种在碱性水溶液中将硫醇和硫醇化合物转化为二硫化物的催化剂和方法。催化剂是由3,3'，4,4'-二苯甲酮四羧酸二酐合成的金属络合物，转化为碱金属盐或酸形式。用于氧化硫醇化合物的方法包括在碱性溶液中将硫醇和硫醇化合物与空气在催化剂存在下接触，随后从所得的二硫化物中分离出碱性溶液。

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