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1. 发明申请

US20050250953A1 Extraction of palm vitamin E, phytosterols and squalene from palm oil 有权
标题翻译：从棕榈油中提取棕榈维生素E，植物甾醇和角鲨烯
公开(公告)号：US20050250953A1
公开(公告)日：2005-11-10
申请号：US10642596
申请日：2003-08-19
申请人： Choo May , Harrison Nang , Ma Ngan , Yusof Basiron
发明人： Choo May , Harrison Nang , Ma Ngan , Yusof Basiron
IPC分类号： C07D311/58 , B01D9/02 , B01D11/04 , C07C7/10 , C07C11/21 , C07C401/00 , C07D311/72 , C07J9/00 , C11B3/12 , C11C3/00 , C07D311/76
CPC分类号： C11B3/12 , C07D311/72 , C07J9/00 , C11C3/003
摘要： Phytosterols, squalene and Vitamin E are recovered from phytonutrients concentrate derived from crude palm oil by the disclosed invention via esterification, transesterification, vacuum distillation, saponification, crystallization and organic solvents partitioning. Crude palm oil is subjected to esterification and transesterification for the production of crude palm oil methyl esters. Phytonutrients concentrate containing phytosterols, squalene, Vitamin E and unreacted monoglycerides is recovered from crude palm oil methyl esters by multi-stages vacuum distillation in which components with higher molecular weight are filtered during second stage vacuum distillation. The purified phytonutrients concentrate is subjected to saponification process and the unsaponifiable matter is added to a combination of solvents for crystallization of phytosterols. The filtrate enriched in squalene and Vitamin E is separated to its individual squalene-rich layer and vitamin E-rich layer via organic solvents partitioning.
摘要翻译：通过酯化，酯交换，真空蒸馏，皂化，结晶和有机溶剂分配，通过公开的本发明从植物营养素粗制油中回收植物甾醇，角鲨烯和维生素E. 粗棕榈油经过酯化和酯交换反应以生产粗棕榈油甲酯。含有植物甾醇，角鲨烯，维生素E和未反应的单甘油酯的植物营养素浓缩物通过多级真空蒸馏从粗制棕榈油甲酯中回收，其中在第二级真空蒸馏过程中过滤分子量较高的组分。将纯化的植物营养素浓缩物进行皂化过程，并将不皂化物质加入用于植物甾醇结晶的溶剂的组合中。将富含角鲨烯和维生素E的滤液通过有机溶剂分配分离成其单独的富含烯醇的富含层和富含维生素E的层。

2. 发明申请

US20050101820A1 Recovery of palm phytonutrients 有权
标题翻译：恢复棕榈植物营养素
公开(公告)号：US20050101820A1
公开(公告)日：2005-05-12
申请号：US10642597
申请日：2003-08-19
申请人： Choo May , Harrison Nang , Puah Wei , Ma Ngan , Yusof Basiron
发明人： Choo May , Harrison Nang , Puah Wei , Ma Ngan , Yusof Basiron
IPC分类号： C07C7/08 , C07C7/00 , C07C7/10 , C07C13/28 , C07C403/00 , C07C403/24
CPC分类号： C07C403/24
摘要： A process for the recovery of phytonutrients such as carotenes, phospholipids and ubiquinones from palm oil esters is disclosed. This process comprises the steps of vacuum distillation, treatment and purification of concentrate containing these phytonutrients. The alkyl esters is subjected to at least one stage vacuum distillation at temperature from 80° C. to 220° C. and pressure less than 40 mTorr. The carotenes concentrate is subjected to various physical and chemical treatments to yield higher carotenes concentration enriched with ubiquinones in indigenous diacylglycerols.
摘要翻译：公开了一种从棕榈油酯中回收植物营养素如胡萝卜素，磷脂和泛醌的方法。该方法包括真空蒸馏，处理和纯化含有这些植物营养素的浓缩物的步骤。烷基酯在80℃至220℃的温度和低于40mTorr的压力下进行至少一级真空蒸馏。对胡萝卜素浓缩物进行各种物理和化学处理以在本地二酰基甘油中产生富含泛素的较高胡萝卜素浓度。

3. 发明申请

US20050256022A1 High performance cleaning agent 审中-公开
标题翻译：高性能清洗剂
公开(公告)号：US20050256022A1
公开(公告)日：2005-11-17
申请号：US11127586
申请日：2005-05-12
申请人： Choo May , Tong Wei , Cheng Foon , Ma Ngan , Yusof Basiron
发明人： Choo May , Tong Wei , Cheng Foon , Ma Ngan , Yusof Basiron
IPC分类号： C11D1/66 , C11D3/20 , C11D7/26 , C11D7/50 , C11D1/00
CPC分类号： C09D9/005 , C11D3/2093 , C11D7/266 , C11D7/5022
摘要： A cleaning agent which provides effective solvency for a broad range of tasks and exhibits high flash point is disclosed. This cleaning agent comprises a C1-C4 ester of a C6-C20 fatty acid or a mixture of such esters having a total unsaturation of not more than 60 percent and/or a total saturation of not less than 40 percent or an iodine value of not more than 70. The fatty acid is preferably lauric acid or a mixture of fatty acids comprising lauric acid and not more than 60 percent unsaturated fatty acids and/or not less than 40 percent saturated fatty acids. Meanwhile, the C1-C4 ester is preferably methyl ester, butyl ester, isopropyl ester or a mixture thereof.
摘要翻译：公开了一种清洁剂，其为广泛的任务提供有效的偿付能力并且表现出高闪点。该清洁剂包含C 6 -C 20脂肪酸的C 1 -C 4 - 4酸酯或者C 6 -C 20脂肪酸的C 1 -C 4 - 总不饱和度不超过60％和/或总饱和度不低于40％或碘值不大于70的这些酯的混合物。脂肪酸优选为月桂酸或脂肪酸的混合物，其包含月桂酸和不超过60％的不饱和脂肪酸和/或不少于40％的饱和脂肪酸。同时，C 1 -C 4 - 酯优选为甲酯，丁酯，异丙酯或其混合物。

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