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1. 发明授权

US08808807B2 Functionalized inorganic films for ion conduction 有权
标题翻译：用于离子传导的官能化无机膜
公开(公告)号：US08808807B2
公开(公告)日：2014-08-19
申请号：US11566104
申请日：2006-12-01
申请人： Bradley F. Chmelka , George L. Athens
发明人： Bradley F. Chmelka , George L. Athens
IPC分类号： B01D69/00
CPC分类号： C08J5/22 , B01D67/0048 , B01D67/0088 , B01D67/0093 , B01D69/10 , B01D69/105 , B01D71/027 , B01D2323/38 , B01D2325/14 , C08J2383/02 , H01B1/06 , H01M8/1016 , H01M2300/0068
摘要： Novel membranes based on functionalized porous inorganic materials for ion exchange and conduction have been synthesized and characterized. The preparation procedure of these new membranes involves the synthesis of porous inorganic films, into which hydrophilic moieties are incorporated along the interior pore surfaces of the inorganic framework. Ion-conducting species are grafted into the pores via reactions with surface groups of the inorganic framework to allow for ion transport through the pore network.
摘要翻译：基于用于离子交换和传导的官能化多孔无机材料的新型膜已被合成和表征。这些新膜的制备方法涉及多孔无机膜的合成，其中亲水部分沿着无机骨架的内孔表面并入其中。离子传导物质通过与无机骨架的表面基团的反应接枝到孔中，以允许离子通过孔网络传递。

2. 发明授权

US08758653B2 Molecular optimization of multiply-functionalized mesostructured materials 有权
标题翻译：多官能化介孔结构材料的分子优化
公开(公告)号：US08758653B2
公开(公告)日：2014-06-24
申请号：US12792590
申请日：2010-06-02
申请人： Bradley F. Chmelka , George L. Athens , Robert Messinger
发明人： Bradley F. Chmelka , George L. Athens , Robert Messinger
IPC分类号： B05D5/12 , B82Y30/00 , B82Y40/00
CPC分类号： C01B37/00 , C01B39/026 , C07F7/21
摘要： A material and method for producing mesostructured materials with multiple functionalities that are independently adjustable and collectively optimizable is provided. The method uses a series of discrete synthesis steps under otherwise mutually incompatible conditions, e.g., from acidic, alkaline, and/or non-aqueous solutions, allows different functionalities to be introduced to the materials and optimized. To illustrate the method, cubic mesoporous silica films were prepared from strongly acidic solutions that were separately functionalized under highly alkaline conditions to incorporate hydrophilic aluminosilica moieties and under non-aqueous conditions to introduce perfluorosulfonic-acid surface groups.
摘要翻译：提供了一种用于生产具有独立可调整和可共同优化的多种功能的介观材料的材料和方法。该方法在另外相互不相容的条件下使用一系列离散的合成步骤，例如从酸性，碱性和/或非水溶液中，允许将不同的官能团引入材料并进行优化。为了说明该方法，从强酸性溶液制备立方介孔二氧化硅膜，其在高碱性条件下分别官能化以掺入亲水性铝硅氧烷部分，并在非水条件下引入全氟磺酸表面基团。

3. 发明申请

US20100311856A1 MOLECULAR OPTIMIZATION OF MULTIPLY-FUNCTIONALIZED MESOSTRUCTURED MATERIALS 有权
标题翻译：多功能结构材料的分子优化
公开(公告)号：US20100311856A1
公开(公告)日：2010-12-09
申请号：US12792590
申请日：2010-06-02
申请人： Bradley F. Chmelka , George L. Athens , Robert Messinger
发明人： Bradley F. Chmelka , George L. Athens , Robert Messinger
IPC分类号： C08J9/00
CPC分类号： C01B37/00 , C01B39/026 , C07F7/21
摘要： A material and method for producing mesostructured materials with multiple functionalities that are independently adjustable and collectively optimizable is provided. The method uses a series of discrete synthesis steps under otherwise mutually incompatible conditions, e.g., from acidic, alkaline, and/or non-aqueous solutions, allows different functionalities to be introduced to the materials and optimized. To illustrate the method, cubic mesoporous silica films were prepared from strongly acidic solutions that were separately functionalized under highly alkaline conditions to incorporate hydrophilic aluminosilica moieties and under non-aqueous conditions to introduce perfluorosulfonic-acid surface groups.
摘要翻译：提供了一种用于生产具有独立可调整和可共同优化的多种功能的介观材料的材料和方法。该方法在另外相互不相容的条件下使用一系列离散的合成步骤，例如从酸性，碱性和/或非水溶液中，允许将不同的官能团引入材料并进行优化。为了说明该方法，从强酸性溶液制备立方介孔二氧化硅膜，其在高碱性条件下分别官能化以掺入亲水性铝硅氧烷部分，并在非水条件下引入全氟磺酸表面基团。

4. 发明授权

US07837909B2 Mesostructured inorganic materials prepared with controllable orientational ordering 失效
标题翻译：用可控取向排列制备的中等结构无机材料
公开(公告)号：US07837909B2
公开(公告)日：2010-11-23
申请号：US11735252
申请日：2007-04-13
申请人： Bradley F. Chmelka , Jordi Nolla , Christian A. Steinbeck , George L. Athens , Douglas Wildemuth
发明人： Bradley F. Chmelka , Jordi Nolla , Christian A. Steinbeck , George L. Athens , Douglas Wildemuth
IPC分类号： C04B35/634
CPC分类号： C01B37/02 , B82Y30/00 , C08G83/001 , C09D1/00 , D01D5/00 , D01F9/00
摘要： Mesostructured inorganic-organic materials, in the form of patterned films, monoliths, and fibers, can be prepared with controllable orientational ordering over macroscopic length scales. They are synthesized by controlling solvent removal rates across material interfaces, in conjunction with the rates of surfactant self-assembly and inorganic cross-linking and surface interactions. A method for controlling the rates and directions of solvent removal from a heterogeneous material synthesis mixture that allows the nucleation and directional alignment of self-assembling mesostructures to be controlled during synthesis is disclosed. The aligned mesostructured inorganic-organic materials and mesoporous inorganic or carbon materials can be prepared in the form of patterned films, monoliths, and fibers with controllable orientational ordering. Such materials possess anisotropic structural, mechanical, optical, reaction, or transport properties that can be exploited for numerous applications in opto-electronics, separations, fuel cells, catalysis, MEMS/microfluidics, for example.
摘要翻译：以图案化膜，整料和纤维的形式的中间结构的无机 - 有机材料可以通过宏观长度尺度以可控的取向顺序制备。它们通过控制材料界面处的溶剂去除速率以及表面活性剂自组装速率和无机交联和表面相互作用而合成。公开了一种用于控制从异质材料合成混合物中去除溶剂的速率和方向的方法，其允许在合成期间控制自组装介孔结构的成核和定向排列。对准的介孔结构的无机 - 有机材料和介孔无机或碳材料可以以具有可控取向顺序的图案化膜，整料和纤维的形式制备。这些材料具有各向异性的结构，机械，光学，反应或传输特性，可用于光电子，分离，燃料电池，催化，MEMS /微流体等众多应用。

5. 发明授权

US08563124B2 Carbon materials with interconnected pores 有权
标题翻译：具有互连孔的碳材料
公开(公告)号：US08563124B2
公开(公告)日：2013-10-22
申请号：US12367471
申请日：2009-02-06
申请人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
发明人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
IPC分类号： B32B3/26 , B32B3/06
CPC分类号： C01B32/00 , Y10T428/249953 , Y10T428/249956
摘要： Methods of forming an electrically-conductive mesoporous carbon structure with interconnected pores or highly interconnected pores, and the resulting structures are described. The structure is formed by providing a mesoporous template, filling the mesopores with an organic precursor, polymerizing the organic precursor, pyrolyzing the polymerized organic precursor, and etching away the template.
摘要翻译：描述形成具有互连孔或高度互连的孔的导电介孔碳结构的方法，以及所得结构。通过提供介孔模板，用有机前体填充介孔，聚合有机前体，热解聚合的有机前体和蚀刻掉模板来形成结构。

6. 发明申请

US20090258213A1 CARBON MATERIALS WITH INTERCONNECTED PORES 有权
标题翻译：具有互连孔的碳材料
公开(公告)号：US20090258213A1
公开(公告)日：2009-10-15
申请号：US12367471
申请日：2009-02-06
申请人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
发明人： Bradley F. Chmelka , George L. Athens , An-Hui Lu
IPC分类号： B32B3/26 , B44C1/22
CPC分类号： C01B32/00 , Y10T428/249953 , Y10T428/249956
摘要： Methods of forming an electrically-conductive mesoporous carbon structure with interconnected pores or highly interconnected pores, and the resulting structures are described. The structure is formed by providing a mesoporous template, filling the mesopores with an organic precursor, polymerizing the organic precursor, pyrolyzing the polymerized organic precursor, and etching away the template.
摘要翻译：描述形成具有互连孔或高度互连的孔的导电介孔碳结构的方法，以及所得结构。通过提供介孔模板，用有机前体填充介孔，聚合有机前体，热解聚合的有机前体和蚀刻掉模板来形成结构。

7. 发明授权

US06952436B2 Inorganic/block copolymer-dye composites and dye doped mesoporous materials for optical and sensing applications 有权
标题翻译：无机/嵌段共聚物 - 染料复合材料和用于光学和感测应用的染料掺杂介孔材料
公开(公告)号：US06952436B2
公开(公告)日：2005-10-04
申请号：US10002968
申请日：2001-11-14
申请人： Gernot Wirnsberger , Brian J. Scott , Howard C. Huang , Nicholas A. Melosh , Peidong Yang , Bradley F. Chmelka , Galen D. Stucky
发明人： Gernot Wirnsberger , Brian J. Scott , Howard C. Huang , Nicholas A. Melosh , Peidong Yang , Bradley F. Chmelka , Galen D. Stucky
IPC分类号： C04B26/14 , C04B28/00 , C04B35/14 , C04B38/00 , C08G79/00 , C08G83/00 , G02B1/04 , G02B6/122 , H01S3/00
CPC分类号： C08G77/02 , C04B26/14 , C04B28/00 , C04B35/14 , C04B38/0022 , C04B2111/80 , C04B2111/805 , C08G79/00 , C08G83/001 , C08G2270/00 , G02B1/04 , G02B6/122 , C04B35/00 , C04B38/062 , C04B2103/0067 , C04B2103/54 , C04B38/04 , C04B14/30 , C04B38/00 , C04B24/32
摘要： A method for preparing transparent mesostructured inorganic/block-copolymer composites or inorganic porous solids containing optically responsive species with selective optical, optoelectronic, and sensing properties resulting therefrom. Mesoscopically organized inorganic/block copolymer composites doped with dyes or complexes are prepared for use as optical hosts, chemical/physical/biological sensors, photochromic materials, optical waveguides, tunable solid-state lasers, or optoelectronic devices. The materials can be processed into a variety of different shapes, such as films, fibers, monoliths, for novel optical and sensing applications.
摘要翻译：一种制备透明介孔结构无机/嵌段共聚物复合材料或含有光学响应物质的无机多孔固体的方法，其具有由此产生的选择性光学，光电子和感测特性。制备掺杂有染料或络合物的中等程度组织的无机/嵌段共聚物复合材料，用作光学主体，化学/物理/生物传感器，光致变色材料，光波导，可调固态激光器或光电子器件。这些材料可以加工成各种不同的形状，例如薄膜，纤维，整料，用于新颖的光学和感测应用。

8. 发明授权

US06592764B1 Block copolymer processing for mesostructured inorganic oxide materials 有权
标题翻译：介孔结构无机氧化物材料的嵌段共聚物加工
公开(公告)号：US06592764B1
公开(公告)日：2003-07-15
申请号：US09554259
申请日：2000-12-11
申请人： Galen D. Stucky , Bradley F. Chmelka , Dongyuan Zhao , Nick Melosh , Qisheng Huo , Jianglin Feng , Peidong Yang , David Pine , David Margolese , Wayne Lukens, Jr. , Glenn H. Fredrickson , Patrick Schmidt-Winkel
发明人： Galen D. Stucky , Bradley F. Chmelka , Dongyuan Zhao , Nick Melosh , Qisheng Huo , Jianglin Feng , Peidong Yang , David Pine , David Margolese , Wayne Lukens, Jr. , Glenn H. Fredrickson , Patrick Schmidt-Winkel
IPC分类号： D15
CPC分类号： B01J20/28083 , B01D15/00 , B01D15/08 , B01J20/06 , B01J20/103 , B01J20/26 , B01J20/28014 , B01J20/28023 , B01J20/28033 , B01J20/28042 , B01J20/28057 , B01J20/28069 , B01J20/28078 , B01J20/28085 , B01J20/2809 , B01J29/0308 , B01J29/041 , B01J2220/46 , C07K1/34 , C07K1/36 , C08G65/321 , C08G65/324 , C08G79/00 , C08G83/001 , C08G2650/58 , Y10T428/2962 , Y10T428/2982 , Y10T428/2993
摘要： Mesoscopically ordered, hydrothermally stable metal oxide-block copolymer composite or mesoporous materials are described herein that are formed by using amphiphilic block copolymers which act as structure directing agents for the metal oxide in a self-assembling system.
摘要翻译：本文描述了通过使用在自组装系统中用作金属氧化物的结构导向剂的两亲性嵌段共聚物形成的中等程度的水热稳定的金属氧化物 - 嵌段共聚物复合材料或介孔材料。

9. 发明授权

US07763665B2 Block polymer processing for mesostructured inorganic oxide materials 有权
标题翻译：用于介孔结构无机氧化物材料的嵌段聚合物加工
公开(公告)号：US07763665B2
公开(公告)日：2010-07-27
申请号：US11634744
申请日：2006-12-05
申请人： Galen D. Stucky , Bradley F. Chmelka , Dongyuan Zhao , Nick Melosh , Qisheng Huo , Jianglin Feng , Peidong Yang , David Pine , David Margolese , Wayne Lukens, Jr. , Glenn H. Fredrickson , Patrick Schmidt-Winkel
发明人： Galen D. Stucky , Bradley F. Chmelka , Dongyuan Zhao , Nick Melosh , Qisheng Huo , Jianglin Feng , Peidong Yang , David Pine , David Margolese , Wayne Lukens, Jr. , Glenn H. Fredrickson , Patrick Schmidt-Winkel
IPC分类号： C01B33/152 , C08K9/00
CPC分类号： B01J20/28083 , B01D15/00 , B01D15/08 , B01J20/06 , B01J20/103 , B01J20/26 , B01J20/28014 , B01J20/28023 , B01J20/28033 , B01J20/28042 , B01J20/28057 , B01J20/28069 , B01J20/28078 , B01J20/28085 , B01J20/2809 , B01J29/0308 , B01J29/041 , B01J2220/46 , C07K1/34 , C07K1/36 , C08G65/321 , C08G65/324 , C08G79/00 , C08G83/001 , C08G2650/58 , Y10T428/2962 , Y10T428/2982 , Y10T428/2993
摘要： Mesoscopically ordered, hydrothermally stable metal oxide-block copolymer composite or mesoporous materials are described herein that are formed by using amphiphilic block polymers which act as structure directing agents for the metal oxide in a self-assembling system.
摘要翻译：本文描述了通过使用在自组装系统中用作金属氧化物的结构导向剂的两亲嵌段聚合物形成的中等程度的水热稳定的金属氧化物 - 嵌段共聚物复合材料或介孔材料。

10. 发明申请

US20090162616A1 MESOSTRUCTURED MATERIALS WITH CONTROLLED ORIENTATIONAL ORDERING 审中-公开
标题翻译：具有控制定向订购的结构材料
公开(公告)号：US20090162616A1
公开(公告)日：2009-06-25
申请号：US12335225
申请日：2008-12-15
申请人： Bradley F. Chmelka , Douglas Wildemuth , George L. Athens , Jordi Nolla , Justin Jahnke
发明人： Bradley F. Chmelka , Douglas Wildemuth , George L. Athens , Jordi Nolla , Justin Jahnke
IPC分类号： B32B3/30 , B32B5/02 , B29C59/00
CPC分类号： B81C1/00031 , B81C2201/0149 , B82Y20/00 , B82Y30/00 , H01L51/0012 , H01L51/005 , H01L51/5012 , Y10T428/2457 , Y10T428/2913
摘要： Methods of controlling orientational ordering in self-assembled materials are described. These methods include controlling the nucleation rate and growth of block-copolymer-templated silica domains to yield macroscopically aligned mesostructured materials, and forming patterned mesostructured films or monoliths with control over the direction of alignment of a hexagonally-packed, block-copolymer-directed mesostructure across macroscopic lengths scales are described. Self-assembled materials with controlled orientational ordering are described, including those that contain a surfactant or block-copolymer species, and materials that include an organic (e.g., resin) or inorganic (e.g., silica or titania) network-forming component.
摘要翻译：描述了在自组装材料中控制取向排序的方法。这些方法包括控制嵌段共聚物 - 模板二氧化硅域的成核速率和生长以产生宏观取向的介观结构材料，以及形成图案化的介孔结构化膜或整料，其对六边形填充的嵌段共聚物指向的介孔结构的取向方向进行控制描述了宏观长度尺度。描述了具有受控定向排列的自组装材料，包括含有表面活性剂或嵌段共聚物物质的材料，以及包括有机（例如树脂）或无机（例如二氧化硅或二氧化钛）网络形成组分的材料。

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