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1. 发明授权

US5889088A Composite particle aqueous suspension and process for producing same 失效
标题翻译：复合颗粒水悬浮液及其制备方法
公开(公告)号：US5889088A
公开(公告)日：1999-03-30
申请号：US796180
申请日：1997-02-07
申请人： Atsushi Kisuno , Tatsuo Ansai , Shihoko Aizawa
发明人： Atsushi Kisuno , Tatsuo Ansai , Shihoko Aizawa
IPC分类号： A01N25/04 , A01N25/26 , A61K9/50 , C09B67/08 , C09D17/00 , C08K9/04
CPC分类号： A61K9/5073 , A01N25/04 , A01N25/26 , C09B67/0013 , C09D17/001 , Y10S514/937 , Y10S514/975 , Y10T428/2995 , Y10T428/2998
摘要： A stable aqueous suspension of composite particles each including a core formed from a solid or liquid particle and a coating layer formed on the core particle and including at least one high molecular weight surfactant compound having an average molecular weight of 1100 or more and at least one low molecular weight surfactant compound having an average molecular weight of 1100 or less and at least 400 below the average molecular weight of the high molecular weight surfactant compound and optionally a suspension stabilizer, is produced by subjecting a particulate solid substance or a liquid substance to a suspending treatment in an aqueous medium containing the above-mentioned high and low molecular weight surfactant compounds, and optionally the suspension stabilizer.
摘要翻译：一种复合颗粒的稳定水性悬浮液，每个复合颗粒包括由固体或液体颗粒形成的芯和形成在芯颗粒上的涂层，并且包含至少一种平均分子量为1100以上的高分子量表面活性剂化合物和至少一种低分子量表面活性剂化合物的平均分子量为1100以下且低于高分子量表面活性剂化合物的平均分子量至少为400，任选的悬浮稳定剂是通过将颗粒状固体物质或液体物质在含有上述高分子量和低分子量表面活性剂化合物的水性介质中以及任选的悬浮稳定剂的悬浮处理。

2. 发明授权

US6153657A Process for producing a solvent-less O/W type emulsion 失效
标题翻译：无溶剂O / W型乳液的制造方法
公开(公告)号：US6153657A
公开(公告)日：2000-11-28
申请号：US88383
申请日：1998-06-01
申请人： Atsushi Kisuno , Tatsuo Ansai , Shihoko Aizawa
发明人： Atsushi Kisuno , Tatsuo Ansai , Shihoko Aizawa
IPC分类号： B01J13/00 , C09K3/00 , A01N61/00 , B01F3/08 , B01F17/00
CPC分类号： B01J13/00 , Y10S514/941
摘要： An organic solvent-less O/W type emulsion having an excellent stability for storage and water-dilution is produced by a specific process in which (1) a mixture of (a) water with (b) an oily substance selected from oily effective materials and oily liquid materials, the oily substance and water being capable of forming an interface therebetween, (c) a high molecular weight surfactant and (d) a low molecular weight surfactant is stirred at a temperature of 40.degree. C. or less, to provide an O/W type emulsion; (2) the emulsion is heated to gel the emulsion; (3) the gel is heated to phase invert from O/W to W/O; (4) the W/O emulsion is cooled to a temperature below the gelling temperature; and (5) the resultant O/W emulsion is further stirred, and optionally in or after the cooling step (4), a particulate solid substance or an aqueous suspension thereof is mixed with the emulsion.
摘要翻译：通过具体方法制备具有优异的储存和水稀释稳定性的无机无溶剂O / W型乳液，其中（1）水与（b）选自油性有效物质的油性物质的混合物和油性液体材料，油性物质和水能够在其间形成界面，（c）高分子量表面活性剂和（d）低分子量表面活性剂在40℃或更低的温度下搅拌，以提供 O / W型乳液; （2）将乳液加热以凝胶化乳液; （3）将凝胶加热至从O / W转换为W / O; （4）将W / O乳液冷却至低于凝胶化温度的温度; 和（5）所得O / W乳液进一步搅拌，任选地在冷却步骤（4）中或之后，将颗粒固体物质或其水性悬浮液与乳液混合。

3. 发明申请

US20110003695A1 METHOD FOR PREPARATION OF AQUEOUS EMULSION USING INTERFACIALLY ACTIVE ORGANIC COMPOUND AS EMULSIFYING AGENT 失效
标题翻译：使用界面活性有机化合物作为乳化剂制备水性乳液的方法
公开(公告)号：US20110003695A1
公开(公告)日：2011-01-06
申请号：US12918943
申请日：2009-02-25
申请人： Masumi Asakawa , Masaki Kogiso , Toshimi Shimizu , Atsushi Kisuno
发明人： Masumi Asakawa , Masaki Kogiso , Toshimi Shimizu , Atsushi Kisuno
IPC分类号： A01N47/10 , C08K5/00 , G03G9/00 , C08K5/20 , A01P13/00
CPC分类号： A61K8/062 , A61Q19/00 , G03G9/0804 , G03G9/08755
摘要： The present invention provides a method for obtaining O/W emulsions by emulsifying various to-be-emulsified material without the use of any organic solvent, and drying and making into powder the O/W emulsion. The invention relates to a method for producing an O/W emulsion including after preliminarily dispersing a to-be-emulsified material and an interfacially active organic compound in water, heating the preliminary dispersion to a temperature equal to or higher than the melting point of the to-be-emulsified material and equal to or higher than the phase transition temperature of a self-assembled product of the interfacially active organic compound in the absence of an organic solvent, and performing emulsification under a pressure.
摘要翻译：本发明提供一种通过在不使用任何有机溶剂的情况下乳化各种待乳化材料并干燥并制成O / W乳液粉末来获得O / W乳液的方法。本发明涉及一种生产O / W乳液的方法，其包括将预乳化物和界面活性有机化合物预先分散在水中，将预分散体加热至等于或高于待乳化的材料，并且在不存在有机溶剂的情况下等于或高于界面活性有机化合物的自组装产物的相转变温度，并且在压力下进行乳化。

4. 发明授权

US08551916B2 Method for preparation of aqueous emulsion using interfacially active organic compound as emulsifying agent 失效
标题翻译：使用界面活性有机化合物作为乳化剂制备水性乳液的方法
公开(公告)号：US08551916B2
公开(公告)日：2013-10-08
申请号：US12918943
申请日：2009-02-25
申请人： Masumi Asakawa , Masaki Kogiso , Toshimi Shimizu , Atsushi Kisuno
发明人： Masumi Asakawa , Masaki Kogiso , Toshimi Shimizu , Atsushi Kisuno
IPC分类号： A01N63/00 , A01N37/00 , A01N37/18 , A01N47/10 , A61K38/00 , A61K31/27
CPC分类号： A61K8/062 , A61Q19/00 , G03G9/0804 , G03G9/08755
摘要： The present invention provides a method for obtaining O/W emulsions by emulsifying various to-be-emulsified material without the use of any organic solvent, and drying and making into powder the O/W emulsion. The invention relates to a method for producing an O/W emulsion including after preliminarily dispersing a to-be-emulsified material and an interfacially active organic compound in water, heating the preliminary dispersion to a temperature equal to or higher than the melting point of the to-be-emulsified material and equal to or higher than the phase transition temperature of a self-assembled product of the interfacially active organic compound in the absence of an organic solvent, and performing emulsification under a pressure.
摘要翻译：本发明提供一种通过在不使用任何有机溶剂的情况下乳化各种待乳化材料并干燥并制成O / W乳液粉末来获得O / W乳液的方法。本发明涉及一种生产O / W乳液的方法，其包括将预乳化物和界面活性有机化合物预先分散在水中，将预分散体加热至等于或高于待乳化的材料，并且在不存在有机溶剂的情况下等于或高于界面活性有机化合物的自组装产物的相转变温度，并且在压力下进行乳化。

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