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1. 发明授权

US08759575B2 Method for catalytically producing formic acid 有权
标题翻译：催化生产甲酸的方法
公开(公告)号：US08759575B2
公开(公告)日：2014-06-24
申请号：US13823453
申请日：2011-08-26
申请人： Andreas Bösmann , René Wölfel , Peter Wasserscheid , Nicola Taccardi , Jakob Albert
发明人： Andreas Bösmann , René Wölfel , Peter Wasserscheid , Nicola Taccardi , Jakob Albert
IPC分类号： C07C53/02 , C07C51/21
CPC分类号： C07C51/235 , C07C51/23 , Y02P20/127 , C07C53/02
摘要： The invention relates to a method for catalytically producing formic acid. A polyoxometallate ion, which is used as a catalyst, of the general formula [PMoxVyO40]5− is brought into contact with an alpha-hydroxyaldehyde, an alpha-hydroxycarboxylic acid, a carbohydrate, or a glycoside in a liquid solution at a temperature below 120° C., wherein 6
摘要翻译：本发明涉及催化生产甲酸的方法。用作催化剂的通式为[PMoxVyO40] 5的多金属氧酸盐离子在液体溶液中与α-羟基醛，α-羟基羧酸，碳水化合物或糖苷接触，温度低于 120℃，其中6

2. 发明授权

US07544807B2 Ionic liquids 有权
标题翻译：离子液体
公开(公告)号：US07544807B2
公开(公告)日：2009-06-09
申请号：US11833529
申请日：2007-08-03
申请人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
发明人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
IPC分类号： C07D401/04 , C07D213/26 , C07D233/00 , C07F9/02 , C07D229/00
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： Low melting ionic compounds of the general formula (cation) (R′SO4) in which R′ is a branched or linear, saturated or unsaturated, aliphatic or alicyclic functionalized or non-functionalized hydrocarbon chain with 3-36 carbon atoms are provided. These compounds can serve as ionic liquids, e.g. as solvents or solvent additives in chemical reactions, as extraction agents or as heat carriers. The compounds comprise a cation and anionic sulfate ester.
摘要翻译：提供通式（阳离子）（R'SO 4）的低熔点离子化合物，其中R'是具有3-36个碳原子的支链或直链，饱和或不饱和的脂族或脂环族官能化或非官能化烃链。这些化合物可以作为离子液体，例如作为化学反应中的溶剂或溶剂添加剂，作为萃取剂或作为热载体。该化合物包括阳离子和阴离子硫酸酯。

3. 发明申请

US20130245319A1 METHOD FOR CATALYTICALLY PRODUCING FORMIC ACID 有权
标题翻译：用于催化生产形式酸的方法
公开(公告)号：US20130245319A1
公开(公告)日：2013-09-19
申请号：US13823453
申请日：2011-08-26
申请人： Andreas Bösmann , René Wölfel , Peter Wasserscheid , Nicola Taccardi , Jakob Albert
发明人： Andreas Bösmann , René Wölfel , Peter Wasserscheid , Nicola Taccardi , Jakob Albert
IPC分类号： C07C51/235
CPC分类号： C07C51/235 , C07C51/23 , Y02P20/127 , C07C53/02
摘要： The invention relates to a method for catalytically producing formic acid. A polyoxometallate ion, which is used as a catalyst, of the general formula [PMoxVyO40]5− is brought into contact with an alpha-hydroxyaldehyde, an alpha-hydroxycarboxylic acid, a carbohydrate, or a glycoside in a liquid solution at a temperature below 120° C., wherein 6
摘要翻译：本发明涉及催化生产甲酸的方法。用作催化剂的通式为[PMoxVyO40] 5的多金属氧酸盐离子在液体溶液中与α-羟基醛，α-羟基羧酸，碳水化合物或糖苷接触，温度低于 120℃，其中6

4. 发明申请

US20110203972A1 Process for Removing Sulphur From Liquid Hydrocarbons 有权
标题翻译：从液态碳中除去硫的方法
公开(公告)号：US20110203972A1
公开(公告)日：2011-08-25
申请号：US12293767
申请日：2007-03-21
申请人： Gordon John Gargano , Thomas Ruether , Friederike Elisabeth Agel , Andreas Bösmann
发明人： Gordon John Gargano , Thomas Ruether , Friederike Elisabeth Agel , Andreas Bösmann
IPC分类号： C10G29/20 , C10G17/02 , C07C7/10
CPC分类号： C10G53/04 , C10G21/06 , C10G21/08 , C10G27/04 , C10G53/14
摘要： A process for the deep desulfurisation of hydrocarbons (HC), in particular Natural Gas Condensate (NGC), and HC comprising diesel, pre-extracted diesel and naphtha, is described which is capable of reducing the sulfur content of these HC from 500 to 30 ppm. The process comprises contacting the hydrocarbon material with an oxidant selected from organic peroxy acids, organic peroxides, inorganic peroxides and mixtures thereof, in at least a stochiometric amount sufficient to oxidise a sulfur compound to a sulfone compound; contacting the hydrocarbon material with an aqueous extractant to allow at least a portion of the oxidised sulfur compounds to be extracted into the aqueous extractant, and separating the hydrocarbon material from the aqueous extractant to give a hydrocarbon material of reduced sulfur content. Optionally, the process may include a second and subsequent extractions with the aqueous extractant to further reduce sulfur content. A final extraction with an IL may be conducted. The invention also provides for substitution of the aqueous extractant with an IL in one or more of the other extraction steps. The extractants and by products generated during f01 oxidation can be recovered by simple distillation techniques.
摘要翻译：描述了一种用于烃（HC），特别是天然气冷凝物（NGC）以及包含柴油，预萃取柴油和石脑油的HC的深度脱硫的方法，其能够将这些HC的硫含量从500降低至30 ppm。该方法包括使烃材料与选自有机过氧酸，有机过氧化物，无机过氧化物及其混合物的氧化剂以至少足以将硫化合物氧化成砜化合物的试剂量使之接触; 使烃材料与水性萃取剂接触以允许将至少一部分氧化的硫化合物萃取到水性萃取剂中，并将烃材料与水性萃取剂分离，得到具有降低的硫含量的烃材料。任选地，该方法可以包括第二次和随后的萃取水提取物以进一步降低硫含量。可以进行IL的最终提取。本发明还提供在一个或多个其它提取步骤中用IL替代含水萃取剂。在f01氧化期间产生的萃取剂和产物可以通过简单的蒸馏技术回收。

5. 发明授权

US08936719B2 Process for removing sulphur from liquid hydrocarbons 有权
标题翻译：从液态烃中除去硫的方法
公开(公告)号：US08936719B2
公开(公告)日：2015-01-20
申请号：US12293767
申请日：2007-03-21
申请人： John Gargano Gordon , Thomas Ruether , Friederike Elisabeth Agel , Andreas Bösmann
发明人： John Gargano Gordon , Thomas Ruether , Friederike Elisabeth Agel , Andreas Bösmann
IPC分类号： C10G53/04 , C10G53/14 , C10G21/06 , C10G21/08 , C10G27/04
CPC分类号： C10G53/04 , C10G21/06 , C10G21/08 , C10G27/04 , C10G53/14
摘要： A process for the deep desulfurisation of hydrocarbons (HC), in particular Natural Gas Condensate (NGC), and HC comprising diesel, pre-extracted diesel and naphtha, is described which is capable of reducing the sulfur content of these HC from 500 to 30 ppm. The process comprises contacting the hydrocarbon material with an oxidant selected from organic peroxy acids, organic peroxides, inorganic peroxides and mixtures thereof, in at least a stochiometric amount sufficient to oxidise a sulfur compound to a sulfone compound; contacting the hydrocarbon material with an aqueous extractant to allow at least a portion of the oxidised sulfur compounds to be extracted into the aqueous extractant, and separating the hydrocarbon material from the aqueous extractant to give a hydrocarbon material of reduced sulfur content. Optionally, the process may include a second and subsequent extractions with the aqueous extractant to further reduce sulfur content. A final extraction with an IL may be conducted. The invention also provides for substitution of the aqueous extractant with an IL in one or more of the other extraction steps. The extractants and by products generated during f01 oxidation can be recovered by simple distillation techniques.
摘要翻译：描述了一种用于烃（HC），特别是天然气冷凝物（NGC）以及包含柴油，预萃取柴油和石脑油的HC的深度脱硫的方法，其能够将这些HC的硫含量从500降低至30 ppm。该方法包括使烃材料与选自有机过氧酸，有机过氧化物，无机过氧化物及其混合物的氧化剂以至少足以将硫化合物氧化成砜化合物的试剂量使之接触; 使烃材料与水性萃取剂接触以允许将至少一部分氧化的硫化合物萃取到水性萃取剂中，并将烃材料与水性萃取剂分离，得到具有降低的硫含量的烃材料。任选地，该方法可以包括第二次和随后的萃取水提取物以进一步降低硫含量。可以进行IL的最终提取。本发明还提供在一个或多个其它提取步骤中用IL替代含水萃取剂。在f01氧化期间产生的萃取剂和产物可以通过简单的蒸馏技术回收。

6. 发明申请

US20080033178A1 Ionic Liquids 有权
标题翻译：离子液体
公开(公告)号：US20080033178A1
公开(公告)日：2008-02-07
申请号：US11833529
申请日：2007-08-03
申请人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
发明人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
IPC分类号： C07D213/02 , B01F1/00 , C07D231/02 , C07D249/04 , C23G5/00 , C07F9/02 , C07D233/00 , C07C211/62
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： Low melting ionic compounds of the general formula (cation) (R′SO4) in which R′ is a branched or linear, saturated or unsaturated, aliphatic or alicyclic functionalized or non-functionalized hydrocarbon chain with 3-36 carbon atoms are provided. These compounds can serve as ionic liquids, e.g. as solvents or solvent additives in chemical reactions, as extraction agents or as heat carriers. The compounds comprise a cation and anionic sulfate ester.
摘要翻译：通式（阳离子）（R'SO 4 S）的低熔点离子化合物，其中R'是支链或直链，饱和或不饱和的脂族或脂环族官能化或非官能化烃链，其中3 -36个碳原子。这些化合物可以作为离子液体，例如作为化学反应中的溶剂或溶剂添加剂，作为萃取剂或作为热载体。该化合物包括阳离子和阴离子硫酸酯。

7. 发明授权

US07252791B2 Ionic liquids 有权
标题翻译：离子液体
公开(公告)号：US07252791B2
公开(公告)日：2007-08-07
申请号：US10798796
申请日：2004-03-11
申请人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
发明人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
IPC分类号： B01F1/00 , C23G5/00
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： Low melting ionic compounds of the general formula (cation) (R′SO4) in which R′ is a branched or linear, saturated or unsaturated, aliphatic or alicyclic functionalized or non-functionalized hydrocarbon chain with 3-36 carbon atoms are provided. These compounds can serve as ionic liquids, e.g. as solvents or solvent additives in chemical reactions, as extraction agents or as heat carriers. The compounds comprise a cation and anionic sulfate ester.
摘要翻译：通式（阳离子）（R'SO 4 S）的低熔点离子化合物，其中R'是支链或直链，饱和或不饱和的脂族或脂环族官能化或非官能化烃链，其中3 -36个碳原子。这些化合物可以作为离子液体，例如作为化学反应中的溶剂或溶剂添加剂，作为萃取剂或作为热载体。该化合物包括阳离子和阴离子硫酸酯。

8. 发明授权

US07863458B2 Halogen-free ionic liquids 有权
标题翻译：无卤离子液体
公开(公告)号：US07863458B2
公开(公告)日：2011-01-04
申请号：US10930674
申请日：2004-08-31
申请人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
发明人： Peter Wasserscheid , Andreas Bösmann , Roy Van Hal
IPC分类号： C07D233/56 , B01F1/00 , C23G5/00
CPC分类号： C09K5/10 , C07B63/00 , C07C45/50 , C07C305/10 , C07D213/20 , C07D233/54 , Y02P20/542 , C07C47/02
摘要： An ionic liquid according to the invention is substantially halogen-free, has a low viscosity and is stable to hydrolytic degradation under test conditions. The ionic liquid is a compound of the formula (cation) (R′—O—SO3), (cation) (R′—SO3), or a mixture of the two compounds. It can be used in processes for the chemical conversion and separation of materials by employing the ionic liquid as a solvent, solvent additive, extraction agent or phase-transfer catalyst. It can also be used in a heat exchange device wherein the ionic liquid serves as a heat carrier or heat carrier additive.
摘要翻译：根据本发明的离子液体基本上是无卤素的，具有低粘度并且在测试条件下对水解降解是稳定的。离子液体是式（阳离子）（R'-O-SO3），（阳离子）（R'-SO3）或两种化合物的混合物的化合物。它可以用于通过使用离子液体作为溶剂，溶剂添加剂，萃取剂或相转移催化剂进行化学转化和分离的方法。它还可用于热交换装置，其中离子液体用作热载体或热载体添加剂。

9. 发明授权

US07553406B2 Process for removing polar impurities from hydrocarbons and mixtures of hydrocarbons 失效
标题翻译：从碳氢化合物和烃混合物中除去极性杂质的方法
公开(公告)号：US07553406B2
公开(公告)日：2009-06-30
申请号：US10836106
申请日：2004-04-30
申请人： Peter Wasserscheid , Andreas Bösmann , Andreas Jess , Leonid Datsevich , Christoph Schmitz , Andrea Wendt
发明人： Peter Wasserscheid , Andreas Bösmann , Andreas Jess , Leonid Datsevich , Christoph Schmitz , Andrea Wendt
IPC分类号： C10G29/20 , C10M169/04 , C07C7/10
CPC分类号： C10G21/08 , C07B63/00 , C07C7/10 , C07C2527/126
摘要： This invention relates to a process for removing polarizable impurities from hydrocarbons and mixtures of hydrocarbons using ionic liquids as an extraction medium. By way of extraction, the degree of contamination of the hydrocarbon or mixture of hydrocarbons is reduced to a low or very low level. The specific ionic liquids are compounds of the Formula 1, which are organic salts that are liquid or can be melted to form a liquid and that can form at least a biphasic mixture with a hydrocarbon. The process is suitable for purifying a wide range of hydrocarbons under a wide range of process conditions.
摘要翻译：本发明涉及一种使用离子液体作为萃取介质从碳氢化合物和烃类混合物中除去可极化杂质的方法。通过提取，烃或烃混合物的污染程度降低到很低或非常低的水平。特定的离子液体是式1的化合物，其是液体的或可以熔融形成液体并且可以与烃形成至少两相混合物的有机盐。该方法适用于在广泛的工艺条件下纯化各种各样的烃。

10. 发明授权

US06900313B2 Chiral ionic liquids 失效
标题翻译：手性离子液体
公开(公告)号：US06900313B2
公开(公告)日：2005-05-31
申请号：US10182388
申请日：2001-01-29
申请人： Peter Wasserscheid , Wilhelm Keim , Carsten Bolm , Andreas Bösmann
发明人： Peter Wasserscheid , Wilhelm Keim , Carsten Bolm , Andreas Bösmann
IPC分类号： C07B53/00 , C07B57/00 , C07C215/90 , C07D263/32 , C07D277/04 , C07D233/00 , C07D263/02 , C07D277/08 , C07D413/00
CPC分类号： C07B57/00 , C07B53/00 , C07B2200/07 , C07C215/90 , C07D263/32
摘要： The invention relates to chiral ionic liquids of the general formula [A]n+[Y]n−, whereby n=1 or 2, the anion [Y]n− is the anion of an organic or inorganic proton acid and the cation [A]+ an optically active organic ammonium cation with up to 50 carbon atoms, at least one chirality center and at least one functional group that can produce a coordination by forming hydrogen bridges or by providing free electron pairs. At least one chirality center is provided with a distance of up to 5 atomic bonds from the functional group. The invention also relates to a method for producing said chiral ionic liquids and to the use thereof in methods for the asymmetric synthesis, the asymmetric catalysis and for separating racemates.
摘要翻译：本发明涉及通式<？in-line-formula description =“In-line Formulas”end =“lead”？> [A] ^{的手性离子液体， SUP> [Y] ^{n ，<？in-line-formula description =“In-line Formulas”end =“tail”？>其中n = 1或2，阴离子[Y] SUP> n - 是有机或无机质子酸的阴离子，阳离子[A]具有至多50个碳原子的光学活性有机铵阳离子，至少一个手性中心和至少一个可以通过形成氢桥或通过提供自由电子对来产生配位的官能团。至少一个手性中心具有与官能团最多5个原子键的距离。本发明还涉及一种制备所述手性离子液体的方法及其在不对称合成，不对称催化和分离外消旋体的方法中的用途。}}

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