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1. 发明授权

US08815328B2 Hydroxyapatite with controllable size and morphology 有权
标题翻译：具有可控尺寸和形态的羟基磷灰石
公开(公告)号：US08815328B2
公开(公告)日：2014-08-26
申请号：US13504143
申请日：2010-10-26
申请人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
发明人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
IPC分类号： B05D3/02 , A61F2/28 , A61L27/32 , B05D1/18 , A61L27/06 , A61L27/12 , B01J20/04 , B01J20/286 , B01J20/32 , B01J27/18 , B01J37/02 , C01B25/32 , C04B28/34 , C23C22/62 , C23C22/64 , A61F2/02
CPC分类号： B05D1/18 , A61F2/02 , A61L27/06 , A61L27/12 , A61L27/32 , B01J20/048 , B01J20/286 , B01J20/3204 , B01J20/3236 , B01J27/1806 , B01J37/0225 , C01B25/32 , C04B28/34 , C23C22/62 , C23C22/64 , C04B22/06 , C04B22/062 , C04B22/064 , C04B40/0082
摘要： Methods are presented for a continuous, two-step, phase sequenced deposition of hydroxyapatite film over the surface of the substrate.
摘要翻译：提出了在基底表面上连续的两步相位沉积羟基磷灰石膜的方法。

2. 发明授权

US08757259B2 Heterogeneous proppant placement in a fracture with removable channelant fill 有权
$Heterogeneous proppant placement in a fracture with removable channelant fill$
标题翻译：不均匀的支撑剂放置在具有可移除的通道填充物的断裂中
公开(公告)号：US08757259B2
公开(公告)日：2014-06-24
申请号：US12945426
申请日：2010-11-12
申请人： Timothy Lesko , J. Ernest Brown , Dean M. Willberg , Ivan V. Kosarev , Anatoly Medvedev , Jonathan Abbott , Alexander Burukhin
发明人： Timothy Lesko , J. Ernest Brown , Dean M. Willberg , Ivan V. Kosarev , Anatoly Medvedev , Jonathan Abbott , Alexander Burukhin
IPC分类号： E21B43/267
CPC分类号： E21B43/267 , C09K8/665 , C09K8/68 , C09K8/72 , C09K8/80
摘要： A method of heterogeneous proppant placement in a subterranean fracture is disclosed. The method comprises injecting well treatment fluid including proppant (16) wherein the proppant comprises from 1 to 100 percent in weight of stiff, low-elasticity and low-deformability elongated particles (34) and proppant-spacing filler material called a channelant (18) through a wellbore (10) into the fracture (20), heterogeneously placing the proppant in the fracture in a plurality of proppant clusters or islands (22) spaced apart by the channelant (24), and removing the channelant filler material (24) to form open channels (26) around the pillars (28) for fluid flow from the formation (14) through the fracture (20) toward the wellbore (10). The proppant and channelant can be segregated within the well treatment fluid, or segregated during placement in the fracture. The channelant can be dissolvable particles, initially acting as a filler material during placement of the proppant in the fracture, and later dissolving to leave the flow channels between the proppant pillars. The well treatment fluid can include fibers to provide reinforcement and consolidation of the proppant and, additionally or alternatively, to inhibit settling of the proppant in the treatment fluid.
摘要翻译：公开了一种在地下裂缝中布置非均相支撑剂的方法。该方法包括注入包括支撑剂（16）在内的井处理流体，其中支撑剂包含1至100重量％的刚性，低弹性和低变形性细长颗粒（34）和称为通道（18）的支撑剂间隔填料，通过井眼（10）进入裂缝（20），将支撑剂不均匀地放置在由通道（24）间隔开的多个支撑剂团簇或岛（22）中的断裂中，并将通道填料（24）移除到在所述柱（28）周围形成用于从所述地层（14）穿过所述断裂（20）流向所述井筒（10）的开放通道（26）。支撑剂和输送管可以在井内处理液中分离，或在放置在裂缝中时分离。通道剂可以是可溶解的颗粒，最初在将支撑剂置于断裂中时充当填料，然后溶解以留下支撑剂柱之间的流动通道。井处理流体可以包括纤维以提供支撑剂的增强和固结，并且还可以或另外地抑制支撑剂在处理流体中的沉降。

3. 发明申请

US20110114313A1 HETEROGENEOUS PROPPANT PLACEMENT IN A FRACTURE WITH REMOVABLE CHANNELANT FILL 有权
标题翻译：具有可移动通道填充物的破裂物中的异质特殊放置
公开(公告)号：US20110114313A1
公开(公告)日：2011-05-19
申请号：US12945426
申请日：2010-11-12
申请人： Timothy Lesko , J. Ernest Brown , Dean M. Willberg , Ivan V. Kosarev , Anatoly Medvedev , Jonathan Abbott , Alexander Burukhin
发明人： Timothy Lesko , J. Ernest Brown , Dean M. Willberg , Ivan V. Kosarev , Anatoly Medvedev , Jonathan Abbott , Alexander Burukhin
IPC分类号： E21B43/267
CPC分类号： E21B43/267 , C09K8/665 , C09K8/68 , C09K8/72 , C09K8/80
摘要： A method of heterogeneous proppant placement in a subterranean fracture is disclosed. The method comprises injecting well treatment fluid including proppant (16) wherein the proppant comprises from 1 to 100 percent in weight of stiff, low-elasticity and low-deformability elongated particles (34) and proppant-spacing filler material called a channelant (18) through a wellbore (10) into the fracture (20), heterogeneously placing the proppant in the fracture in a plurality of proppant clusters or islands (22) spaced apart by the channelant (24), and removing the channelant filler material (24) to form open channels (26) around the pillars (28) for fluid flow from the formation (14) through the fracture (20) toward the wellbore (10). The proppant and channelant can be segregated within the well treatment fluid, or segregated during placement in the fracture. The channelant can be dissolvable particles, initially acting as a filler material during placement of the proppant in the fracture, and later dissolving to leave the flow channels between the proppant pillars. The well treatment fluid can include fibers to provide reinforcement and consolidation of the proppant and, additionally or alternatively, to inhibit settling of the proppant in the treatment fluid.
摘要翻译：公开了一种在地下裂缝中布置非均相支撑剂的方法。该方法包括注入包括支撑剂（16）在内的井处理流体，其中支撑剂包含1至100重量％的刚性，低弹性和低变形性细长颗粒（34）和称为通道（18）的支撑剂间隔填料，通过井眼（10）进入裂缝（20），将支撑剂不均匀地放置在由通道（24）间隔开的多个支撑剂团簇或岛（22）中的断裂中，并将通道填料（24）移除到在所述柱（28）周围形成用于从所述地层（14）穿过所述断裂（20）流向所述井筒（10）的开放通道（26）。支撑剂和输送管可以在井内处理液中分离，或在放置在裂缝中时分离。通道剂可以是可溶解的颗粒，最初在将支撑剂置于断裂中时充当填料，然后溶解以留下支撑剂柱之间的流动通道。井处理流体可以包括纤维以提供支撑剂的增强和固结，并且还可以或另外地抑制支撑剂在处理流体中的沉降。

4. 发明申请

US20080000638A1 PROPPANT MATERIAL AND FORMATION HYDRAULIC FRACTURING METHOD 有权
标题翻译：专用材料和形成液压破碎方法
公开(公告)号：US20080000638A1
公开(公告)日：2008-01-03
申请号：US11768393
申请日：2007-06-26
申请人： Alexander Burukhin , Anatoly Matveev
发明人： Alexander Burukhin , Anatoly Matveev
IPC分类号： E21B43/267
CPC分类号： C09K8/80 , C09K8/68 , Y10S507/924 , Y10T428/2982
摘要： A proppant material is provided that is in the form of generally rigid, elastic plate-like particles having a maximum to minimum dimension ratio of more than about 5. The proppant may be formed from a corrosion resistant material or having a corrosion resistant material formed thereon. The plate-like particles may be substantially non-deformable and may be formed from stainless steel or carbon steel provided with a corrosion resistant coating. The particles may have a thickness of from about 100 to about 300 μm and may be in the form of a grating. A method of hydraulic fracturing in a formation penetrated by a wellbore is also provided wherein proppant material in the form of generally rigid, elastic plate-like particles having a maximum to minimum dimension ratio of more than about 5 are introduced into the wellbore. The particles may be formed from a corrosion resistant material or having a corrosion resistant material formed thereon. Non-plate-like proppant may be introduced into the wellbore in conjunction with the plate-like proppant.
摘要翻译：提供支撑剂材料，其为通常刚性的弹性板状颗粒的形式，其最大至最小尺寸比大于约5.支撑剂可由耐腐蚀材料形成或具有形成在其上的耐腐蚀材料。板状颗粒可以是基本上不可变形的，并且可以由设置有耐腐蚀涂层的不锈钢或碳钢形成。颗粒可以具有约100至约300μm的厚度，并且可以是格栅的形式。还提供了在井眼穿透的地层中的水力压裂的方法，其中具有最大至最小尺寸比大于约5的通常刚性的弹性板状颗粒形式的支撑剂材料被引入井眼。颗粒可以由耐腐蚀材料形成或在其上形成耐腐蚀材料。非板状支撑剂可以与板状支撑剂一起引入井眼。

5. 发明授权

US07998219B2 Hydroxyapatite with controllable size and morphology 有权
标题翻译：具有可控尺寸和形态的羟基磷灰石
公开(公告)号：US07998219B2
公开(公告)日：2011-08-16
申请号：US11813368
申请日：2005-12-21
申请人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
发明人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
IPC分类号： B05D3/00 , C01B25/32 , A61F2/28 , B01J27/18
CPC分类号： C23C18/1208 , A61L27/32 , B01J20/048 , B01J20/28004 , B01J20/28014 , B01J20/28019 , B01J20/282 , B01J20/3071 , C01B25/32 , C04B41/009 , C04B41/5048 , C04B41/87 , C04B2111/00836 , Y10T428/258 , C04B41/4537 , C04B35/48
摘要： A ceramic powder of non-agglomerated non-aggregated phase-pure hydroxyapatite having a controllable morphology. Also presented is a film of phasepure crystalline hydroxyapatite grains having a controllable morphology. Methods for preparing the same are also provided.
摘要翻译：具有可控形态的非凝聚非凝聚相纯羟基磷灰石的陶瓷粉末。还提出了具有可控形态的相晶体羟基磷灰石晶粒的薄膜。还提供了制备它们的方法。

6. 发明申请

US20080206554A1 Hydroxyapatite With Controllable Size And Morphology 有权
标题翻译：具有可控尺寸和形态的羟基磷灰石
公开(公告)号：US20080206554A1
公开(公告)日：2008-08-28
申请号：US11813368
申请日：2005-12-21
申请人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
发明人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
IPC分类号： C01B25/26 , B32B5/16 , B05D1/18
CPC分类号： C23C18/1208 , A61L27/32 , B01J20/048 , B01J20/28004 , B01J20/28014 , B01J20/28019 , B01J20/282 , B01J20/3071 , C01B25/32 , C04B41/009 , C04B41/5048 , C04B41/87 , C04B2111/00836 , Y10T428/258 , C04B41/4537 , C04B35/48
摘要： A ceramic powder of non-agglomerated non-aggregated phase-pure hydroxyapatite having a controllable morphology. Also presented is a film of phasepure crystalline hydroxyapatite grains having a controllable morphology. Methods for preparing the same are also provided.
摘要翻译：具有可控形态的非凝聚非凝聚相纯羟基磷灰石的陶瓷粉末。还提出了具有可控形态的相晶体羟基磷灰石晶粒的薄膜。还提供了制备它们的方法。

7. 发明申请

US20130078476A1 HYDROXYAPATITE WITH CONTROLLABLE SIZE AND MORPHOLOGY 有权
标题翻译：具有可控尺寸和形态学的羟基磷灰石
公开(公告)号：US20130078476A1
公开(公告)日：2013-03-28
申请号：US13504143
申请日：2010-10-26
申请人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
发明人： Richard E. Riman , Alexander Burukhin , Eugene Zlotnikov , Dan Haders
IPC分类号： B05D1/18 , A61F2/02
CPC分类号： B05D1/18 , A61F2/02 , A61L27/06 , A61L27/12 , A61L27/32 , B01J20/048 , B01J20/286 , B01J20/3204 , B01J20/3236 , B01J27/1806 , B01J37/0225 , C01B25/32 , C04B28/34 , C23C22/62 , C23C22/64 , C04B22/06 , C04B22/062 , C04B22/064 , C04B40/0082
摘要： Methods are presented for a continuous, two-step, phase sequenced deposition of hydroxyapatite film over the surface of the substrate.
摘要翻译：提出了在基底表面上连续的两步相位沉积羟基磷灰石膜的方法。

8. 发明授权

US07931966B2 Proppant material and formation hydraulic fracturing method 有权
$Proppant material and formation hydraulic fracturing method$
标题翻译：支撑材料和地层水力压裂法
公开(公告)号：US07931966B2
公开(公告)日：2011-04-26
申请号：US11768393
申请日：2007-06-26
申请人： Alexander Burukhin , Anatoly Matveev
发明人： Alexander Burukhin , Anatoly Matveev
IPC分类号： C09K8/80 , E21B43/267 , B32B23/00
CPC分类号： C09K8/80 , C09K8/68 , Y10S507/924 , Y10T428/2982
摘要： A proppant material is provided that is in the form of generally rigid, elastic plate-like particles having a maximum to minimum dimension ratio of more than about 5. The proppant may be formed from a corrosion resistant material or having a corrosion resistant material formed thereon. The plate-like particles may be substantially non-deformable and may be formed from stainless steel or carbon steel provided with a corrosion resistant coating. The particles may have a thickness of from about 100 to about 300 μm and may be in the form of a grating. A method of hydraulic fracturing in a formation penetrated by a wellbore is also provided wherein proppant material in the form of generally rigid, elastic plate-like particles having a maximum to minimum dimension ratio of more than about 5 are introduced into the wellbore. The particles may be formed from a corrosion resistant material or having a corrosion resistant material formed thereon. Non-plate-like proppant may be introduced into the wellbore in conjunction with the plate-like proppant.
摘要翻译：提供支撑剂材料，其为通常刚性的弹性板状颗粒的形式，其最大至最小尺寸比大于约5.支撑剂可由耐腐蚀材料形成或具有形成在其上的耐腐蚀材料。板状颗粒可以是基本上不可变形的，并且可以由设置有耐腐蚀涂层的不锈钢或碳钢形成。颗粒可以具有约100至约300μm的厚度，并且可以是格栅的形式。还提供了在井眼穿透的地层中的水力压裂的方法，其中具有最大至最小尺寸比大于约5的通常刚性的弹性板状颗粒形式的支撑剂材料被引入井眼。颗粒可以由耐腐蚀材料形成或在其上形成耐腐蚀材料。非板状支撑剂可以与板状支撑剂一起引入井眼。

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