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1. 发明授权

US6126855A Reaction products of lyotropic liquid crystal salt complexes 失效
标题翻译：溶致液晶盐络合物的反应产物
公开(公告)号：US6126855A
公开(公告)日：2000-10-03
申请号：US131835
申请日：1998-08-10
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： G01N27/22 , H01L39/12 , C09K19/52 , C09K19/38 , H01B1/12
CPC分类号： G01N27/225 , H01L39/121 , Y10S505/785
摘要： The invention provides superior reaction products of copper, especially ultra-clean copper and polymeric chemical complexes. The polymers are unusual in that they provide polymeric systems of extensive conjugated double bond networks well suited for electron flow. The polymers are the covalent reaction products of aroylacrylates and isocyanates or thioisocyanates and are of stability and ease of manufacture.The materials provide superior electrical conductors and superconductors. Through the use of lattice modifiers and stabilizers the lattices of the polymers may be "fine tuned" easily so as to optimize important characteristics such as electron flow.The organic coatings on the copper perform best as thin films, especially as films thinner than lambda, the penetration depth of the magnetic flux into the superconductor. The long term widely accepted use of copper as an electrical conductor, with its flexibility, durability, and strength is preserved while its electrical current capacity is greatly enhanced. Whether the copper is in the form of wire, sheet, foil, or thin films on supporting substrates, the reaction product coating profoundly enhances the commercial potential of the materials.Systems for providing both non-polymeric and polymeric liquid crystal complexes of enhanced purity have been developed and contribute to the excellent performance of these materials. These systems can readily be formulated so as to enhance both their electrical conductance and their diamagnetic qualities. Thus, as maglev materials for satellites, as components of motors, as ingredients in static-dissipative compositions, or EMI-control plastics, and similar applications they are of great utility.
摘要翻译：本发明提供铜的优异反应产物，特别是超清洁铜和聚合物化合物。聚合物是不寻常的，因为它们提供了非常适合于电子流的广泛共轭双键网络的聚合体系。聚合物是芳族丙烯酸酯和异氰酸酯或硫代异氰酸酯的共价反应产物，并且具有稳定性和易于制造。这些材料提供优良的电导体和超导体。通过使用晶格调节剂和稳定剂，可以容易地将聚合物的晶格“微调”以优化诸如电子流的重要特征。铜上的有机涂层最好作为薄膜，特别是薄膜比λ薄膜，磁通量进入超导体的穿透深度。长期广泛接受使用铜作为电导体，具有其柔性，耐久性和强度，同时其电流容量大大提高。铜是否是支撑基板上的线，片，箔或薄膜的形式，反应产物涂层深深地增强了材料的商业潜力。已经开发了用于提供高纯度的非聚合物和聚合物液晶复合物的系统，并且有助于这些材料的优异性能。这些系统可以容易地配制，以便增强它们的导电性和它们的抗磁性质。因此，作为用于卫星的磁悬浮材料，作为电动机的组分，作为静电消散组合物中的成分，或EMI控制塑料以及类似应用，它们具有很大的效用。

2. 发明授权

US5354496A Lyotropic liquid crystal salt/inorganic compound complexation products 失效
标题翻译：溶致液晶盐/无机复合络合物
公开(公告)号：US5354496A
公开(公告)日：1994-10-11
申请号：US821084
申请日：1992-01-16
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： G01N21/81 , G01N27/22 , C09K19/52 , B01D9/00
CPC分类号： G01N21/81 , C09K19/062 , C09K19/32 , C09K19/322 , G01N27/225 , C09K2019/122 , Y02P20/544
摘要： The invention provides novel chemical complexation products for use as superconductors, polymer electrolytes for alkali metal batteries, electrolytes for electrochromic windows, static dissipative plastics, etc. It also provides for manufacturing such complexation products. The complexation products may comprise (a) lyotropic liquid crystal salts ordinarily insoluble in anhydrous, aprotic, ligand-type solvents, (b) non-polymeric ligand-type solvents containing the NCO group, (c) polymeric-type ligands containing repetitive, oxygen-bearing groups along a substantially linear chain, and (d) from 1% to 98% by weight of inorganic compounds of high surface area. The complexation and solubilization can be carried out so as to secure liquids or low viscosity pastes by heating and mixing the components in appropriate ratios. Or the components can be fluxed in a Banbury mixer or its equivalent at an elevated temperature using limited quantities of a non-polymeric, ligand-type solvent so that the final product is a solid. Vacuum processing can be used to degas these systems and insure superb wetting. Formed shapes of the products can be heated so as to remove additional non-polymeric, ligand-type solvents where desired. Depending on the inorganic compound of high surface area selected and its concentration in the final product, enhanced yield value, enhanced and stabilized superconductivity, improved abrasion resistance, and other desirable features may be secured. As an alternate mode of preparing liquid or paste compositions, the solid salt complexes can be complexed and fluidized by heating with liquid polymers such as polyethelene glycol and inorganic compounds of high surface area.
摘要翻译：本发明提供用作超导体的新型化学络合产物，用于碱金属电池的聚合物电解质，用于电致变色窗的电解质，静电耗散塑料等。它还提供制造这种络合产物。络合产物可以包含（a）通常不溶于无水，非质子，配体型溶剂的溶致液晶盐，（b）含有NCO基团的非聚合配体型溶剂，（c）含有重复的氧的聚合型配体 - （d）1至98重量％的高表面积的无机化合物。可以进行络合和溶解以便通过以适当的比例加热和混合组分来确保液体或低粘度浆料。或者组分可以使用有限量的非聚合物配体型溶剂在Banbury混合器或其等同物中在高温下熔化，使得最终产物为固体。真空处理可用于对这些系统进行脱气并确保极好的润湿。可以加热形成的产品形状，以便在需要时去除另外的非聚合的配体型溶剂。取决于所选择的高表面积和其在最终产品中的浓度的无机化合物，可以确保增强的屈服值，增强和稳定的超导性，改善的耐磨性和其它所需特征。作为制备液体或糊料组合物的替代方式，固体盐络合物可以通过用诸如聚乙二醇和高表面积的无机化合物的液体聚合物加热来络合和流化。

3. 发明授权

US4175207A Visual-type hygrometer 失效
标题翻译：视觉式湿度计
公开(公告)号：US4175207A
公开(公告)日：1979-11-20
申请号：US795163
申请日：1977-05-09
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： C07C65/24 , G01N31/22 , G02B27/26 , C07C65/20
CPC分类号： G02B27/26 , C07C65/24 , G01N31/222
摘要： A composition of matter for use in a visual-type instrument which includes a polarizer for a light beam and an analyzer for a light beam, the chemical composition being birefringent at a first relative humidity and nonbirefringent at a second relative humidity.
摘要翻译：一种用于包括光束偏振器和光束分析仪的视觉仪器中的物质组合物，所述化学成分在第一相对湿度下是双折射的，并且在第二相对湿度下是非双折射的。

4. 发明授权

US5022045A Optical-type, phase transition humidity-responsive devices 失效
标题翻译：光学型，相变湿度响应装置
公开(公告)号：US5022045A
公开(公告)日：1991-06-04
申请号：US547314
申请日：1990-07-05
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： G01N21/81
CPC分类号： G01N21/81
摘要： The invention is directed to chemical compositions suitable for use in salt-solution transition temperature or hot mirror devices. It also provides methods of using these sensors (for the measurement of the humidity of gases) as well as the apparatus. The chemical composition which of itself senses the changes of water vapor pressure is birefringent at a first water vapor pressure and temperature, but non-birefringent at a second vapor pressure and temperature. The optical changes which accompany these phase changes may be amplified with polarizers. The means for heating the chemical composition can vary widely. Various thermometric devices can be used for temperature sensing. The accuracy required of the particular instrument model, the device's configuration, and the other components, selected for the particular system all affect the choice of thermometric device selected. The light detector is responsive to observable changes in the brightness and intensity of the light emerging from the chemical composition, the light from the composition at a particular water vapor pressure and temperature being of sufficient brightness and intensity to provide an optical signal to activate the light-detecting electrical means.
摘要翻译：本发明涉及适用于盐溶液转变温度或热反射镜装置的化学组合物。它还提供了使用这些传感器（用于测量气体湿度）以及设备的方法。本身感觉到水蒸汽压力变化的化学组成在第一水蒸气压和温度下是双折射的，但在第二蒸气压和温度下是双折射的。伴随这些相变的光学变化可以用偏振器放大。用于加热化学成分的方法可以变化很大。各种测温装置可用于温度检测。为特定系统选择的特定仪器型号，设备配置和其他组件所需的精度都会影响所选择的温度计设备的选择。光检测器响应于从化学成分出现的光的亮度和强度的可观察的变化，来自组合物的光在特定水蒸汽压力和温度下具有足够的亮度和强度，以提供光信号来激活光 - 检测电气装置。

5. 发明授权

US4166891A Visual-type hygrometer 失效
公开(公告)号：US4166891A
公开(公告)日：1979-09-04
申请号：US654087
申请日：1976-02-02
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： C08K5/00 , G02B27/26 , C08L1/28 , C08L33/02 , C08L35/06
CPC分类号： G02B27/26 , C08K5/0091 , Y10S252/963
摘要： A composition of matter for use in a visual-type instrument which includes a polarizer for a light beam and an analyzer for a light beam, the chemical composition being birefringent at a first relative humidity and nonbirefringent at a second relative humidity.

6. 发明授权

US4072055A Visual-type temperature-responsive device 失效
标题翻译：视觉型温度敏感装置
公开(公告)号：US4072055A
公开(公告)日：1978-02-07
申请号：US759483
申请日：1977-01-14
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： G01K11/06 , G01K11/12
CPC分类号： G01K11/06 , G01K11/12
摘要： A visual-type temperature-responsive device and a method for indicating and measuring temperature including a source for providing a light beam, and means for providing observable changes in temperature of a chemical composition that of itself senses changes in temperature by being abruptly triggered at a desired temperature.
摘要翻译：视觉型温度响应装置和用于指示和测量包括用于提供光束的光源的温度的方法，以及用于提供本身感觉温度变化的化学组成的可观察到的温度变化的装置，所需温度。

7. 发明授权

US5833877A Reaction products of lyotropic liquid crystal salt complexes 失效
标题翻译：溶致液晶盐络合物的反应产物
公开(公告)号：US5833877A
公开(公告)日：1998-11-10
申请号：US676775
申请日：1996-07-08
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： B01D21/01 , C04B33/30 , C09K19/40 , G01N21/81 , G01N27/22 , H01L39/12 , C09K19/52 , H01B1/00
CPC分类号： B01D21/01 , C04B33/30 , C09K19/40 , G01N21/81 , G01N27/225 , H01L39/121 , Y10T428/10
摘要： The invention provides novel non-polymeric and polymeric complexes and reaction products of lyotropic liquid crystal salts of aroyl acids which when anhydrous are excellent electrical conductors and superconductors of high critical temperature. The salts can be of various metals but especially of the alkali metals. The invention also provides reaction products of the complexes with copper metal, the products having excellent tarnish-resistant properties which make them suitable for protecting circuit boards and such from corrosion during storage. Copper/polymeric aroylacrylate salt reaction products when amorphous, especially when present in a thin film form, make superconductors of high critical temperature and current. Further, the invention provides a flexible process for converting various essential, water-bearing components of these complexes and reaction products into stable, anhydrous solutions well suited for applying to various substrates. A modification of the process provides products which can be used to coat substrates which wet poorly. Thin films of the alkali metal polymeric lyotropic liquid crystal salt complexes, because of their affinity for water, which is accompanied by a rapid, sensitive change in electrical resistance, make excellent hygrometric devices. They are especially well suited for monitoring processes which require that these complexes, reaction products, and complexation products be maintained in the anhydrous state, since the hygrometer sensor material's electrical response parallels that of the product being produced, rising to very high resistances as the anhydrous state is approached.
摘要翻译：本发明提供新颖的非聚合物和聚合物络合物和芳族酸溶致液晶盐的反应产物，当无水是优异的电导体和高临界温度的超导体时。盐可以是各种金属，但特别是碱金属。本发明还提供了复合物与铜金属的反应产物，该产品具有优异的抗晦暗性能，使其适合于保护电路板，并且在储存期间不受腐蚀。当非晶体时，铜/聚合丙烯酸丙烯酸酯盐反应产物，特别是以薄膜形式存在时，使超导体具有高临界温度和电流。此外，本发明提供了一种灵活的方法，用于将这些络合物和反应产物的各种必需的含水组分转化成稳定的，非常适用于各种基材的无水溶液。该方法的改进提供了可用于涂覆不良润湿的基材的产品。碱金属聚合物溶致液晶盐络合物的薄膜由于它们对水的亲和力，伴随着电阻的快速，敏感的变化，使得优异的湿度测定装置。它们特别适用于需要将这些络合物，反应产物和络合产物保持在无水状态的监测过程，因为湿度计传感器材料的电响应与正在生产的产品的电响应相似，随着无水状态的升高至非常高的电阻接近状态。

8. 发明授权

US5595683A Reaction products of lyotropic liquid crystal salt complexes 失效
标题翻译：溶致液晶盐络合物的反应产物
公开(公告)号：US5595683A
公开(公告)日：1997-01-21
申请号：US447990
申请日：1995-05-23
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： B01D21/01 , C04B33/30 , G01N21/81 , G01N27/22 , C09K19/52 , C09K19/34 , C09K19/32
CPC分类号： G01N27/225 , B01D21/01 , C04B33/30 , C09K19/062 , C09K19/066 , C09K19/32 , C09K19/322 , G01N21/81 , C09K2019/122 , C09K2019/3422 , Y02P20/544 , Y10T428/10
摘要： The invention provides novel polymeric and non-polymeric, liquid crystal type, chemical salt complexes of aroyl acids and monovalent and polyvalent metals. They are formed by covalent and coordinate bonding for use as electrical superconductors, as electrolytes in alkali metal batteries, electrochromic windows, static dissipative polymers, etc. The invention also provides processes for manufacturing such complexes, including the in situ formation in and on various metals and oxides. The processes also include the use of supercritical solvents such as carbon dioxide to solubilize the complexes for introduction into plastics and inorganic superconductors. The chemical complexes include the triads formed of liquid crystal aroyl salts, non-polymeric ligand solvents, and polymeric aroylacrylate salts. Both homopolymer and copolymer complexes of the metal aroylacrylates may be prepared and the latter may be cross-linked. Novel covalent, liquid crystal, reaction product complexes of lyotropic liquid crystal, metal aroylacrylate complexes and isocyanates (both polymeric and non-polymeric) are prepared. These are dyes having a high degree of conjugated unsaturation. Solutions of the reaction products of monovalent and polyvalent metal complexes can be prepared. Excess ligand solvent; used in preparing these materials can be vaporized in a controlled way to produce liquid crystal systems. These systems can be cross-linked. Supercritical fluids such as carbon dioxide can be used to dissolve these various complexes and allow their distribution into both plastic particles and powdered inorganic superconductors so as to distribute complexes uniformly throughout the particles so as to enhance properties such as electrical conductivity when the particles are formed into larger systems.
摘要翻译：本发明提供新颖的聚合物和非聚合物，液晶型的芳酰基酸和一价和多价金属的化学盐络合物。它们通过共价和配位键形成，用作电超导体，作为碱金属电池中的电解质，电致变色窗，静电耗散聚合物等。本发明还提供了制造这种络合物的方法，包括在各种金属中以及其上的原位形成和氧化物。该方法还包括使用超临界溶剂如二氧化碳来溶解配合物以引入塑料和无机超导体中。化学络合物包括由液晶芳酰基盐，非聚合配体溶剂和聚合丙烯酸丙烯酸酯盐形成的三单元组。可以制备金属丙烯酸芳基酯的均聚物和共聚物络合物，后者可以是交联的。制备新型共价液晶，溶致液晶的反应产物络合物，丙烯酸丙烯酸金属络合物和异氰酸酯（聚合物和非聚合物）。这些是具有高度共轭不饱和度的染料。可以制备单价和多价金属络合物的反应产物的溶液。过量配体溶剂; 用于制备这些材料的物质可以以受控的方式蒸发以产生液晶体系。这些系统可以交互。可以使用诸如二氧化碳的超临界流体来溶解这些各种配合物，并使它们分布在塑料颗粒和无机超导体粉末中，以便将复合物均匀地分布在整个颗粒中，以便当颗粒形成时提高诸如导电性的性能较大的系统。

9. 发明授权

US5443753A Reaction products of lyotropic liquid crystal salt complexes 失效
标题翻译：溶致液晶盐络合物的反应产物
公开(公告)号：US5443753A
公开(公告)日：1995-08-22
申请号：US239619
申请日：1994-05-09
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： B01D21/01 , C04B33/30 , G01N21/81 , G01N27/22 , C09K19/52
CPC分类号： G01N27/225 , B01D21/01 , C04B33/30 , C09K19/062 , C09K19/066 , C09K19/32 , C09K19/322 , G01N21/81 , C09K2019/122 , C09K2019/3422 , Y02P20/544 , Y10T428/10
摘要： The invention provides novel polymeric and non-polymeric, liquid crystal type, chemical salt complexes of aroyl acids and monovalent and polyvalent metals. They are formed by covalent and coordinate bonding for use as electrical superconductors, as electrolytes in alkali metal batteries, electrochromic windows, static dissipative polymers, etc. The invention also provides processes for manufacturing such complexes, including the in situ formation in and on various metals and oxides. The processes also include the use of supercritical solvents such as carbon dioxide to solubilize the complexes for introduction into plastics and inorganic superconductors. The chemical complexes include the triads formed of liquid crystal aroyl salts, non-polymeric ligand solvents, and polymeric aroylacrylate salts. Both homopolymer and copolymer complexes of the metal aroylacrylates may be prepared and the latter may be cross-linked. Novel covalent, liquid crystal, reaction product complexes of lyotropic liquid crystal, metal aroylacrylate complexes and isocyanates (both polymeric and non-polymeric) are prepared. These are dyes having a high degree of conjugated unsaturation. Solutions of the reaction products of monovalent and polyvalent metal complexes can be prepared. Excess ligand solvents used in preparing these materials can be vaporized in a controlled way to produce liquid crystal systems. These systems can be cross-linked. Supercritical fluids such as carbon dioxide can be used to dissolve these various complexes and allow their distribution into both plastic particles and powdered inorganic superconductors so as to distribute complexes uniformly throughout the particles so as to enhance properties such as electrical conductivity when the particles are formed into larger systems.
摘要翻译：本发明提供新颖的聚合物和非聚合物，液晶型的芳酰基酸和一价和多价金属的化学盐络合物。它们通过共价和配位键形成，用作电超导体，作为碱金属电池中的电解质，电致变色窗，静电耗散聚合物等。本发明还提供了制造这种络合物的方法，包括在各种金属中以及其上的原位形成和氧化物。该方法还包括使用超临界溶剂如二氧化碳来溶解配合物以引入塑料和无机超导体中。化学络合物包括由液晶芳酰基盐，非聚合配体溶剂和聚合丙烯酸丙烯酸酯盐形成的三单元组。可以制备金属丙烯酸芳基酯的均聚物和共聚物络合物，后者可以是交联的。制备新型共价液晶，溶致液晶的反应产物络合物，丙烯酸丙烯酸金属络合物和异氰酸酯（聚合物和非聚合物）。这些是具有高度共轭不饱和度的染料。可以制备单价和多价金属络合物的反应产物的溶液。用于制备这些材料的过量配体溶剂可以以受控的方式蒸发以产生液晶体系。这些系统可以交互。可以使用诸如二氧化碳的超临界流体来溶解这些各种配合物，并使它们分布在塑料颗粒和无机超导体粉末中，以便将复合物均匀地分布在整个颗粒中，以便当颗粒形成时提高诸如导电性的性能较大的系统。

10. 发明授权

US5354499A Reaction products of lyotropic liquid crystal salt complexes 失效
标题翻译：溶致液晶盐络合物的反应产物
公开(公告)号：US5354499A
公开(公告)日：1994-10-11
申请号：US954556
申请日：1992-09-30
申请人： Stanley B. Elliott
发明人： Stanley B. Elliott
IPC分类号： G01N21/81 , G01N27/22 , C09K19/54 , B01D9/00 , C09K19/52
CPC分类号： G01N21/81 , C09K19/062 , C09K19/32 , C09K19/322 , G01N27/225 , C09K2019/122 , Y02P20/544
摘要： The invention provides novel polymeric and non-polymeric, liquid crystal type, chemical salt complexes of aroyl acids and monovalent and polyvalent metals. They are formed by covalent and coordinate bonding for use as electrical superconductors, as electrolytes in alkali metal batteries, electrochromic windows, static dissipative polymers, etc. The invention also provides processes for manufacturing such complexes, including the in situ formation in and on various metals and oxides. The processes also include the use of supercritical solvents such as carbon dioxide to solubilize the complexes for introduction into plastics and inorganic superconductors. The chemical complexes include the triads formed of liquid crystal aroyl salts, non-polymeric ligand solvents, and polymeric aroylacrylate salts. Both homopolymer and copolymer complexes of the metal aroylacrylates may be prepared and the latter may be cross-linked. Novel covalent, liquid crystal, reaction product complexes of lyotropic liquid crystal, metal aroylacrylate complexes and isocyanates (both polymeric and non-polymeric) are prepared. These are dyes having a high degree of conjugated unsaturation. Solutions of the reaction products of monovalent and polyvalent metal complexes can be prepared. Excess ligand solvents used in preparing these materials can be vaporized in a controlled way to produce liquid crystal systems. These systems can be cross-linked. Supercritical fluids such as carbon dioxide can be used to dissolve these various complexes and allow their distribution into both plastic particles and powdered inorganic superconductors so as to distribute complexes uniformly throughout the particles so as to enhance properties such as electrical conductivity when the particles are formed into larger systems.
摘要翻译：本发明提供新颖的聚合物和非聚合物，液晶型的芳酰基酸和一价和多价金属的化学盐络合物。它们通过共价和配位键形成，用作电超导体，作为碱金属电池中的电解质，电致变色窗，静电耗散聚合物等。本发明还提供了制造这种络合物的方法，包括在各种金属中以及其上的原位形成和氧化物。该方法还包括使用超临界溶剂如二氧化碳来溶解配合物以引入塑料和无机超导体中。化学络合物包括由液晶芳酰基盐，非聚合配体溶剂和聚合丙烯酸丙烯酸酯盐形成的三单元组。可以制备金属丙烯酸芳基酯的均聚物和共聚物络合物，后者可以是交联的。制备新型共价液晶，溶致液晶的反应产物络合物，丙烯酸丙烯酸金属络合物和异氰酸酯（聚合物和非聚合物）。这些是具有高度共轭不饱和度的染料。可以制备单价和多价金属络合物的反应产物的溶液。用于制备这些材料的过量配体溶剂可以以受控的方式蒸发以产生液晶体系。这些系统可以交互。可以使用诸如二氧化碳的超临界流体来溶解这些各种配合物，并使它们分布在塑料颗粒和无机超导体粉末中，以便将复合物均匀地分布在整个颗粒中，以便当颗粒形成时提高诸如导电性的性能较大的系统。

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