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1. 发明申请

US20210078923A1 METHOD FOR PRODUCTION OF A HALOGENATED ALKANE USING AN ABSORBER-REACTOR COMBINATION 有权
公开(公告)号：US20210078923A1
公开(公告)日：2021-03-18
申请号：US17041321
申请日：2019-04-02
申请人： BLUE CUBE IP LLC
发明人： John D. Myers , Max Tirtowidjojo , Marc Sell , Thomas Luebbe
IPC分类号： C07C17/275
摘要： The present invention provides improved processes for preparing halogenated alkanes. The processes comprise contacting at least one alkene, a halogenated alkene, or combinations thereof with a halogenated methane with at least one chlorine atom to form a liquid phase. This liquid phase is then contacted with at least one catalytic species which initiates the reaction with at least one alkene, a halogenated alkene, or combinations thereof with a halogenated methane with at least one chlorine atoms.

2. 发明授权

US10442941B2 Curable compositions 有权
公开(公告)号：US10442941B2
公开(公告)日：2019-10-15
申请号：US15558796
申请日：2016-03-17
申请人： BLUE CUBE IP LLC
发明人： Hamed Lakrout , Katherine Clement , Maurice J. Marks
IPC分类号： C09D11/101 , C09D11/30 , C09D11/322 , C09D11/38
摘要： A heat stable radiation curable epoxy resin composition for preparing an ink composition including: (a) at least one divinylarene dioxide compound; (b) at least one photoinitiator compound; (c) at least one pigment; and (d) at least one optional additive wherein the at least one photoinitiator compound is a triarylsulfonium salt; wherein the at least one pigment is (i) a cyan pigment, or (ii) a magenta pigment; a process for preparing the above heat stable radiation curable epoxy resin composition; and a cured inkjet ink product prepared by curing the above heat stable radiation curable epoxy resin composition.

3. 发明授权

US10329226B2 Process for the production of chlorinated methanes 有权
公开(公告)号：US10329226B2
公开(公告)日：2019-06-25
申请号：US15759728
申请日：2016-09-22
申请人： BLUE CUBE IP LLC
发明人： John D. Myers , Matthew L. Grandbois
IPC分类号： C07C17/04 , C07C17/10 , C07C17/25 , C07C19/03 , C07C19/04 , C07C19/05 , C07C21/10 , C07C17/013 , C07C17/383 , C07C17/395 , C07C19/041 , C07C19/043 , C07C19/045 , C07C19/055
摘要： The present invention provides processes for the production of chlorinated methanes via the direct chlorination of methane. The processes include a dehydrochlorination and/or chlorination step that converts up to 100% of the higher chlorinated alkanes in a process stream from the methane chlorination reaction into more highly chlorinated alkanes. These more highly chlorinated alkanes can be easily removed from the process stream. The use of a cost effective feedstream of crude methane is thus rendered possible, without additional capital expenditure for the sophisticated separation equipment required to separate ethane and other hydrocarbon components from the methane feed.

4. 发明申请

US20190169100A1 PROCESS FOR THE DEHYDROCHLORINATION OF A CHLOROALKANE 审中-公开
公开(公告)号：US20190169100A1
公开(公告)日：2019-06-06
申请号：US16311761
申请日：2017-06-22
申请人： BLUE CUBE IP LLC
发明人： John D. Myers , Max Tirtowidjojo
IPC分类号： C07C17/25 , C07C17/04 , B01J27/10
摘要： A process for the production of a chloroalkene that includes contacting a liquid phase chloroalkane with a solid catalyst, a catalyst deposited on a solid substrate, or combinations thereof, thereby causing the dehydrochlorination of the chloroalkane to produce a chloroalkene product and HCl. Processes for the production of 1,1,2,3-tetrachloropropene and 1,1,1,2,3-pentachloropropane are further provided.

5. 发明授权

US09695271B2 Distilled epoxy novolac resins 有权
公开(公告)号：US09695271B2
公开(公告)日：2017-07-04
申请号：US15103097
申请日：2014-12-17
申请人： BLUE CUBE IP LLC
发明人： William W. Fan , Dennis W. Jewell , Stephen B. Wallace , Marvin L. Dettloff , Travis H. Larsen
IPC分类号： C08G64/00 , C08G59/02 , C08G59/08 , B01D5/00 , B01D3/32 , C08G63/02
CPC分类号： C08G59/025 , B01D3/32 , B01D5/006 , C08G59/08
摘要： A continuous process comprising a) separating an epoxy novolac resin comprising oligomers having an average functionality of greater than 2.5 and a hydrolyzable chlorine content of less than 450 ppm with a continuous evaporator apparatus to form i) a first distillate vapor fraction comprising epoxy novolac resin having more than 75 weight percent of 2 functional components and wherein the mass of the first distillate vapor fraction is in the range of from 15 to 40 weight percent of the starting epoxy novolac resin; and ii) a first bottom fraction comprising epoxy novolac resin having less than 5 weight percent of 2 functional components and having a glass transition temperature of at least 15 C higher compared to the starting epoxy novolac resin when cured; b) recovering the first bottom fraction product; and c) condensing the first distillate vapor fraction to form a first condensed distillate vapor fraction; d) separating the first condensed distillate vapor fraction with a second continuous evaporator apparatus to form i) a second distillate vapor fraction wherein the mass of the second distillate vapor fraction is in the range of from 40 to 70 weight percent of the first condensed distillate vapor fraction; and ii) a second bottom fraction; e) recovering the second bottom fraction product; and f) condensing the second distillate vapor fraction to form a second condensed distillate vapor fraction product comprising at least 98 weight percent of 2 functional components with a total chlorine content less than 900 ppm, is disclosed.

6. 发明授权

US09605161B2 Conductive carbonized layered article 有权
公开(公告)号：US09605161B2
公开(公告)日：2017-03-28
申请号：US14391714
申请日：2013-05-17
申请人： Blue Cube IP LLC
发明人： Hamed Lakrout , Maurice J. Marks , Ludovic Valette
IPC分类号： C09D5/24 , C04B35/524 , C08J3/00 , C08L63/00 , C04B35/626 , C04B35/634 , H01B1/24 , B82Y10/00 , H01B1/04 , C03C17/22 , H01L51/00 , H01L51/44
CPC分类号： C09D5/24 , B82Y10/00 , C03C17/22 , C03C2217/28 , C04B35/524 , C04B35/6269 , C04B35/63452 , C04B2235/9653 , C08J3/00 , C08L63/00 , H01B1/04 , H01B1/24 , H01L51/0045 , H01L51/442 , Y10T428/265
摘要： A process for preparing a conductive carbonized layered article including the steps of: (I) providing a liquid carbon precursor formulation comprising (a) at least one aromatic epoxy resin; and (b)(i) at least one aromatic co-reactive curing agent, (b) (ii) at least one catalytic curing agent, or (b)(iii) a mixture thereof; wherein the liquid precursor composition has a neat viscosity of less than 10,000 mPa-s at 25° C. prior to adding optional components, prior to curing, and prior to carbonizing; and wherein the liquid precursor composition being cured has a carbon yield of at least 35 weight percent disregarding the weight of the substrate and any optional components present in the composition; (II) applying the liquid formulation of step (I) as a thin coating layer onto at least a portion of the surface of a substrate; (III) curing the liquid formulation of step (II) to form a cured product, wherein the cured product has a carbon yield of at least 35 weight percent disregarding the weight of the substrate and any optional components present in the composition; and (IV) carbonizing the cured product of step (III) to form a conductive carbonized layered article; and a conductive carbonized layered article such as a carbon optical transparent electrode (COTE) prepared by the above process.

7. 发明授权

US09388297B2 Phosphorus-containing compounds useful for making halogen-free, ignition-resistant polymers 有权
标题翻译：含磷化合物可用于制备无卤素，耐点火聚合物
公开(公告)号：US09388297B2
公开(公告)日：2016-07-12
申请号：US14110939
申请日：2012-05-01
申请人： Anteneh Z. Worku , Michael J. Mullins
发明人： Anteneh Z. Worku , Michael J. Mullins
IPC分类号： C08K5/5313 , C07F9/6571 , C08K5/527 , C08K5/5393 , C09J11/06 , C08K5/00
CPC分类号： C08K5/51 , C07F9/28 , C07F9/657172 , C07F9/657181 , C08J5/24 , C08J2363/04 , C08K5/0066 , C08K5/527 , C08K5/5313 , C08K5/5393 , C09D163/04 , C09J11/06 , C09J163/04 , H05K1/0353
摘要： A process for making a phosphorus-containing compound is disclosed. The process comprises contacting a compound of formula (A) wherein RA and RB are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups or can be combined to form cyclic structures; and RC is methyl, ethyl, isopropyl, n-butyl, i-butyl, t-butyl, phenyl or benzyl; and a compound of formula (B) wherein R1-R4 are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups. The phosphorus-containing compound can then be used as a flame retardants for polymers, especially for epoxy, polyurethane, thermosetting resins and thermoplastic polymers. Such flame retardant-containing polymers can be used to make protective coating formulations and ignition-resistant fabricated articles, such as electrical laminates, polyurethane foams, and various molded and/or foamed thermoplastic products.
摘要翻译：公开了一种制备含磷化合物的方法。该方法包括使其中RA和RB选自任选取代的芳基，芳氧基，烷基和烷氧基的式（A）化合物或可以组合形成环状结构; 乙基，异丙基，正丁基，异丁基，叔丁基，苯基或苄基; 和式（B）的化合物，其中R 1 -R 4选自任选取代的芳基，芳氧基，烷基和烷氧基。然后可以将含磷化合物用作聚合物的阻燃剂，特别是用于环氧树脂，聚氨酯，热固性树脂和热塑性聚合物。这种含阻燃剂的聚合物可用于制备保护性涂料配方和耐点火制造品，例如电层压材料，聚氨酯泡沫以及各种模制和/或发泡热塑性产品。

8. 发明授权

US09267030B2 Compositions having phosphorus-containing compounds 有权
标题翻译：具有含磷化合物的组合物
公开(公告)号：US09267030B2
公开(公告)日：2016-02-23
申请号：US13575617
申请日：2011-01-26
申请人： Kamesh Vyakaranam , Mark B. Wilson , Endre Szuromi , Michael J. Mullins
发明人： Kamesh Vyakaranam , Mark B. Wilson , Endre Szuromi , Michael J. Mullins
IPC分类号： H01B3/40 , C08L63/04 , C08G59/40
CPC分类号： C08L63/04 , C08G59/4014
摘要： Embodiments of the present disclosure provide a composition that includes a phosphorous-containing compound, a cyanate ester, an epoxy resin, and a maleimide. For the various embodiments, a viscosity of the composition increases less than 100% as measured by Gardner Bubble Viscosity a temperature of 23° C. in at least 3 days. For the various embodiments, the composition of the present disclosure can also include an aprotic solvent, such as a ketone. Embodiments of the present disclosure further include a composition that includes the phosphorous-containing compound, the cyanate ester, and the aprotic solvent. For the various embodiments, the composition can also include the epoxy resin and the maleimide. For the various embodiments, the composition does not include an aliphatic alcohol.
摘要翻译：本公开的实施方案提供了包含含磷化合物，氰酸酯，环氧树脂和马来酰亚胺的组合物。对于各种实施方案，组合物的粘度增加小于100％，如通过Gardner Bubble Viscosity在至少3天内23℃的温度测量的。对于各种实施方案，本公开的组合物还可以包括非质子溶剂，例如酮。本公开的实施方案还包括包含含磷化合物，氰酸酯和非质子传递溶剂的组合物。对于各种实施方案，组合物还可以包括环氧树脂和马来酰亚胺。对于各种实施方案，组合物不包括脂族醇。

9. 发明授权

US09102787B2 Curable compositions 有权
标题翻译：可固化组合物
公开(公告)号：US09102787B2
公开(公告)日：2015-08-11
申请号：US13508450
申请日：2010-11-12
申请人： Markus Schroetz , Eva-Maria Michalski , Klaus Reinhold , Christina Fritsche
发明人： Markus Schroetz , Eva-Maria Michalski , Klaus Reinhold , Christina Fritsche
IPC分类号： B32B27/38 , C09D163/00 , C08G59/38 , C08G59/50 , C08G59/62 , C08G59/18 , C08L63/00
CPC分类号： C08G59/623 , C08G59/184 , C08L63/00 , C09D163/00 , C08L2666/22
摘要： Embodiments include curable compositions including a resin component and a hardener component. The resin component can include an epoxy compound that is selected from the group consisting of aromatic epoxy compounds, alicyclic epoxy compounds, aliphatic epoxy compounds, and combinations thereof, and a reactive diluent that includes a polymeric glycidyl ether. The hardener component can include an adduct and a Mannich base.
摘要翻译：实施方案包括包括树脂组分和硬化剂组分的可固化组合物。树脂组分可以包括选自芳族环氧化合物，脂环族环氧化合物，脂肪族环氧化合物及其组合的环氧化合物，以及包含聚合缩水甘油醚的反应性稀释剂。硬化剂组分可以包括加合物和曼尼希碱。

10. 发明授权

US09074041B2 Curable epoxy resin compositions and composites made therefrom 有权
标题翻译：可固化的环氧树脂组合物和由其制成的复合材料
公开(公告)号：US09074041B2
公开(公告)日：2015-07-07
申请号：US13389028
申请日：2010-09-21
申请人： Marvin L. Dettloff , Gary A. Hunter , Susan K. Falcone-Potts , Ha Q. Pham , Martine Rousse , Bernd Hoevel
发明人： Marvin L. Dettloff , Gary A. Hunter , Susan K. Falcone-Potts , Ha Q. Pham , Martine Rousse , Bernd Hoevel
IPC分类号： B32B27/04 , B32B27/20 , B32B27/26 , B32B27/38 , C08J5/24 , C08G59/22 , C08G59/50 , C08G59/56 , C08G59/64 , C08G59/62 , C08L63/00 , C08K5/13
CPC分类号： C08G59/64 , C08G59/621 , C08J5/24 , C08J2363/02
摘要： A curable epoxy resin composite composition including a reinforcing material and an epoxy resin composition, and a process for preparing a composite from such composition; wherein a combination of at least one alkanolamine and at least one styrenated phenol are present in the epoxy resin composition in a sufficient amount to increase the rate of reaction of the at least one epoxy resin and the at least one alkanolamine curing agent while maintaining the thermal and mechanical properties of the composite upon curing of the epoxy resin composition.
摘要翻译：包含增强材料和环氧树脂组合物的可固化环氧树脂复合组合物及其制备方法。其中至少一种链烷醇胺和至少一种苯乙烯化酚的组合以足够的量存在于环氧树脂组合物中以提高至少一种环氧树脂和至少一种链烷醇胺固化剂的反应速率同时保持热以及环氧树脂组合物固化时复合材料的机械性能。

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