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1. 发明申请

US20140263673A1 Thermally-Responsive Record Material 有权
标题翻译：热敏记录材料
公开(公告)号：US20140263673A1
公开(公告)日：2014-09-18
申请号：US14051906
申请日：2013-10-11
申请人： Fadi Selim Chakar , Mark Robert Fisher
发明人： Fadi Selim Chakar , Mark Robert Fisher
IPC分类号： B41M5/333 , G06K19/06 , B41M5/337
CPC分类号： B41M5/3336 , B41M5/3275 , B41M5/3375 , G06K19/06028
摘要： The invention describes an improved thermally-responsive record material substantially free of aromatic isocyanate yielding an image of high intensity and useful for bar codes. The record material comprises a support having provided thereon a heat-sensitive composition comprising a substantially colorless color former comprising a fluoran; and a developer material selected from the group consisting of 4,4′-diaminodiphenylsulfone and 3,3′-diaminodiphenylsulfone, and an organic acid which upon being heated reacts with said color former to develop color, and including a binder material. Optionally, a modifier compound is included in the heat-sensitive composition. The compound can be selected from the group consisting of a fatty acid amide, such as stearmide. Optionally, magnesium state is included.
摘要翻译：本发明描述了一种基本上不含芳族异氰酸酯的改进的热响应记录材料，产生高强度的图像并且可用于条形码。记录材料包括其上提供有热敏组合物的载体，所述组合物包含基本上无色的着色剂，其包含荧烷; 和选自4,4'-二氨基二苯砜和3,3'-二氨基二苯砜的显影剂材料，以及被加热的有机酸与所述成色剂反应显色，并包括粘合剂材料。任选地，在热敏组合物中包括改性剂化合物。化合物可以选自脂肪酸酰胺如硬脂酰胺。任选地，包括镁状态。

2. 发明授权

US09534156B2 Linerless record material 有权
标题翻译：无衬里记录材料
公开(公告)号：US09534156B2
公开(公告)日：2017-01-03
申请号：US14488829
申请日：2014-09-17
申请人： APPVION, INC.
发明人： Mark Robert Fisher
IPC分类号： B41M5/26 , B41M5/50 , G09F3/10 , C09J133/08 , C09D133/08 , C08K5/101 , B41M5/42 , B41M5/44 , G09F3/02
CPC分类号： C09J133/08 , B32B2519/02 , B41M5/42 , B41M5/44 , B41M5/504 , B41M2205/04 , B41M2205/36 , C08K5/101 , C09D133/08 , G09F3/10 , G09F2003/0211 , Y10T428/2817 , C08K5/12
摘要： The invention describes a composition and method of providing an improved recording material, such as an ink receptive recording material or thermally responsive record material useful for linerless labels. The record material comprises a support having provided thereon on one surface an adhesive material, and on at least one other surface, an ink receptive coating or a heat sensitive imaging coating. The method comprises applying to a first surface a first layer of a coating of an ink receptive material or of a heat sensitive color-forming composition comprising a binder material and a substantially colorless dye precursor and an acidic developer material in substantially contiguous relationship. The adhesive is heat activated. The record material exhibits substantially no tack at 23° C., 40% relative humidity when pressure is applied, however develops high peel strength (300 grams/inch) upon application of 7 mJ/mm2 to 13 mJ/mm2 of heat energy.
摘要翻译：本发明描述了提供改进的记录材料的组合物和方法，例如可用于无衬标签的油墨接受记录材料或热响应记录材料。记录材料包括在一个表面上在其上提供粘合剂材料的支撑件，以及在至少一个其它表面上的油墨接受涂层或热敏成像涂层。该方法包括向基片的第一表面施加第一层油墨接收材料或热敏成色组合物的第一层，其包含粘合剂材料和基本上无色的染料前体和基本连续的关系的酸性显影剂材料。粘合剂被热激活。记录材料在施加压力时在23℃，40％的相对湿度下基本上没有粘性，但是当施加7mJ / mm 2至13mJ / mm 2的热能时，其产生高的剥离强度（300克/英寸）。

3. 发明申请

US20150125617A1 ACTIVATOR MEANS FOR PRE-APPLIED ADHESIVES 有权
标题翻译：激活剂用于预应用粘合剂的方法
公开(公告)号：US20150125617A1
公开(公告)日：2015-05-07
申请号：US14550984
申请日：2014-11-22
申请人： Appvion, Inc.
发明人： John MacKay Lazar , Todd Arlin Schwantes , Frederick Edward Charles Lidington
IPC分类号： C09J5/00 , B05D3/12 , B32B37/12
CPC分类号： C09J5/00 , B01J13/02 , B05D3/12 , B32B37/12 , B32B2037/1269 , C08J3/24 , C08J3/241 , Y10T156/1798 , Y10T428/24479
摘要： An activator means for use in activating or re-activating adhesive and sealant compositions that have been pre-applied to a bonding surface prior to mating said bonding surface said means having a plurality of features for directly acting upon the pre-applied composition.
摘要翻译：用于活化或重新活化粘合剂和密封剂组合物的活化剂装置，其在配合所述粘合表面之前预先施加到粘合表面，所述装置具有用于直接作用于预先施用的组合物的多个特征。

4. 发明授权

US08916496B2 Thermally-responsive record material 有权
标题翻译：耐热响应记录材料
公开(公告)号：US08916496B2
公开(公告)日：2014-12-23
申请号：US14051906
申请日：2013-10-11
申请人： Fadi Selim Chakar , Mark Robert Fisher
发明人： Fadi Selim Chakar , Mark Robert Fisher
IPC分类号： B41M5/327 , B41M5/333 , B41M5/337 , G06K19/06
CPC分类号： B41M5/3336 , B41M5/3275 , B41M5/3375 , G06K19/06028
摘要： The invention describes an improved thermally-responsive record material substantially free of aromatic isocyanate yielding an image of high intensity and useful for bar codes. The record material comprises a support having provided thereon a heat-sensitive composition comprising a substantially colorless color former comprising a fluoran; and a developer material selected from the group consisting of 4,4′-diaminodiphenylsulfone and 3,3′-diaminodiphenylsulfone, and an organic acid which upon being heated reacts with said color former to develop color, and including a binder material. Optionally, a modifier compound is included in the heat-sensitive composition. The compound can be selected from the group consisting of a fatty acid amide, such as stearmide. Optionally, magnesium state is included.
摘要翻译：本发明描述了一种基本上不含芳族异氰酸酯的改进的热响应记录材料，产生高强度的图像并且可用于条形码。记录材料包括其上提供有热敏组合物的载体，所述组合物包含基本上无色的着色剂，其包含荧烷; 和选自4,4'-二氨基二苯砜和3,3'-二氨基二苯砜的显影剂材料，以及被加热的有机酸与所述成色剂反应显色，并包括粘合剂材料。任选地，在热敏组合物中包括改性剂化合物。化合物可以选自脂肪酸酰胺如硬脂酰胺。任选地，包括镁状态。

5. 发明申请

US20140186630A1 Microcapsule Particles 审中-公开
标题翻译：微胶囊颗粒
公开(公告)号：US20140186630A1
公开(公告)日：2014-07-03
申请号：US14104307
申请日：2013-12-12
申请人： Todd Arlin Schwantes
发明人： Todd Arlin Schwantes
IPC分类号： C09D167/04
CPC分类号： B01J13/14 , A01N25/28 , A23L27/72 , B01J13/185 , C09B67/0097 , C11D3/505 , C11D17/0039 , F28D20/023 , Y02E60/145 , Y10T428/2989
摘要： The present invention teaches microcapsule particles comprising an oil soluble or dispersible core material; and a wall material at least partially surrounding the core material, the microcapsule wall material consisting of the reaction product of a first composition in the presence of a second composition; the first composition comprising a water phase: the water phase comprising a water soluble or dispersible initiator having at least one —COOH or amine functional group and a nonionic emulsifier, the emulsifier comprising a water soluble or dispersible material at a pH from 4 to 12, the water soluble or dispersible initiator is selected from initiators having a C—N═N—C type structure and of formulas I, II or III (set forth in the specification) having amine or carboxyl functionality.The second composition comprises an oil phase. The oil phase comprises: i) one or more multi functional acrylate or methacrylate monomers or oligomers and substantially free of amine acrylate or amine methacrylate monomer or oligomer, and an initiator dispersible in the oil phase; ii) from 0 to 10% by weight of the oil phase, of a monofunctional acrylate or methacrylate monomer or oligomer; iii) an intended core material; and iv) a diluent selected from esters of glycerol and fatty acids wherein at least one of the fatty acids is C12 or greater; wherein the ratio of the water phase initiator to multifunctional acrylate or methacrylate is from 0.1:99.9 to 20:80 by weight; wherein the ratio of the diluent to the core material is from 0.1:99.9 to 90:10 on a weight basis; and whereby the reaction product of the first composition and second composition results in the formation of a population of microcapsules.
摘要翻译：本发明教导了包含油溶性或可分散核心材料的微胶囊颗粒; 以及至少部分地围绕所述芯材料的壁材料，所述微胶囊壁材料由第二组合物存在下的第一组合物的反应产物组成; 所述第一组合物包含水相：所述水相包含具有至少一个-COOH或胺官能团的水溶性或可分散的引发剂和非离子乳化剂，所述乳化剂包含pH为4至12的水溶性或可分散材料，水溶性或可分散的引发剂选自具有C-N = N-C型结构的引发剂和具有胺或羧基官能团的式I，II或III（在说明书中阐述）。第二组合物包含油相。油相包括：i）一种或多种多官能丙烯酸酯或甲基丙烯酸酯单体或低聚物，基本上不含胺丙烯酸酯或胺甲基丙烯酸酯单体或低聚物，和可分散在油相中的引发剂; ii）0至10重量％的油相，单官能丙烯酸酯或甲基丙烯酸酯单体或低聚物; iii）预期的核心材料; 和iv）选自甘油和脂肪酸的酯的稀释剂，其中至少一种脂肪酸为C12或更大; 其中水相引发剂与多官能丙烯酸酯或甲基丙烯酸酯的重量比为0.1:99.9至20:80; 其中所述稀释剂与所述芯材料的重量比为0.1:99.9至90:10; 并且由此第一组合物和第二组合物的反应产物导致形成一组微胶囊。

6. 发明授权

US09126451B2 Thermal recording materials 有权
标题翻译：热敏记录材料
公开(公告)号：US09126451B2
公开(公告)日：2015-09-08
申请号：US14132984
申请日：2013-12-18
申请人： Appvion, Inc.
发明人： Fadi Chakar , John Charles Warner , Justin Robert Whitfield , Michelle Wanchi Li Lugus , Deboshri Banerjee
IPC分类号： B41M5/337 , B41M5/327 , B41M5/333
CPC分类号： B41M5/3375 , B41M5/327 , B41M5/3275 , B41M5/3333 , B41M5/3335 , B41M5/3372 , B41M2205/04 , B41M2205/24
摘要： A thermal recording material having a heat-sensitive color-forming layer that contains a phosphate modifier in addition to an activator and lueco dye can provide good imaging. The phosphate modifier such as unsubstituted dibenzyl phosphate can be paired with an activator such 3-(4-hydroxyphenyl)propionic acid to provide an environmentally friendly thermal recording material.
摘要翻译：除了活化剂和lueco染料之外，具有含有磷酸酯改性剂的感热成色层的热敏记录材料可以提供良好的成像。磷酸酯改性剂如未取代的二苄基磷酸酯可以与活化剂如3-（4-羟基苯基）丙酸配对以提供环境友好的热敏记录材料。

7. 发明授权

US09034790B2 Thermally-responsive record material 有权
标题翻译：耐热响应记录材料
公开(公告)号：US09034790B2
公开(公告)日：2015-05-19
申请号：US13803824
申请日：2013-03-14
申请人： Fadi Selim Chakar , Mark Robert Fisher
发明人： Fadi Selim Chakar , Mark Robert Fisher
IPC分类号： B41M5/327 , B41M5/333 , B41M5/337
CPC分类号： B41M5/3275 , B41M5/3333 , B41M5/3336 , B41M5/3375 , B41M2205/04
摘要： The invention describes a thermally-responsive record material substantially free of aromatic isocyanate. The record material comprises a support having provided thereon a heat-sensitive composition comprising a substantially colorless dye precursor comprising a fluoran; and a developer material selected from the group consisting of 4,4′-diaminodiphenylsulfone and 3,3′-diaminodiphenylsulfone, which upon being heated react with said dye precursor to develop color, and including a binder material. Optionally, a modifier compound is included in the heat-sensitive composition. The modifier compound can be selected from the group consisting of a fatty acid amide, preferably a saturated fatty acid amide such as an alkyl amide, a bis methylene alkyl amide, or a bis ethylene alkyl amide, or any of 1,2-diphenoxy ethane, dimethyl diphenoxy ethane, and dimethyl phthalate.
摘要翻译：本发明描述了基本上不含芳族异氰酸酯的热响应性记录材料。记录材料包括其上提供有热敏组合物的载体，所述组合物包含基本上无色的包含荧烷的染料前体; 以及选自4,4'-二氨基二苯基砜和3,3'-二氨基二苯基砜的显影剂材料，其在被加热时与所述染料前体反应显色，并且包括粘合剂材料。任选地，在热敏组合物中包括改性剂化合物。改性化合物可以选自脂肪酸酰胺，优选饱和脂肪酸酰胺如烷基酰胺，双亚甲基烷基酰胺或双亚乙基烷基酰胺，或任何1,2-二苯氧基乙烷，二甲基二苯氧基乙烷和邻苯二甲酸二甲酯。

8. 发明授权

US08796381B2 Encapsulated cure systems 有权
标题翻译：封装治疗系统
公开(公告)号：US08796381B2
公开(公告)日：2014-08-05
申请号：US13235357
申请日：2011-09-17
申请人： Todd Arlin Schwantes , Michael Curley Krzoska , Gregory Stephen Kulibert , Adam Gregg Malofsky , Bernard Miles Malofsky , Nagib Maurice Ward
发明人： Todd Arlin Schwantes , Michael Curley Krzoska , Gregory Stephen Kulibert , Adam Gregg Malofsky , Bernard Miles Malofsky , Nagib Maurice Ward
IPC分类号： C09J129/04 , C08L79/04 , B32B15/02 , C08J3/24 , B01J13/02
CPC分类号： C08J3/241 , B01J13/02 , C08J3/24 , Y10T428/14 , Y10T428/1405 , Y10T428/24 , Y10T428/24008 , Y10T428/254 , Y10T428/2984 , Y10T428/2985 , Y10T428/2987 , Y10T428/2989 , Y10T428/31681
摘要： Encapsulated cure systems are provided wherein a curative is incorporated into a solid or semi-solid carrier material whereby mere fracturing or failure of the capsule wall encapsulating such cure systems will not provide for or allow sufficient release of the curative. Also provided are adhesive systems incorporating said encapsulated cure systems.
摘要翻译：提供了封装的固化体系，其中将固化剂掺入固体或半固体载体材料中，从而仅封装这种固化体系的胶囊壁的压裂或破坏将不能提供或允许固化剂的充分释放。还提供了包含所述封装的固化体系的粘合剂体系。

9. 发明授权

US08715544B2 Hydrophilic liquid encapsulates 有权
标题翻译：亲水液体封装
公开(公告)号：US08715544B2
公开(公告)日：2014-05-06
申请号：US12973175
申请日：2010-12-20
申请人： Todd Arlin Schwantes
发明人： Todd Arlin Schwantes
IPC分类号： B01J13/18 , B01J13/02 , B32B5/16
CPC分类号： B01J13/14
摘要： A process of forming a population of microcapsules is described comprising a liquid hydrophilic core material and a wall material at least partially surrounding the core material. The liquid hydrophilic core material can be anionic, cationic, or neutral but polar. The microcapsule population is formed by providing liquid hydrophilic core material; providing an oil continuous phase which is low boiling and preferably nonflammable, the oil continuous phase comprising preferably one or more organic oil materials such as esters with chain length up to about 42 carbons. A mixture is formed by dispersing the liquid hydrophilic material in the oil continuous phase. Either an oil soluble or dispersible monofunctional amine acrylate or monofunctional amine methacrylate, along with acid; or alternatively monofunctional acid acrylate or monofunctional acid methacrylate along with base; or alternatively, monofunctional amine acrylate or monofunctional amine methacrylate along with acid acrylate or methacrylate; is added. A multifunctional acrylate or methacrylate monomer or oligomer is provided along with an initiator. Optionally a surfactant is also added to form the mixture. Emulsification is achieved by subjecting the mixture to high shear agitation and heating the mixture for a time sufficient to enable forming a prepolymer which migrates to the liquid hydrophilic material, thereby forming prepolymers adhered to the hydrophilic core materials. Heating is carried out or light exposure or both for a time and temperature sufficient to crosslink the prepolymers.
摘要翻译：描述了形成微胶囊群的方法，其包括至少部分地围绕芯材料的液体亲水芯材料和壁材料。液体亲水芯材料可以是阴离子，阳离子或中性但极性。通过提供液体亲水芯材料形成微胶囊群; 提供低沸点且优选不易燃的油连续相，油连续相优选包含一种或多种有机油材料，例如链长高达约42个碳的酯。通过将液体亲水材料分散在油连续相中形成混合物。油溶性或分散性单官能胺丙烯酸酯或单官能胺甲基丙烯酸酯，以及酸; 或者单官能酸式丙烯酸酯或单官能酸式甲基丙烯酸酯与碱; 或者单官能胺丙烯酸酯或单官能胺甲基丙烯酸酯与酸性丙烯酸酯或甲基丙烯酸酯; 被添加。与引发剂一起提供多官能丙烯酸酯或甲基丙烯酸酯单体或低聚物。任选地，还加入表面活性剂以形成混合物。通过使混合物经受高剪切搅拌并将混合物加热足以使形成迁移到液体亲水材料的预聚物，从而形成粘附到亲水芯材料上的预聚物来实现乳化。进行加热或曝光或两者都足以使预聚物交联的时间和温度。

10. 发明授权

US11292280B2 Printable and scuff resistant silicone release coating for linerless thermally-responsive record material 有权
公开(公告)号：US11292280B2
公开(公告)日：2022-04-05
申请号：US15855608
申请日：2017-12-27
申请人： APPVION, INC.
发明人： Mark Fisher , Yves Defrenne , Lei Xu
IPC分类号： B41M5/40 , C09D7/61 , C09D183/04 , B41M5/44 , C08G77/20 , B41M5/42
摘要： The present invention is directed to a composition and method of providing a silicone release coating material for a thermally-responsive record material while maintaining strong printability with UV inks and water based inks, as well as scuff resistance. The thermally-responsive record material includes a substrate with first and second surfaces. The first surface includes a heat sensitive coating having a colorless dye precursor and an acidic developer material in contiguous relationship. The release coating is provided with an aqueous mixture of a water soluble or water dispersible polymeric material, a silicone release agent, an excess of platinum catalyst, and a hydrophilic silica. The platinum catalyst is preferably provided in excess of 150 ppm. The hydrophilic silica is preferably fumed silica. The release coating is cured at a temperature of 160° C. or less, or even from 70° C. to 120° C.

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