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81. 发明授权

US5580660A Use of a binder composition for the preparation of a powder coating for use as a top coat in the automotive industry and top-coated automotive substrates 失效
标题翻译：使用粘合剂组合物来制备粉末涂料，用作汽车工业中的顶涂层和顶涂汽车基材
公开(公告)号：US5580660A
公开(公告)日：1996-12-03
申请号：US335884
申请日：1995-02-21
申请人： Franciscus M. Witte , Gerrit Kieft , Wilhelmus H. H. A. Van Den Elshout
发明人： Franciscus M. Witte , Gerrit Kieft , Wilhelmus H. H. A. Van Den Elshout
IPC分类号： C08G18/42 , C08G18/62 , C08G18/79 , C08G18/80 , B23B27/06
CPC分类号： C08G18/807 , C08G18/42 , C08G18/4219 , C08G18/6229 , C08G18/792 , C08G18/808 , C08G2150/20 , Y10T428/31547 , Y10T428/31551 , Y10T428/31605
摘要： The invention relates to a binder composition for powder coatings for use as a topcoat in the automotive industry. The invention also relates to top-coated automotive substrates. The binder composition includes a polyester containing hydroxyl groups and a polyacrylate containing hydroxyl groups and a blocked hexamethylenediisocyanate trimer. The polyester has a hydroxyl number of between 20 and 100 mg KOH/g resin and an acid number of less than 10 mg KOH/g resin and the polyacrylate has a hydroxyl number of between 40 and 150 mg KOH/g resin and an acid number of less than 20 mg KOH/g resin. The trimer is blocked with 1,2,4-triazole.
摘要翻译： PCT No.PCT / NL93 / 00097 Sec。 371日期1995年2月21日 102（e）日期1995年2月21日PCT提交1993年5月12日PCT公布。第WO93 / 23447号公报日本公开日1993年11月25日本发明涉及一种用于汽车工业用作面漆的粉末涂料用粘合剂组合物。本发明还涉及顶涂汽车基材。粘合剂组合物包括含羟基的聚酯和含羟基的聚丙烯酸酯和封端的六亚甲基二异氰酸酯三聚物。聚酯的羟值为20〜100mg KOH / g树脂，酸值小于10mg KOH / g树脂，聚丙烯酸酯的羟值为40〜150mg KOH / g树脂和酸值小于20mg KOH / g树脂。三聚体用1,2,4-三唑封闭。

82. 发明授权

US5508337A Powder coating compositions, a process for their preparation, and their use for the coating of heat resistant substrates 失效
标题翻译：粉末涂料组合物，其制备方法及其用于涂覆耐热基材的用途
公开(公告)号：US5508337A
公开(公告)日：1996-04-16
申请号：US238563
申请日：1994-05-05
申请人： Christian Wamprecht , Reinhard Halpaap , Hans-Ulrich Meier-Westhues , Wolfgang Schultz
发明人： Christian Wamprecht , Reinhard Halpaap , Hans-Ulrich Meier-Westhues , Wolfgang Schultz
IPC分类号： C08G18/40 , C08G18/78 , C08G18/79 , C08G18/80 , C09D5/46 , C08J3/00 , C08F8/30 , C08K3/20 , C08L75/00
CPC分类号： C08G18/7831 , C08G18/4063 , C08G18/792 , C08G18/8077 , C08G2150/20 , Y10T428/31551
摘要： The present invention relates to a powder coating composition having a glass transition temperature of 20.degree. to 80.degree. C. and containing(A) 56 to 86.9% by weight of a polyacrylate polyol component having a hydroxyl number of 30 to 155 and a glass transition temperature of 30.degree. to 120.degree. C.,(B) 0.1 to 9% by weight of a polyester polyol component having a hydroxyl number of 40 to 180 and a glass transition temperature of -40.degree. to 80.degree. C.,(C) 13 to 35% by weight of a polyisocyanate component having a glass transition temperature of -40.degree. to 60.degree. C. and containing at least one ketoxime-blocked polyisocyanate selected from (i) polyisocyanate derivatives prepared from 1,6-diisocyanatohexane and containing biuret, isocyanurate, uretdione, and/or urethane groups, (ii) polyisocyanate derivatives prepared from mixtures of 1,6-diisocyanatohexane and 1-isocyanato-3,3,5-trimethyl-5-isocyanatomethylcyclohexane and containing isocyanurate groups and optionally uretdione groups and (iii) polyisocyanate derivatives prepared from 4,4'-diisocyanato-dicyclohexylmethane and containing urethane groups, and(D) at least one catalyst for the reaction between blocked isocyanate groups and hydroxyl groups,wherein i) the percentages of components (A), (B), and (C) are based on the total weight of these components and ii) components (A), (B), and (C) are present in amounts sufficient to provide an equivalent ratio of blocked isocyanate groups to hydroxyl groups of 0.5:1 to 1.5:1.The present invention is also relates to a process for the preparation of this powder coating composition and to heat-resistant substrates, particularly automotive body parts, coated with this powder coating composition.
摘要翻译：本发明涉及玻璃化转变温度为20〜80℃，含有（A）56〜86.9重量％的羟基数为30〜155的聚丙烯酸酯多元醇成分和玻璃化转变温度的粉末涂料组合物温度为30〜120℃，（B）0.1〜9重量％的羟值为40〜180，玻璃化转变温度为-40〜80℃的聚酯多元醇成分，（C） 13至35重量％的玻璃化转变温度为-40至60℃的多异氰酸酯组分，并含有至少一种酮肟封闭的多异氰酸酯，其选自（i）由1,6-二异氰酸根合己烷制备并含有缩二脲，异氰脲酸酯，脲二酮和/或氨基甲酸酯基团，（ii）由1,6-二异氰酸根合己烷和1-异氰酸根合-3,3,5-三甲基-5-异氰酸甲酯基环己烷的混合物制备并含有异氰脲酸酯基团和任选的脲二酮基团的多异氰酸酯衍生物，（iii ）由4,4'-二异氰酸根合二环己基甲烷制备并含有氨基甲酸酯基团的多异氰酸酯衍生物，和（D）至少一种用于封端异氰酸酯基和羟基之间反应的催化剂，其中i）组分（A），（B ）和（C）基于这些组分的总重量，和ii）组分（A），（B）和（C）以足以提供封端异氰酸酯基与羟基的当量比为0.5的量存在：1〜1.5：1。本发明还涉及这种粉末涂料组合物的制备方法以及涂覆有该粉末涂料组合物的耐热基材，特别是汽车车身部件。

83. 发明授权

US5470912A Polymeric powder coating compositions comprising low molecular weight polyethylene polyols 失效
标题翻译：包含低分子量聚乙烯多元醇的聚合物粉末涂料组合物
公开(公告)号：US5470912A
公开(公告)日：1995-11-28
申请号：US94733
申请日：1993-07-22
申请人： Doanld F. Loar
发明人： Doanld F. Loar
IPC分类号： C08G18/68 , C09D167/06 , C09D175/04 , C09D175/14 , C08L33/08 , C08L23/04
CPC分类号： C09D175/04 , C08G18/68 , C09D167/06 , C09D175/14 , C08G2150/20 , Y10S524/904 , Y10S525/934
摘要： Polymeric powder coating compositions featuring improved physical properties including improved impact strength, improved adhesivity and other properties is provided by a polymeric powder coating composition which comprises: (a) polymeric powder coating resin, (b) at least one low molecular weight ethylene copolymer having a degree of saponification of at least 25%, (c) a further constituent selected from the group consisting of catalyzing agents, flow control agents, coloring agents, fillers, processing aids, wherein the weight ratio of (b) to (a) is preferably in the range of 0.01%-20% to 99.99%-80%. The powder coating composition may be applied to articles using conventional techniques. Processes for producing the polymeric powder coating compostiions, and articles comprising the same are also disclosed.
摘要翻译：通过聚合物粉末涂料组合物提供具有改进的物理性能，包括改进的冲击强度，改善的粘合性和其它性能的聚合物粉末涂料组合物，其包含：（a）聚合物粉末涂料树脂，（b）至少一种低分子量乙烯共聚物，其具有皂化度至少为25％，（c）选自催化剂，流动控制剂，着色剂，填料，加工助剂的另一组分，其中（b）至（a）的重量比优选为在0.01％-20％至99.99％-80％的范围内。粉末涂料组合物可以使用常规技术施用于制品。还公开了用于生产聚合物粉末涂料组合物的方法和包含其的制品。

84. 发明授权

US5310848A Resin composition for powder coating 失效
标题翻译：粉末涂料用树脂组合物
公开(公告)号：US5310848A
公开(公告)日：1994-05-10
申请号：US10763
申请日：1993-01-29
申请人： Tokuzo Nozaki , Katsuyoshi Atsumi , Makiko Sakai
发明人： Tokuzo Nozaki , Katsuyoshi Atsumi , Makiko Sakai
IPC分类号： C09D5/03 , C08G18/42 , C08G18/79 , C09D5/46 , C09D167/00 , C09D175/06 , C08G18/30 , C08G18/80
CPC分类号： C08G18/798 , C08G18/4202 , C09D167/00 , C08G2150/20
摘要： a resin composition for a powder coating comprising a polyester A, which does not substantially set to gel and has a hydroxyl value of at least 1,200 g eq/10.sup.6 g, a polyester B, which does not substantially set to gel and has a hydroxyl value of from 200 to 1,000 g eq/10.sup.6 g, and an inner blocked isocyanate hardener, wherein the weight ratio of polyester A to polyester B is from 70:30 to 10:90 and the difference (absolute value) in gel time between these polyesters A and B is at least 3 minutes.
摘要翻译：用于粉末涂料的树脂组合物，其包含基本上不凝胶并且羟基值至少为1200g eq / 106g的聚酯A，基本上不凝胶化并具有羟值的聚酯B 为200〜1000g eq / 106g，和内封端异氰酸酯硬化剂，其中聚酯A与聚酯B的重量比为70:30至10:90，并且这些聚酯之间的凝胶时间差（绝对值） A和B至少3分钟。

85. 发明授权

US5252670A Powder coating material and a recoat steel plate 失效
标题翻译：粉末涂料和重涂钢板
公开(公告)号：US5252670A
公开(公告)日：1993-10-12
申请号：US974770
申请日：1992-11-12
申请人： Chiaki Sagawa , Eiji Shimada , Shingo Okamoto
发明人： Chiaki Sagawa , Eiji Shimada , Shingo Okamoto
IPC分类号： C08G18/08 , C08G18/16 , C08G18/24 , C08G18/42 , C08G18/80 , C09D5/46
CPC分类号： C08G18/42 , C08G18/089 , C08G18/161 , C08G18/24 , C08G18/8061 , C08G2150/20 , Y10T428/31605
摘要： A powder coating composition comprises 100 weight parts of the total of a polyester resin having a hydroxyl value in the range from 20 to 100 KOH mg/g and a blocked polyisocyanate compound, 0.01 to 3 weight parts of an organotin compound and 0.01 to 10 weight parts of a carboxylic acid compound having an acid value of 1000 KOH mg/g or less which can form a complex compound by reaction with the organotin compound. The amount of the polyester resin is in the range from 95 to 50 weight % and the amount of the blocked polyisocyanate compound is in the range from 5 to 50 weight % respectively based on the total of the polyester resin and the blocked polyisocyanate compound. A precoat steel plate is prepared by coating the powder coating composition described above on a steel plate by a electrostatic powder coating method to form a coating layer having a thickness in the range from 20 to 120 .mu.m and curing the coating composition by baking at a temperature in the range from 190.degree. to 300.degree. C. for a time in the range from 20 seconds to 10 minutes. The powder coating composition can be cured without formation of blisters and pin holes under a desired condition by controlling the rate of the curing reaction.

86. 发明授权

US5130404A Castable thermosetting polyurethane polymer having improved heat stability 失效
标题翻译：具有改善的热稳定性的可浇注热固性聚氨酯聚合物
公开(公告)号：US5130404A
公开(公告)日：1992-07-14
申请号：US710114
申请日：1991-06-04
申请人： Gerard S. Freeland
发明人： Gerard S. Freeland
IPC分类号： C08G18/08 , C08G18/48 , C08G18/66 , C08G18/76
CPC分类号： C08G18/4883 , C08G18/0885 , C08G18/4804 , C08G18/4812 , C08G18/6677 , C08G18/7664 , C08G2120/00 , C08G2150/20
摘要： A castable thermosetting polyurethane polymer, having improved heat-stability characteristics, comprising (A) a polymeric methylene diisocyanate, (B) a propyleneoxide-extended polyol which is preferably a sugar-based polyol, (C) a polyether diol or triol, and (D) dipropylene glycol or diethylene glycol, in amounts respectively between about 35-45 parts by weight, 35-45 parts by weight, and 12-20 parts by weight, per 100 parts by weight of total diol and triol (resin) components, providing an NCO/OH ratio between about 1:1 and about 1.2:1, an effective polyurethane-catalyzing amount of (E) a urethane catalyst, and optionally comprising an effective amount of a drying agent, is disclosed. The cast polyurethane polymer of the invention withstands temperatures of 450.degree. F. (232.degree. C.) for 20 minutes without visual polymer degradation, whereas most other castable polyurethane systems degrade between 350.degree. F. and 375.degree. F., as a result of which heat-stability the polymer of the present invention is especially suitable for post finishing which involves the employment of higher temperatures, such as painting with thermosetting coatings, powder coating, and anodizing.
摘要翻译：具有改进的热稳定性特征的可浇铸的热固性聚氨酯聚合物包括（A）聚合亚甲基二异氰酸酯，（B）优选为糖基多元醇的环氧丙烷延长多元醇，（C）聚醚二醇或三醇，和 D）二丙二醇或二甘醇，每100重量份总二醇和三醇（树脂）组分分别为约35-45重量份，35-45重量份和12-20重量份，提供约1：1至约1.2：1的NCO / OH比，有效的聚氨酯催化量的（E）氨基甲酸酯催化剂，并任选地包含有效量的干燥剂。本发明的铸塑聚氨酯聚合物在450°F（232℃）的温度下保持20分钟，而没有视觉聚合物降解，而大多数其它浇注聚氨酯体系在350°F和375°F之间降解，结果是本发明的聚合物的热稳定性特别适用于涉及使用更高温度的后整理的热稳定性，例如用热固性涂料进行涂漆，粉末涂料和阳极氧化。

87. 发明授权

US4975513A Process for preparing hydroxyl polyester for use in a powder coating and a powder coating composition thereof 失效
标题翻译：制备用于粉末涂料的羟基聚酯及其粉末涂料组合物的方法
公开(公告)号：US4975513A
公开(公告)日：1990-12-04
申请号：US291613
申请日：1988-12-29
申请人： Bong J. Kim , Won S. Kim
发明人： Bong J. Kim , Won S. Kim
IPC分类号： C08G63/78 , C08G18/42 , C08G18/80 , C08G63/20 , C09D5/46 , C09D167/04
CPC分类号： C08G18/4219 , C08G18/8074 , C08G63/20 , C09D175/06 , C08G2150/20 , C08G2250/00
摘要： A crystalline polyester resin derived from the reaction between a prepolymer and trimellitic anhydride in an amount of less than 10 wt % of the prepolymer where prepolymer as an intermediate product formed from the reaction between an alcohol mixture containing at least 40 mole % ethylene glycol and at least 30 mol % neopentyl glycol, and an acid mixture containing terephthalic acid or dimethyl terephthalate of at least 40 mole % and a linear dicarboxylic acid, or between an alcohol mixture containing 100 wt % terephthalic acid or dimethyl terephthalate. The crystalline polyester resin is very suitable for use in powder coating compositions and has a hyodroxyl number of 20 to 100, an average molecular weight of 1000 to 3500 and a melt viscosity at 160.degree. C. of 500 to 4000 cps as well as the characteristics of dense, regular, and repetitive structure.
摘要翻译：衍生自预聚物和偏苯三酸酐之间的反应的结晶聚酯树脂，其量小于其中预聚物作为中间产物的预聚物的量小于10重量％，所述预聚物是由含有至少40摩尔％乙二醇的醇混合物和至少30摩尔％的新戊二醇，以及含有至少40摩尔％的对苯二甲酸或对苯二甲酸二甲酯和线性二羧酸的酸混合物，或含有100重量％对苯二甲酸或对苯二甲酸二甲酯的醇混合物。结晶性聚酯树脂非常适用于粉末涂料组合物，其羟基数为20〜100，平均分子量为1000〜3500，在160℃下的熔体粘度为500〜4000cps，特性密集，规则和重复的结构。

88. 发明授权

US4973646A Powder coating compositions 失效
标题翻译：粉末涂料组合物
公开(公告)号：US4973646A
公开(公告)日：1990-11-27
申请号：US506055
申请日：1990-04-09
申请人： Jonathan S. Witzeman , Yeong-Ho Chang
发明人： Jonathan S. Witzeman , Yeong-Ho Chang
IPC分类号： C08G18/48 , C08G18/42 , C08G18/76 , C08G18/80 , C09D5/03 , C09D5/46 , C09D167/02 , C09D175/00 , C09D175/06
CPC分类号： C09D167/02 , C08G18/4202 , C08G18/4213 , C08G18/423 , C08G18/765 , C08G18/8074 , C09D175/06 , C08G2150/20 , C08G2250/00 , Y10T428/31551 , Y10T428/31616 , Y10T428/31681 , Y10T428/31786
摘要： Disclosed are thermosetting, powder coating compositions comprised of semi-crystalline polyesters and .epsilon.-caprolactam-blocked bis(1-cyanato-1-methylethyl) benzene compounds which are readily curable at relatively-mild temperatures and using cure times commonly used to cure (cross-link) powder coatings. When using equivalent curing conditions, the disclosed coating compositions exhibit a higher degree of cross-linking than do combinations of amorphous polyesters and the .epsilon.-caprolactam-blocked bis(1-cyanato-1-methylethyl)-benzene compounds.
摘要翻译：公开了由半结晶聚酯和ε-己内酰胺封闭的双（1-氰基-1-甲基乙基）苯化合物组成的热固性粉末涂料组合物，其在相对温和的温度下容易固化并且使用通常用于固化的固化时间 -link）粉末涂料。当使用相同的固化条件时，所公开的涂料组合物表现出比无定形聚酯和ε-己内酰胺封端的双（1-氰基-1-甲基乙基） - 苯化合物的组合更高程度的交联。

89. 发明授权

US4937288A Powder coating composition 失效
标题翻译：粉末涂料组合物
公开(公告)号：US4937288A
公开(公告)日：1990-06-26
申请号：US408420
申请日：1989-09-18
申请人： Paul H. Pettit, Jr. , Debra L. Singer , Marvin L. Kaufman
发明人： Paul H. Pettit, Jr. , Debra L. Singer , Marvin L. Kaufman
IPC分类号： C08F8/30 , C08F8/46 , C08G18/83 , C08K5/20 , C08L67/00 , C08L73/02 , C08L81/02 , C09D5/46 , C09D133/06 , C09D133/12
CPC分类号： C09D133/12 , C08F8/30 , C08F8/46 , C08G18/833 , C08K5/20 , C09D133/064 , C08G2150/20 , C08L2205/02 , C08L67/00 , C08L73/02 , C08L81/02 , Y10S525/934
摘要： A thermosetting powder coating composition which has good handling properties and which has a good blend of physical properties such as appearance, flexibility, hardness, solvent resistance, corrosion resistance and exterior durability is disclosed. The composition comprises a co-reactable particulate mixture of a carboxylic acid group-containing acrylic polymer, a second carboxylic acid group-containing material having sufficient crystallinity to assist in flow of the powder coating compositions and a beta-hydroxalkylamide crosslinking agent.
摘要翻译：公开了一种热处理粉末涂料组合物，其具有良好的操作性能，并且具有良好的物理性能如外观，柔韧性，硬度，耐溶剂性，耐腐蚀性和外部耐久性的共混物。该组合物包含含羧酸基的丙烯酸聚合物的共可反应颗粒混合物，具有足够结晶度的第二含羧酸基团的材料以有助于粉末涂料组合物的流动和β-羟烷基酰胺交联剂。

90. 发明授权

US4920008A Powder coating compositions 失效
公开(公告)号：US4920008A
公开(公告)日：1990-04-24
申请号：US325847
申请日：1989-03-20
申请人： Robert B. Barbee
发明人： Robert B. Barbee
IPC分类号： C08G18/42 , C08G18/80 , C09D5/03 , C09D5/46 , C09D167/00 , C09D175/06
CPC分类号： C08G18/4252 , C08G18/4202 , C08G18/8074 , C08G2150/20 , Y10T428/31681
摘要： Disclosed are thermosetting, powder coating compositions comprised of blends of certain amorphous polyesters and polyether-esters in combination with a blocked polyisocyanate which, when applied to a substrate and heated, provide cross-linked coatings having a combination of desirable properties including good gloss, impact strength and flexibility.

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