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81. 发明授权

US4298753A Continuous process for preparing silanes and siloxanes having SiOC groups 失效
标题翻译：制备具有SiOC基团的硅烷和硅氧烷的连续工艺
公开(公告)号：US4298753A
公开(公告)日：1981-11-03
申请号：US209447
申请日：1980-11-24
申请人： Anton Schinabeck , Norbert Zeller , Tassilo Lindner , Georg Engelsberger , Rudolf Riedle
发明人： Anton Schinabeck , Norbert Zeller , Tassilo Lindner , Georg Engelsberger , Rudolf Riedle
IPC分类号： C08G77/00 , C07F7/18 , C08G77/06 , C08G77/22 , C07F7/04 , C07F7/10
CPC分类号： C07F7/188 , C08G77/06
摘要： A continuous process for preparing silanes and siloxanes having SiOC groups which comprises (a) introducing in a liquid phase a chlorosilane and a hydroxyl-containing aliphatic compound in parallel flow into a first stage of a first reactor in an amount such that from 0.5 to 0.9 gram-mole of hydroxyl group is present per gram-atom of Si-bonded chlorine; (b) removing the liquid reaction mixture from the first reactor; (c) introducing the reaction mixture at the head of a column used as the second reactor which is maintained at an elevated temperature; (d) adding a hydroxyl-containing aliphatic compound as a gas at the lower end of the column or at a point between the lower end and the upper end of the lower one-third of the column, in an amount at least sufficient to completely react with the Si-bonded chlorine present in the reaction mixture obtained from the first stage and (e) removing the silane containing SiOC groups or polysiloxane containing SiOC groups from the column at a point below the point of addition of the hydroxyl-containing aliphatic compound.
摘要翻译：一种用于制备具有SiOC基团的硅烷和硅氧烷的连续方法，其包括（a）以液相方式将氯硅烷和含羟基的脂族化合物平行流入第一反应器的第一阶段，其量使得为0.5至0.9 每克原子的硅键合氯存在克分子的羟基; （b）从第一反应器中除去液体反应混合物; （c）将反应混合物引入用作第二反应器的柱头，保持在升高的温度; （d）在柱的下端或在塔的下三分之一的下端和上端之间的点处加入含羟基的脂族化合物作为气体，其量至少足以完全与从第一阶段获得的反应混合物中存在的Si键合的氯反应，和（e）在含羟基的脂族化合物的加入点以下的点从塔中除去含有SiOC基团的含硅烷的硅烷或聚硅氧烷。

82. 发明授权

US4134906A Silylhydrocarbyl phosphine transition metal complexes 失效
公开(公告)号：US4134906A
公开(公告)日：1979-01-16
申请号：US829898
申请日：1977-09-01
申请人： Alexis A. Oswald , Lawrence L. Murrell
发明人： Alexis A. Oswald , Lawrence L. Murrell
IPC分类号： C07C67/36 , B01J31/00 , B01J31/16 , B01J31/20 , B01J31/22 , B01J31/24 , C07B61/00 , C07C1/00 , C07C5/03 , C07C45/00 , C07C45/50 , C07C51/12 , C07C67/00 , C07F7/14 , C07F7/18 , C07F9/02 , C07F13/00 , C07F15/00 , C08F4/16
CPC分类号： C07F9/02 , B01J31/1633 , B01J31/20 , B01J31/24 , B01J31/2404 , C07C5/03 , C07C51/12 , C07F7/14 , C07F7/182 , C07F7/1868 , C07F7/1876 , C07F7/188 , C07F7/1892 , B01J2231/645 , B01J2531/822 , B01J2531/824 , B01J2531/845 , C07C2531/24
摘要： Novel heterogeneous silylhydrocarbyl phosphine transition metal complex catalysts and intermediates therefor are prepared by (a) the selective monoaddition of silane having chlorine, alkoxy or acyloxy groups to an .alpha.,.omega.-diene, (b) followed by the addition of a phosphine to the resulting .omega.-alkenyl silanes to form the corresponding silylalkyl phosphines, (c) which are then covalently anchored as such or in the form of their transition metal complexes via condensation of their reactive silane substituents with hydroxy groups of silica and metal oxides, (d) optionally followed by complexing the free phosphine groups of anchored silylalkyl phosphines with transition metal compounds.

83. 发明授权

US4088669A Method for preparing organosilicon compounds from elemental silicon and hydrocarbon ethers 失效
标题翻译：从元素硅和烃醚制备有机硅化合物的方法
公开(公告)号：US4088669A
公开(公告)日：1978-05-09
申请号：US785882
申请日：1977-04-08
申请人： James R. Malek , John L. Speier , Antony P. Wright
发明人： James R. Malek , John L. Speier , Antony P. Wright
IPC分类号： B01J27/00 , B01J31/00 , C07B61/00 , C07F7/08 , C07F7/18
CPC分类号： C07F7/188 , C07F7/0874
摘要： Organosilicon compounds bearing silicon-bonded hydrocarbon radicals and silicon-bonded hydrocarbonoxy radicals are obtained by contacting activated silicon, a hydrocarbon ether and a halogen-containing catalyst in a closed system at elevated temperature. Silanes and siloxanes, particularly methylmethoxysilanes, may be prepared and used to prepare valuable silicone materials.
摘要翻译：通过在高温下将封闭体系中的活化硅，烃醚和含卤素的催化剂接触，得到带有硅键合的烃基和与硅键合的烃氧基的有机硅化合物。可以制备硅烷和硅氧烷，特别是甲基甲氧基硅烷，并用于制备有价值的硅氧烷材料。

84. 发明授权

US3697568A Iminoxyorganosilanes 失效
标题翻译：氨基氧杂环己烷
公开(公告)号：US3697568A
公开(公告)日：1972-10-10
申请号：US3697568D
申请日：1970-11-12
申请人： RHONE POULENC SA
发明人： BOISSIERAS JEAN , CEYZERIAT LOUIS , POY GUY
IPC分类号： C08L83/00 , C07F7/08 , C07F7/18 , C08G77/00 , C08G77/28 , C08L83/04 , C09D183/04 , C09J11/00
CPC分类号： C07F7/188 , C07F7/0892 , C08L83/04 , Y10S528/901 , C08L2666/44
摘要： Silanes R-Si Ya Q3 a where R is unsubstituted or halo, alkoxy or nitrile substituted hydrocarbon radical, one of Y and Q is ON CR''R'''' and the other is O(DO)nR'''''', a a number from 0.1 to 2.9, where R'' is a hydrocarbon radical, R'''' is H or C1 5 alkyl, or R'' and R'''' together are divalent hydrocarbon radicals, R'''''' is C1 4 aliphatic hydrocarbon radical, D is C1 8 alkylene radical and n O, 1, 2 or 3; are prepared by reacting RSiEaQ3 a with YH where E is halogen or acyloxy. They may be used particularly as cross-linking agents for polydiorganosiloxanes having reactive terminal groups on the chain to give elastomer forming compositions which are storage stable in the absence of water and which cure to form elastomers in the presence of water at about 20* C.

85. 发明授权

US3525764A Production of halogenated phenoxysilanes 失效
标题翻译：生产羟基苯甲酸酯
公开(公告)号：US3525764A
公开(公告)日：1970-08-25
申请号：US3525764D
申请日：1968-01-08
申请人： DYNAMIT NOBEL AG
发明人： KOTZSCH HANS-JOACHIM , ISMAIL ROSHDY
IPC分类号： B27K3/40 , C07F7/04 , C07F7/08 , C07F7/12 , C07F7/18 , D06M13/513 , D06M15/643 , C07F7/06
CPC分类号： C07F7/0896 , C07F7/045 , C07F7/0834 , C07F7/12 , C07F7/1804 , C07F7/188 , D06M13/513 , D06M15/6436

86. 发明授权

US3458553A Process for the production of aminoalkyl silicon compounds 失效
标题翻译：生产氨基硅氧烷化合物的方法
公开(公告)号：US3458553A
公开(公告)日：1969-07-29
申请号：US43947765
申请日：1965-03-12
申请人： BAYER AG
发明人： NIEDERPRUM HANS , HORN ELMAR-MANFRED , SIMMLER WALTER
IPC分类号： C07C209/48 , C07F7/08 , C07F7/18 , C08G77/388 , F28D3/00 , C07F7/10
CPC分类号： C07F7/0889 , C07C209/48 , C07F7/0834 , C07F7/0874 , C07F7/188 , C08G77/388 , F28D3/00

87. 发明授权

US2831011A Method of reacting silanes with ethers 失效
标题翻译：硅烷与醚反应的方法
公开(公告)号：US2831011A
公开(公告)日：1958-04-15
申请号：US47711454
申请日：1954-12-22
申请人： DOW CORNING
发明人： SOMMER LEO H
IPC分类号： C07F7/08 , C07F7/18
CPC分类号： C07F7/188 , C07F7/0885

88. 发明授权

US2745860A Disproportionation of alkoxydisilyl hydrocarbons 失效
标题翻译：烷氧基二硅烷烃的歧化
公开(公告)号：US2745860A
公开(公告)日：1956-05-15
申请号：US31521152
申请日：1952-10-16
申请人： UNION CARBIDE & CARBON CORP
发明人： LEROY BAILEY DONALD
IPC分类号： C07F7/08 , C07F7/18
CPC分类号： C07F7/0896 , C07F7/188

89. 发明公开

US20240368201A1 SILANE HYDROLYZATE AND PROCESSES FOR THE PREPARATION AND USE THEREOF 审中-公开
公开(公告)号：US20240368201A1
公开(公告)日：2024-11-07
申请号：US18683346
申请日：2022-10-10
申请人： Dow Silicones Corporation , Dow Global Technologies LLC
发明人： Lorry Deklippel , Cindy Delvalle , Eric Joffre , Axel Kretschmer , Jeremy Marchand , Donald Eldred , Cheryl Roggenbuck , Xiaoyun Chen , Joe Nowell , Na Li , Giuseppina Lavinaro
IPC分类号： C07F7/18 , A61K8/58 , A61Q5/06
CPC分类号： C07F7/188 , A61K8/585 , A61Q5/06 , A61K2800/805
摘要： A carbamate anion/protonated amine-functional silane hydrolyzate is prepared by a process including combining alkoxysilanes, base catalyst and water to form a silane hydrolyzate, and thereafter combining the silane hydrolyzate with carbon dioxide. The resulting carbamate anion/protonated amine-functional silane hydrolyzate is suitable for use in hair care compositions.

90. 发明公开

US20240352050A1 PROCESS FOR MAKING CYANOETHYLTRIMETHOXYSILANE 审中-公开
公开(公告)号：US20240352050A1
公开(公告)日：2024-10-24
申请号：US18684217
申请日：2022-11-11
申请人： DOW SILICONES CORPORATION
发明人： Michael Depierro , Kitty Liu , Xiaoyuan Zhou , Reza Panah , Aaron Greiner
IPC分类号： C07F7/18 , C08K5/5475 , C09J183/04
CPC分类号： C07F7/188 , C09J183/04 , C08K5/5475
摘要： A process for preparing cyanoethyltrimethoxysilane is performed via transesterification of cyanoethyltriethoxysilane with methanol in the presence of a catalyst. The cyanoethyltrimethoxysilane is useful as an adhesion promoter, a coupling agent, or a crosslinker. The cyanoethyltrimethoxysilane may be formulated in a polyorganosiloxane sealant composition.

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