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81. 发明申请

US20060009655A1 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US20060009655A1
公开(公告)日：2006-01-12
申请号：US11221213
申请日：2005-09-07
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16 , B01J10/00
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

82. 发明授权

US06900346B2 Method for decomposition of michael type adduct 有权
标题翻译：迈克尔型加合物分解方法
公开(公告)号：US06900346B2
公开(公告)日：2005-05-31
申请号：US10183840
申请日：2002-06-27
申请人： Fumio Shibusawa , Naoki Serata , Kazuhiko Sakamoto
发明人： Fumio Shibusawa , Naoki Serata , Kazuhiko Sakamoto
IPC分类号： C07C51/377 , C07B61/00 , C07C51/09 , C07C51/50 , C07C57/04 , C07C57/065 , C07C67/327 , C07C69/52 , C07C51/42
CPC分类号： C07C51/50 , C07C51/09 , C07C67/327 , C07C57/04 , C07C69/54
摘要： A method for the decomposition of a Michael type adduct, characterized by causing a Michael type adduct to react in the presence of an N-oxyl compound thereby decomposing the Michael type adduct into acrylic acid and/or the acrylic ester and/or the alcohol and a method for the production of acrylic acid and/or the acrylic ester, characterized by comprising a step of recovering a Michael type adduct formed in the process for the production of acrylic acid or acrylic ester and a step of decomposing the recovered Michael type adduct by the method of decomposition mentioned above. This invention, therefore, allows promotion of efficient utilization of the raw materials.
摘要翻译：一种分解迈克尔型加合物的方法，其特征在于使迈克尔型加合物在N-氧基化合物存在下反应，从而将迈克尔型加合物分解成丙烯酸和/或丙烯酸酯和/或醇，和制备丙烯酸和/或丙烯酸酯的方法，其特征在于包括回收在制备丙烯酸或丙烯酸酯的方法中形成的迈克尔型加合物的步骤和通过以下步骤分解回收的迈克尔型加合物：上述分解方法。因此，本发明可以促进原料的有效利用。

83. 发明授权

US06899452B2 Apparatus and method for preparation and supply of polymerization inhibitor 有权
标题翻译：聚合抑制剂的制备和供给装置及方法
公开(公告)号：US06899452B2
公开(公告)日：2005-05-31
申请号：US10246361
申请日：2002-09-18
申请人： Kei Hamamoto , Takeshi Nishimura , Kazuhiko Sakamoto , Kunihiko Suzuki
发明人： Kei Hamamoto , Takeshi Nishimura , Kazuhiko Sakamoto , Kunihiko Suzuki
IPC分类号： B01F3/12 , B01F3/08 , B01F15/00 , B01F15/02 , B01F15/04 , B01J8/00 , B01J8/20 , B01J19/00 , B01J19/18 , C08F2/42
CPC分类号： B01J8/20 , B01F3/088 , B01F15/00123 , B01J8/0045 , B01J19/002 , B01J19/0066 , B01J19/18 , B01J2219/00182 , B01J2219/00272
摘要： An apparatus for the preparation and supply of a polymerization inhibitor which constantly effects stable supply of a polymerization inhibitor solution adjusted to a prescribed concentration and enables a compound handled at the next step to be prevented from polymerization is provided. The apparatus for the preparation and supply of a polymerization inhibitor has at least two tanks and a stirring device, a liquid level detector, a polymerization inhibitor input port, a concentration-adjusting liquid input port, and a polymerization inhibitor solution feed opening, each being installed in at least one of said tanks.
摘要翻译：提供了一种制备和供应聚合抑制剂的装置，其提供了恒定地稳定地供应调节到规定浓度的聚合抑制剂溶液并使下一步骤处理的化合物能够防止聚合。用于制备和供应阻聚剂的装置具有至少两个罐和搅拌装置，液位检测器，阻聚剂输入端口，浓度调节液体输入端口和阻聚剂溶液进料口，各自为安装在至少一个所述罐中。

84. 发明授权

US06599397B2 Method for preventing polymerization of (meth)acrylic acid and esters thereof and method for the production thereof 失效
标题翻译：防止（甲基）丙烯酸及其酯的聚合的方法及其制备方法
公开(公告)号：US06599397B2
公开(公告)日：2003-07-29
申请号：US09875541
申请日：2001-06-06
申请人： Kazuhiko Sakamoto , Tomohiro Nakae , Kazuo Okochi , Masahiro Uemura , Sei Nakahara
发明人： Kazuhiko Sakamoto , Tomohiro Nakae , Kazuo Okochi , Masahiro Uemura , Sei Nakahara
IPC分类号： B01D300
CPC分类号： C07C51/50 , C07C57/04
摘要： This method of preventing polymerization of methacrylic acid inn the process of its production is characterized by comprising using, in a refining column, a combination of N-nitrosophenylhydroxylamine or salt thereof with an N-oxyl compound, an N-hydroxy-,2,2,6,6-tetramethylpiperidine compound and a 2,2,6,6-tetramethylpiperidine compound. In this method, N-nitrosophenylhydroxylamine or a salt thereof rises inside a refining column under splitting part thereof to effectively inhibit polymerization of (meth)acrylic acid or the like. The above polymerization in both vapor and liquid phases can be inhibited more effectively by the combined use of the compounds mentioned above.
摘要翻译：这种防止甲基丙烯酸在其生产过程中聚合的方法的特征在于包括在精炼塔中使用N-亚硝基苯基羟胺或其盐与N-氧基化合物，N-羟基 - ，2,2' 6,6-四甲基哌啶化合物和2,2,6,6-四甲基哌啶化合物。在该方法中，N-亚硝基苯基羟胺或其盐在分解部分的内部在精炼塔内升高，有效抑制（甲基）丙烯酸等的聚合。通过上述化合物的组合使用，可以更有效地抑制气相和液相中的上述聚合。

85. 发明授权

US06568415B2 Storing device for easily polymerizable and coagulating liquid substance and method for pressure control thereof 有权
公开(公告)号：US06568415B2
公开(公告)日：2003-05-27
申请号：US09906255
申请日：2001-07-16
申请人： Kenji Nakahara , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato , Masakatsu Mori
发明人： Kenji Nakahara , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato , Masakatsu Mori
IPC分类号： F16K4900
CPC分类号： F16K49/00 , Y10T137/0318 , Y10T137/4606 , Y10T137/4643 , Y10T137/6253 , Y10T137/6579 , Y10T137/7771 , Y10T137/7779
摘要： A storing device is disclosed having a gas-sealing device and/or a heating device provided for a pipe connecting a storing tank for an easily polymerizable and/or coagulating liquid substance and a liquid sealing implement-protecting device. A method for the control of the pressure in the storing device is also disclosed. This invention contemplates protecting a storing device against deformation and fracture.

86. 发明授权

US06540881B1 Method for refining (meth)acrylic acid 有权
标题翻译：精制（甲基）丙烯酸的方法
公开(公告)号：US06540881B1
公开(公告)日：2003-04-01
申请号：US09532225
申请日：2000-03-22
申请人： Kazuhiko Sakamoto , Kouji Ueno , Sei Nakahara , Masatoshi Ueoka
发明人： Kazuhiko Sakamoto , Kouji Ueno , Sei Nakahara , Masatoshi Ueoka
IPC分类号： B01D342
CPC分类号： C07C51/44 , C07C51/23 , C07C51/252 , C07C51/50 , Y10S203/22 , C07C57/04
摘要： This invention relates to a method for preventing (meth)acrylic acid from polymerizing during the course of distillation. The method provides for refining (meth)acrylic acid by a procedure including the steps of feeding a mixed gas obtained by catalytic gas phase oxidation of propylene and/or acrolein with a molecular oxygen-containing gas or a mixed gas obtained by catalytic gas phase oxidation of at least one compound of isobutylene, t-butyl alcohol, or methacrolein with a molecular oxygen-containing gas, to a (meth)acrylic acid collection column, collecting a (meth)acrylic acid-containing solution from the mixed gas, and feeding the (meth)acrylic acid-containing solution to a distillation column while maintaining the total concentration of aldehydes of 2-4 carbon atoms and acetone in the solution at a level of not more than 2000 ppm based on the amount of (meth)acrylic acid.
摘要翻译：本发明涉及一种在蒸馏过程中防止（甲基）丙烯酸聚合的方法。该方法通过以下步骤提供（甲基）丙烯酸的精制，包括以下步骤：将通过丙烯和/或丙烯醛的催化气相氧化获得的混合气体与含分子氧的气体或通过催化气相氧化获得的混合气体的至少一种异丁烯，叔丁醇或甲基丙烯醛的化合物与含分子氧的气体反应到（甲基）丙烯酸收集塔，从混合气体中收集（甲基）丙烯酸的溶液，并进料（甲基）丙烯酸溶液，同时维持2-4个碳原子的醛和丙酮的总浓度在不超过2000ppm的水平下，基于（甲基）丙烯酸的量。

87. 发明授权

US06441228B2 Apparatus and process for producing (meth)acrylic acid 有权
公开(公告)号：US06441228B2
公开(公告)日：2002-08-27
申请号：US09735091
申请日：2000-12-12
申请人： Sei Nakahara , Kazuhiko Sakamoto , Yukihiro Matsumoto , Kenji Sanada , Masatoshi Ueoka
发明人： Sei Nakahara , Kazuhiko Sakamoto , Yukihiro Matsumoto , Kenji Sanada , Masatoshi Ueoka
IPC分类号： C07C5142
CPC分类号： C07C51/252 , B01D3/225 , B01D3/322 , B01J19/02 , B01J2219/00101 , B01J2219/0277 , C07C51/44 , Y10S159/15 , C07C57/04
摘要： The present invention provides an apparatus for producing (meth)acrylic acid and a process for producing (meth)acrylic acid with this apparatus wherein the apparatus enables to produce (meth)acrylic acid stably for a long period of time by effectively inhibiting the polymerization of (meth)acrylic acid in its production process (for example, in a reboiler). At least a part of the apparatus is made of a nickel-chromium-iron alloy with a molybdenum content of 3 to 20 mass %, but not including 3 mass %, or with a molybdenum content of 1 to 4 mass % and a copper content of 0.5 to 7 mass %.

88. 发明授权

US06414183B1 Method for handling waste oil 有权
标题翻译：处理废油的方法
公开(公告)号：US06414183B1
公开(公告)日：2002-07-02
申请号：US09543743
申请日：2000-04-05
申请人： Kazuhiko Sakamoto , Sei Nakahara , Masatoshi Ueoka
发明人： Kazuhiko Sakamoto , Sei Nakahara , Masatoshi Ueoka
IPC分类号： C07C6954
CPC分类号： C07C51/42 , C07C51/252 , C07C67/39 , C07C57/04 , C07C69/54
摘要： The present invention provides a method for stabilizing waste oil which is taken of each chemical apparatus of the manufacturing line of (meth)acryl acid and/or ester thereof, and treating the waste oil such as draining it out of the production apparatus, for example, a distillation tower from its bottom, sending and transporting it by a pump through a pipeline, and storing it in a storage tank in a simple manner while keeping the waste oil in a stable state. The waste oil can be stabilized by coexisting with solvent. The solvent used in the present invention is typically at least one selected from the group consisting of water, alcohol, ether, carboxylic acid, ketone, aromatic hydrocarbons, and aliphatic hydrocarbons.
摘要翻译：本发明提供了一种稳定废油的方法，该方法取自（甲基）丙烯酸和/或其酯的生产线的每个化学装置，并将废油例如从生产装置中排出，例如，蒸馏塔从底部通过泵送出并通过管道运输，并以简单的方式将其储存在储罐中，同时保持废油处于稳定状态。废油可以通过与溶剂共存而稳定。本发明中使用的溶剂通常为选自水，醇，醚，羧酸，酮，芳族烃和脂族烃中的至少一种。

89. 发明授权

US06340381B1 Method and apparatus for the preparation of clean gases 失效
标题翻译：清洁气体的制备方法和装置
公开(公告)号：US06340381B1
公开(公告)日：2002-01-22
申请号：US09620247
申请日：2000-07-20
申请人： Toshiaki Fujii , Tsukuru Suzuki , Hidetomo Suzuki , Kazuhiko Sakamoto
发明人： Toshiaki Fujii , Tsukuru Suzuki , Hidetomo Suzuki , Kazuhiko Sakamoto
IPC分类号： B01D5304
CPC分类号： B01D53/04 , B01D46/0036 , B01D46/12 , B01D2253/106 , B01D2253/108 , B01D2253/202 , B01D2256/24 , B01D2258/0216 , B01D2267/40 , B01D2279/51
摘要： A method and apparatus for preventing contamination of a substrate or a substrate surface, and particularly relates to prevention of contamination of raw materials, semi-finished products, base materials of products and substrate surface in a high-tech industry such as in the production of semiconductors and liquid crystals. A gas coming into contact with a base material or substrate is purified by dust removing apparatus and adsorption and/or absorption apparatus so that the concentration of fine particles in the gas is below class 1,000 and a non-methane hydrocarbon concentration is below 0.2 ppm. Thereafter, the base material or the substrate surface is exposed to this gas.
摘要翻译：防止基材或基材表面污染的方法和装置，特别涉及防止在高科技行业例如生产中的原料，半成品，产品的基材和基材表面的污染半导体和液晶。与基材或基材接触的气体通过除尘装置和吸附和/或吸收装置进行净化，使得气体中的微粒浓度低于1000，非甲烷烃浓度低于0.2ppm。此后，将基材或基板表面暴露于该气体。

90. 发明授权

US5922105A Method and apparatus for the preparation of clean gases 失效
公开(公告)号：US5922105A
公开(公告)日：1999-07-13
申请号：US44235
申请日：1998-03-19
申请人： Toshiaki Fujii , Tsukuru Suzuki , Hidetomo Suzuki , Kazuhiko Sakamoto
发明人： Toshiaki Fujii , Tsukuru Suzuki , Hidetomo Suzuki , Kazuhiko Sakamoto
IPC分类号： B01D53/04 , F24F3/16
CPC分类号： B01D53/0407 , B01D53/04 , F24F3/161 , B01D2253/10 , B01D2253/102 , B01D2253/106 , B01D2253/108 , B01D2253/202 , B01D2256/26 , B01D2257/702 , B01D2259/40001 , B01D2259/40083 , B01D53/0462 , B01D53/047
摘要： A method and apparatus for preventing contamination of a substrate or a substrate surface, and particularly relates to prevention of contamination of raw materials, semi-finished products, base materials of products and substrate surface in a high-tech industry such as in the production of semiconductors and liquid crystals. A gas coming into contact with a base material or substrate is purified by dust removing apparatus and adsorption and/or absorption apparatus so that the concentration of fine particles in the gas is below class 1,000 and a non-methane hydrocarbon concentration is below 0.2 ppm. Thereafter, the base material or the substrate surface is exposed to this gas.

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