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81. 发明申请

US20100286411A1 PROCESS FOR THE PREPARATION OF AN N-ALKYL LACTAM WITH IMPROVED COLOUR QUALITY 审中-公开
标题翻译：制备具有改善颜色质量的N-ALKYL LACTAM的方法
公开(公告)号：US20100286411A1
公开(公告)日：2010-11-11
申请号：US12842228
申请日：2010-07-23
申请人： Tobias Wabnitz , Rolf Pinkos , Karl Ott
发明人： Tobias Wabnitz , Rolf Pinkos , Karl Ott
IPC分类号： C07D207/12
CPC分类号： C07D201/18 , C07D207/267 , C07D211/76 , C07D223/10
摘要： A process for preparing an N-alkyllactam with improved color quality, wherein from 0.01 to 10% by weight of a C1-10-alcohol or a compound which releases from 0.01 to 10% by weight of a C1-10-alcohol is added to the N-alkyllactam.A mixture comprising at least 99.0% by weight of an N-alkyllactam and in the range from 100 to 5000 ppm by weight of a C1-10-alcohol or of an acetal, aminal or of an Orthoester which releases in the range from 100 to 5000 ppm by weight of a C1-10-alcohol.
摘要翻译：一种制备具有改进的颜色质量的N-烷基内酰胺的方法，其中将0.01至10重量％的C 1-10醇或从0.01至10重量％的C 1-10醇释放的化合物加入到 N-烷基内酰胺。一种混合物，其包含至少99.0重量％的N-烷基内酰胺，并且在100至5000重量ppm的C 1-10醇或缩醛，缩醛或直角酯中，其释放范围为100至 5000重量ppm的C 1-10醇。

82. 发明申请

US20100240864A1 METHOD FOR CHANGING THE PREDEFINED MEAN MOLECULAR WEIGHT MN DURING THE CONTINUOUS PRODUCTION OF POLYTETRAHYDROFURANES OR THE COPOLYMERS 有权
标题翻译：在连续生产聚四氢呋喃或共聚物期间改变预测的均分子量MN的方法
公开(公告)号：US20100240864A1
公开(公告)日：2010-09-23
申请号：US12295152
申请日：2007-12-10
申请人： Rolf Pinkos , Jochen Steiner , Stefan Käshammer , Tobias Wabnitz
发明人： Rolf Pinkos , Jochen Steiner , Stefan Käshammer , Tobias Wabnitz
IPC分类号： C08G65/20
CPC分类号： C08G65/20 , C08G65/2657 , C08G65/266 , C08G65/2696
摘要： The present invention provides a process for changing the given mean molecular weight Mn in the continuous preparation of polytetrahydrofuran or tetrahydrofuran copolymers, the mono- or diesters of polytetrahydrofuran or of tetrahydrofuran copolymers by polymerizing tetrahydrofuran in the presence of a telogen and/or of a comonomer over an acidic catalyst, wherein a) the molar ratio of telogen to tetrahydrofuran or to tetrahydrofuran and comonomer is changed, b) then the mean molecular weight of at least one sample is determined, c) until the mean molecular weight thus determined differs from the molecular weight to be achieved by the change, the already formed polytetrahydrofuran or the tetrahydrofuran copolymers, the mono- or diesters of polytetrahydrofuran or tetrahydrofuran copolymer is at least partly depolymerized over an acidic catalyst and d) the tetrahydrofuran recovered by depolymerization is recycled at least partly into the polymerization.
摘要翻译：本发明提供了在四氢呋喃或四氢呋喃共聚物的连续制备中改变给定的平均分子量Mn的方法，所述共聚单体是四氢呋喃或四氢呋喃共聚物的单酯或二酯，其在四环缩聚物和/或共聚单体存在下聚合四氢呋喃在酸性催化剂上，其中a）季戊四醇与四氢呋喃或四氢呋喃和共聚单体的摩尔比改变，b）确定至少一种样品的平均分子量，c）直到如此确定的平均分子量与通过改变实现的分子量，已经形成的聚四氢呋喃或四氢呋喃共聚物，聚四氢呋喃或四氢呋喃共聚物的单酯或二酯在酸性催化剂上至少部分解聚，以及d）通过解聚回收的四氢呋喃至少部分地再循环进入聚合。

83. 发明申请

US20100044626A1 METHOD FOR PRODUCING PYRROLIDONES FROM SUCCINATES FROM FERMENTATION BROTHS 有权
标题翻译：从发酵生产来自成员的吡咯烷酮的方法
公开(公告)号：US20100044626A1
公开(公告)日：2010-02-25
申请号：US11722263
申请日：2005-12-17
申请人： Wolfgang Fischer , Daniella Klein , Andreas Kuenkel , Rolf Pinkos , Edzard Scholten
发明人： Wolfgang Fischer , Daniella Klein , Andreas Kuenkel , Rolf Pinkos , Edzard Scholten
IPC分类号： C12P17/10 , C09K3/00
CPC分类号： C07D207/408 , C07D207/267 , Y02P20/582
摘要： The present invention relates to a process for preparing a compound II or a composition comprising the compound II to a composition comprising succinimide and to a composition prepared by the process according to the invention
摘要翻译：本发明涉及一种制备化合物II或包含化合物II的组合物的方法，其包含琥珀酰亚胺的组合物和通过本发明的方法制备的组合物

84. 发明申请

US20100016643A1 PROCESS FOR PREPARING 1,4-BUTANEDIOL 有权
标题翻译：制备1,4-丁二醇的方法
公开(公告)号：US20100016643A1
公开(公告)日：2010-01-21
申请号：US12527139
申请日：2007-03-14
申请人： Rolf Pinkos , Rudolf Erich Lorenz , York Alexander Beste
发明人： Rolf Pinkos , Rudolf Erich Lorenz , York Alexander Beste
IPC分类号： C07C29/14
CPC分类号： C07C29/42 , C07C29/172 , Y02P20/125 , C07C33/046 , C07C31/207
摘要： The present invention provides an integrated process for continuously preparing 1,4-butanediol, which comprises the following stages:(I) reacting formaldehyde with acetylene in the presence of a copper catalyst at a pH of from 5 to 8 and a molar ratio of formaldehyde to acetylene of at most 2:1, (II) intermediately buffering the resulting butynediol-containing aqueous mixture for from 0.1 to 100 h, (III) hydrogenating the mixture obtained after the intermediate buffering and (IV) distilling the hydrogenation product obtained in stage III to obtain 1,4-butanediol.
摘要翻译：本发明提供连续制备1,4-丁二醇的一体化方法，其包括以下步骤：（I）在铜催化剂存在下，在5至8的pH下与甲醛与乙炔反应，并且甲醛的摩尔比至最多2:1的乙炔，（II）将所得的含丁炔二醇的含水混合物中间缓冲0.1至100小时，（III）将中间缓冲后获得的混合物氢化，并且（IV）蒸馏阶段获得的氢化产物 III得到1,4-丁二醇。

85. 发明授权

US07456249B2 Catalyst, its preparation and the polymerization of cyclic ethers over this catalyst 有权
标题翻译：催化剂，其制备和在该催化剂上聚合环醚
公开(公告)号：US07456249B2
公开(公告)日：2008-11-25
申请号：US11971931
申请日：2008-01-10
申请人： Stephan Schlitter , Martin Haubner , Michael Hesse , Stefan Kaeshammer , Rolf Pinkos , Christoph Sigwart
发明人： Stephan Schlitter , Martin Haubner , Michael Hesse , Stefan Kaeshammer , Rolf Pinkos , Christoph Sigwart
IPC分类号： C08G59/68 , C08G65/26 , B01J21/16 , B01J35/00
CPC分类号： C08G61/125 , B01J21/16 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J35/108 , C08G65/2657
摘要： The present invention relates to a solid, acid catalyst for the preparation of polytetrahydrofuran, polytetrahydrofuran copolymers, diesters or monoesters of these polymers by polymerization of tetrahydrofuran in the presence of at least one telogen and/or comonomer, which has a BET surface area of at least 160 m2/g and an acid center density of at least 0.05 mmol/g for pKa values of from 1 to 6, to a process for preparing it and to a process for the polymerization of cyclic ethers over this catalyst.
摘要翻译：本发明涉及一种固体酸催化剂，用于通过四氢呋喃在至少一种具有BET表面积的前体和/或共聚单体的存在下聚合来制备这些聚合物的聚四氢呋喃，聚四氢呋喃共聚物，二酯或单酯至少160m 2 / g，对于pK值为1至6的酸中心密度至少为0.05mmol / g，其制备方法和在该催化剂上聚合环醚的方法。

86. 发明申请

US20080275276A1 Method for Producing Cyclododecanone 审中-公开
标题翻译：生产环十二烷酮的方法
公开(公告)号：US20080275276A1
公开(公告)日：2008-11-06
申请号：US10573327
申请日：2004-09-23
申请人： Joaquim Henrique Teles , Beatrice Rossler , Rolf Pinkos , Thomas Genger , Thomas Preiss
发明人： Joaquim Henrique Teles , Beatrice Rossler , Rolf Pinkos , Thomas Genger , Thomas Preiss
IPC分类号： C07C45/28
CPC分类号： C07C45/28 , C07C2601/20 , C07C49/413
摘要： A process for preparing cyclododecanone by reacting cyclododecene with dinitrogen monoxide, comprising in particular steps (I) and (II): (I) preparing cyclododecene by partially hydrogenating cyclododecatriene; (II) reacting cyclododecene obtained in (I) with dinitrogen monoxide to obtain cyclododecanone.
摘要翻译：通过环十二碳烯与一氧化二氮反应制备环十二烷酮的方法，特别包括步骤（I）和（II）：（I）通过部分氢化环十二碳三烯制备环十二烯; （II）使得（I）中得到的环十二碳烯与一氧化二氮反应，得到环十二烷酮。

87. 发明申请

US20080216390A1 Biodiesel Fuel Mixture Containing Polyoxymethylene Dialkyl Ether 审中-公开
标题翻译：含有聚甲醛二烷基醚的生物柴油燃料混合物
公开(公告)号：US20080216390A1
公开(公告)日：2008-09-11
申请号：US11994123
申请日：2006-06-26
申请人： Gerd-Dieter Tebben , Heiner Schelling , Eckhard Stroefer , Rolf Pinkos , Andrea Haunert , Matthias Eiermann , Jorn Karl
发明人： Gerd-Dieter Tebben , Heiner Schelling , Eckhard Stroefer , Rolf Pinkos , Andrea Haunert , Matthias Eiermann , Jorn Karl
IPC分类号： C10L1/00
CPC分类号： C10L1/14 , C10G2300/1011 , C10G2300/307 , C10G2300/80 , C10L1/026 , C10L1/1616 , C10L1/1852 , C10L1/19 , C10L1/1985 , C10L10/02 , C10L10/12 , Y02E50/13 , Y02P30/20
摘要： A biodiesel fuel mixture having a cetane number of >40, comprising a) from 1 to 100% by weight of biodiesel, b) from 0 to 98.9% by weight of diesel oil of fossil origin, c) from 0.1 to 20% by weight of polyoxyalkylene dialkyl ether of the formula RO(CH2O)nR in which R is an alkyl group having from 1 to 10 carbon atoms and n=from 2 to 10, and d) from 0 to 5% by weight of further additives.
摘要翻译：十六烷值> 40的生物柴油燃料混合物，其包含a）1至100重量％的生物柴油，b）0至98.9重量％的源自化石油的柴油，c）0.1至20重量％具有式<β的聚氧化烯二烷基醚，其中式-β-line-formula description =“In-line Formulas”end =“lead”→> RO（CH 2 O 2）n < 其中R为具有1至10个碳原子且n = 2至10个碳原子的烷基，d）为0以上，其中R为直链式公式描述=“In-line Formula”end =“tail” 至5重量％的其它添加剂。

88. 发明申请

US20070135650A1 Method for the production of defined mixtures of thf, bdo and gbl by gas phase hydrogenation 失效
公开(公告)号：US20070135650A1
公开(公告)日：2007-06-14
申请号：US10581074
申请日：2004-12-04
申请人： Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
发明人： Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
IPC分类号： C07D307/02
CPC分类号： C07D307/33 , C07D307/08
摘要： The present invention provides a process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) in a first step in the gas phase, hydrogenating a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a catalyst at a pressure of from 2 to 100 bar and a temperature of from 200° C. to 300° C. in a first reactor in the presence of a catalyst in the form of shaped catalyst bodies having a volume of less than 20 mm3, said catalyst from 5 to 95% by weight of oxide of copper and from 5 to 95% by weight of an oxide having acidic sites, to give a stream mainly containing of optionally alkyl-substituted GBL and THF, b) removing any succinic anhydride formed by partial condensation, c) converting the products remaining predominantly in the gas phase in the partial condensation, THF, water and GBL, under the same pressure or under a pressure reduced by the pressure drops in the hydrogenation circuit and at a temperature of from 150 to 240° C., in a second reactor over a catalyst which ≦95% by weight of CuO and from 5 to 95% by weight of one or more oxides selected from the group of ZnO, Al2O3, SiO2, TiO2, ZrO2, CeO2, MgO, CaO, SrO, BaO, La2O3 and Mn2O3 to give a stream comprising a mixture of BDO, GBL and THF, d) removing the hydrogen from the products and recycling it into the hydrogenation, e) distillatively separating the products, THF, BDO, GBL and water, if appropriate recycling a GBL-rich stream into the second reactor or if appropriate discharging it, and working up BDO, THF and GBL distillatively, and setting the ratio of the products, THF, GBL and BDO, relative to one another within the range from 10 to 100% by weight of THF, from 0 to 90% by weight of GBL and from 0 to 90% by weight of BDO only by varying the temperatures in the two hydrogenation zones and also if appropriate the GBL recycle stream.

89. 发明授权

US07098349B2 Method for producing tetrahydrofuran 有权
公开(公告)号：US07098349B2
公开(公告)日：2006-08-29
申请号：US10524851
申请日：2003-07-30
申请人： Rolf Pinkos , Stefan Käshammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
发明人： Rolf Pinkos , Stefan Käshammer , Volkmar Menger , Martin Haubner , Peter Groll , Stephan Schlitter , Klaus-Peter Pfaff
IPC分类号： C07D307/02
CPC分类号： C08G65/20 , C07D307/08 , C08G65/2666
摘要： The invention relates to a process for the continuous preparation of THF by reaction of a 1,4-butanediol-containing reaction mixture over a heteropolyacid catalyst which has not been predried, wherein the reaction mixture comprises 2-(4-hydroxybutoxy)tetrahydrofuran.

90. 发明授权

US07094933B2 Method for producing tetrahydrofurane copolymers 失效
标题翻译：制备四氢呋喃共聚物的方法
公开(公告)号：US07094933B2
公开(公告)日：2006-08-22
申请号：US10524555
申请日：2003-07-30
申请人： Martin Haubner , Rolf Pinkos , Alexander Weck
发明人： Martin Haubner , Rolf Pinkos , Alexander Weck
IPC分类号： C07C43/13 , C07C43/11
CPC分类号： C08G65/20
摘要： The present invention provides a process for one-stage preparation of polyoxyalkylene glycols by copolymerizing tetrahydrofuran and alpha,omega-diols in the presence of a heteropolyacid and of a hydrocarbon, which comprises distilling water in a mixture with this hydrocarbon out of the copolymerization.
摘要翻译：本发明提供了通过在杂多酸和烃的存在下共聚合四氢呋喃和α，ω-二醇来一步法制备聚氧亚烷基二醇的方法，该方法包括在共聚合中将该混合物中的水与该烃进行蒸馏。

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