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81. 发明申请

US20110237841A1 NOVEL SELECTIVE HYDROGENATION CATALYST COMPRISING PALLADIUM ON POROUS SILICA GLASS AND THE USE THEREOF 有权
标题翻译：含多孔二氧化硅玻璃的新型选择性氢化催化剂及其用途
公开(公告)号：US20110237841A1
公开(公告)日：2011-09-29
申请号：US13059477
申请日：2009-08-20
申请人： Werner Bonrath , Bernd Ondruschka , Christine Schmoeger , Achim Stolle
发明人： Werner Bonrath , Bernd Ondruschka , Christine Schmoeger , Achim Stolle
IPC分类号： C07C29/17 , B01J21/08 , B01J35/10 , B01J35/02
CPC分类号： C07C5/09 , B01J21/08 , B01J23/44 , B01J35/023 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1061 , B01J35/1066 , C07C29/17 , C07C2523/44 , C07C33/02 , C07C33/025
摘要： The present invention is directed to a catalyst comprising palladium on a porous Silica glass as carrier, as well as to the use of such catalyst for the selective hydrogenation of alkines to alkenes.
摘要翻译：本发明涉及一种催化剂，其包含作为载体的多孔二氧化硅玻璃上的钯，以及这种催化剂用于将烯烃选择性氢化为烯烃的催化剂。

82. 发明授权

US07842841B2 Process for the preparation of timberone 有权
标题翻译：木材制备工艺
公开(公告)号：US07842841B2
公开(公告)日：2010-11-30
申请号：US12532419
申请日：2008-03-17
申请人： Werner Bonrath , Jan Schuetz
发明人： Werner Bonrath , Jan Schuetz
IPC分类号： C07C45/00
CPC分类号： C07C45/62 , C07C45/74 , C07C403/16 , C07C2601/14 , C07C2601/16 , C07C49/11 , C07C49/203
摘要： This invention relates to a novel process for the preparation of timberone useful for perfume or cosmetics.
摘要翻译：本发明涉及一种制备用于香料或化妆品的木材的新方法。

83. 发明申请

US20100063325A1 NOVEL PROCESS FOR THE PREPARATION OF TIMBERONE 有权
标题翻译：制备TIMBERONE的新工艺
公开(公告)号：US20100063325A1
公开(公告)日：2010-03-11
申请号：US12532419
申请日：2008-03-17
申请人： Werner Bonrath , Jan Schuetz
发明人： Werner Bonrath , Jan Schuetz
IPC分类号： C07C45/00
CPC分类号： C07C45/62 , C07C45/74 , C07C403/16 , C07C2601/14 , C07C2601/16 , C07C49/11 , C07C49/203
摘要： This invention relates to a novel process for the preparation of timberone useful for perfume or cosmetics.
摘要翻译：本发明涉及一种制备用于香料或化妆品的木材的新方法。

84. 发明申请

US20090227819A1 PROCESS FOR UBIQUINONE INTERMEDIATES 有权
标题翻译： UBIQUINONE中间体的方法
公开(公告)号：US20090227819A1
公开(公告)日：2009-09-10
申请号：US12097836
申请日：2006-12-08
申请人： Werner Bonrath , Francesco Pace
发明人： Werner Bonrath , Francesco Pace
IPC分类号： C07C33/048
CPC分类号： C07C29/42 , C07B2200/09 , C07C33/048 , C07C33/02
摘要： A process for the preparation of terminally ethylenically unsaturated isopolyprenols characterized in that a carbonyl compound is reacted with ethine in the presence of ammonia and low amounts of an alkaline metal hydroxide and, if desired, the terminally acetylenically unsaturated isopolyprenol obtained is partially hydrogenated in the presence of a catalyst suitable for selective hydrogenation.
摘要翻译：一种用于制备末端烯键式不饱和异戊二烯的方法，其特征在于羰基化合物在氨和少量碱金属氢氧化物的存在下与乙胺反应，如果需要，所得到的末端炔属不饱和异戊二烯醇在存在下部分氢化的适合选择性氢化的催化剂。

85. 发明申请

US20090221860A1 TRANSPORT OF ETHYNE IN FORM OF A-ALKYNOLS AS ETHYNE PRECURSORS 有权
标题翻译：乙腈在乙腈前驱体中的运输
公开(公告)号：US20090221860A1
公开(公告)日：2009-09-03
申请号：US12298371
申请日：2007-03-30
申请人： Angela Wildermann , Werner Bonrath , Gunther Hellmann
发明人： Angela Wildermann , Werner Bonrath , Gunther Hellmann
IPC分类号： C07C7/20
CPC分类号： C07C29/42 , C07C1/20 , C07C7/20 , C07C11/24 , C10L3/02 , C07C33/042 , C07C33/048
摘要： The present invention relates to a new method for a safe transport of ethyne in form of α-alkynols as precursors for ethyne. The new method comprises three steps. In a first step the synthesis of the α-alkynol(s) is performed by reacting ethyne with (a) carbonyl compound(s). The second step comprises the transport of the resulting α-alkynol(s) in a safe manner, whereas the safety requirements for this transport are not as high as for ethyne because α-alkynol(s) are normally classified for transportation as hazardous class 3. In the third step the α-alkynol(s) can be cleaved and the ethyne and the carbonyl compound(s) can be obtained in the cleavage reaction and can be separated to yield pure products for further applications.
摘要翻译：本发明涉及一种以α-炔醇形式的乙炔安全运输作为乙炔前体的新方法。新方法包括三个步骤。在第一步中，α-炔醇的合成通过使乙炔与（a）羰基化合物反应来进行。第二步包括以安全的方式运输所得的α-炔醇，而这种运输的安全要求不如乙炔那么高，因为α-炔醇通常被分类为危险品类3 在第三步中，可以裂解α-炔醇，并且可以在裂解反应中获得乙炔和羰基化合物，并且可以分离以产生用于进一步应用的纯产物。

86. 发明申请

US20060293529A1 Process for the manufacture of tocyl and tocopheryl acylates 有权
标题翻译：制备辛酰基和生育酚酰化物的方法
公开(公告)号：US20060293529A1
公开(公告)日：2006-12-28
申请号：US10554885
申请日：2004-04-27
申请人： Werner Bonrath , Lisa Giraudi
发明人： Werner Bonrath , Lisa Giraudi
IPC分类号： C07D311/02
CPC分类号： C07D311/72
摘要： A process for the manufacture of a tocyl acylate or a tocopheryl acylate comprises reacting tocol or a tocopherol with an acylating agent in the presence of a solid heterogeneous Brönsted acid catalyst, said catalyst being an inorganic Brönsted acid on a solid carrier material which comprises silicon dioxide, titanium dioxide or both silicon dioxide and titanium dioxide, or being an organofunctional polysilonaxe featuring sulpho groups, the solid heterogeneous Brönsted acid catalyst further featuring a BET surface area from about 10 m2/g to about 800 m2/g and a pore volume from about 0.1 ml/g to about 2.0 ml/g. The main commercial form of vitamin E, being (all-rac)-α-tocopheryl acetate, can be manufactured by acylation of (all-rac)-α-tocopherol according to this process.
摘要翻译：制备酰基酰化物或生育酚酰基化物的方法包括在固体异质布朗斯台德酸催化剂存在下，将酰基转化成醇或生育酚，所述催化剂是固体载体材料上的无机布朗斯台德酸，其包含二氧化硅，二氧化钛或二氧化硅二氧化钛，或者是具有硫酸基的有机官能聚异氰酸酯，该固体异质布朗斯台德酸催化剂还具有约10m 2 / g至约800μm的BET表面积 2 / g，孔体积为约0.1ml / g至约2.0ml / g。维生素E的主要商业形式是（全脱氧）-α-生育酚乙酸酯，可以通过根据该方法酰化（全 - 外消旋）-α-生育酚来制备。

87. 发明授权

US06949685B2 Ethynylation process 失效
公开(公告)号：US06949685B2
公开(公告)日：2005-09-27
申请号：US10489523
申请日：2002-09-19
申请人： Werner Bonrath , Bernd Englert , Reinhard Karge , Michael Schneider
发明人： Werner Bonrath , Bernd Englert , Reinhard Karge , Michael Schneider
IPC分类号： C07B61/00 , C07C29/42 , C07C33/042 , C07C33/048 , C07C33/04 , C07C33/044 , C07C33/046
CPC分类号： C07C29/42 , C07C33/02
摘要： A process for the manufacture of an acetylenically unsaturated alcohol comprising reacting formaldehyde, an aldehyde or a ketone (a carbonyl compound) with acetylene in the presence of ammonia and a strongly basic macroporous anion exchange resin, the latter preferably featuring a polystyrene matrix and quaternary ammonium groups, preferably of type I or Type II. The reaction products, which depending on the starting carbonyl compound are propargyl alcohol or 1-monosubstituted or 1,1-disubstituted derivatives thereof, are of use as intermediates in the synthesis of many useful end products, inter alia in the field of vitamins and carotenoids.

88. 发明申请

US20050059844A1 Ethynylation process 失效
标题翻译：乙炔化过程
公开(公告)号：US20050059844A1
公开(公告)日：2005-03-17
申请号：US10489523
申请日：2002-09-19
申请人： Werner Bonrath , Bernd Englert , Reinhard Karge , Michael Schneider
发明人： Werner Bonrath , Bernd Englert , Reinhard Karge , Michael Schneider
IPC分类号： C07B61/00 , C07C29/42 , C07C33/042 , C07C33/048 , C07C27/18
CPC分类号： C07C29/42 , C07C33/02
摘要： A process for the manufacture of an acetylenically unsaturated alcohol comprising reacting formaldehyde, an aldehyde or a ketone (a carbonyl compound) with acetylene in the presence of ammonia and a strongly basic macroporous anion exchange resin, the latter preferably featuring a polystyrene matrix and quaternary ammonium groups, preferably of type I or Type II. The reaction products, which depending on the starting carbonyl compound are propargyl alcohol or 1-monosubstituted or 1,1-disubstituted derivatives thereof, are of use as intermediates in the synthesis of many useful end products, inter alia in the field of vitamins and carotenoids.
摘要翻译：一种制备炔属不饱和醇的方法，包括在氨和强碱性大孔阴离子交换树脂的存在下使甲醛，醛或酮（羰基化合物）与乙炔反应，后者优选具有聚苯乙烯基质和季铵组，优选I型或II型。取决于起始羰基化合物的反应产物是炔丙醇或其1-取代或1,1-二取代的衍生物，可用作合成许多有用的终产物的中间体，特别是在维生素和类胡萝卜素领域。

89. 发明授权

US06482961B2 Method of making (all-rac)-&agr;-tocopherol 有权
标题翻译：制造（全脱色）-α-生育酚的方法
公开(公告)号：US06482961B2
公开(公告)日：2002-11-19
申请号：US09931663
申请日：2001-08-16
申请人： Werner Bonrath , Alois Haas , Eike Hoppmann , Horst Pauling
发明人： Werner Bonrath , Alois Haas , Eike Hoppmann , Horst Pauling
IPC分类号： C07D31104
CPC分类号： C07D311/72
摘要： The present invention is a method of making (all-rac)-&agr;-tocopherol in a reaction having the following steps: a) reacting trimethylhydroquinone and a phytol selected from the group consisting of isophytol and phytol in the presence of a bis(perfluorinated hydrocarbyl sulphonyl)imide catalyst or a metal salt thereof of formula I: [(R1SO2)2N]xR2 (I) wherein each R1, independently, signifies a perfluoroalkyl group CnF2n+1 or a pentafluorophenyl, or both symbols R1 together signify a poly-difluoromethylene group—(CF2)m—, with the proviso that both symbols R1 cannot simultaneously signify trifluoromethyl, R2 signifies a proton or a cationic form of a metal selected from the group consisting of boron, magnesium, aluminum, silicon, scandium, titanium, vanadium, manganese, iron, cobalt, nickel, copper, zinc, yttrium, zirconium, rhodium, palladium, silver, tin, lanthanum, cerium, praseodymium, neodymium, europium, dysprosium, thulium, ytterbium, hafnium, platinum, and gold, m is an integer from 2 to 4, n is an integer from 1 to 10, and x is the corresponding valency of the proton (1) or the metal cation (1, 2, 3, or 4), in organic solvent; and b) recovering (all-rac)-&agr;-tocopherol from the reaction mixture.
摘要翻译：本发明是在具有以下步骤的反应中制备（全脱氧）-α-生育酚的方法：a）在双（全氟化烃基）的存在下，使三甲基对苯二酚和选自异麦芽糖醇和植醇的植醇磺酰基）酰亚胺催化剂或其金属盐：其中R1独立地表示全氟烷基CnF2n + 1或五氟苯基，或两个符号R1一起表示聚二氟亚甲基 - （CF 2）m - ，条件是两个符号R1不能同时表示三氟甲基，R2表示选自硼，镁，铝，硅，钪，钛，钒，锰，铁，钴，镍，铜等的金属的质子或阳离子形式。锌，钇，锆，铑，钯，银，锡，镧，铈，镨，钕，铕，镝，ium，镱，铪，铂和金，m为2〜4的整数，n为 ger为1至10，andx为有机溶剂中质子（1）或金属阳离子（1,2,3或4）的相应化合价; 和b）从反应混合物中回收（全 - 外）-α-生育酚。

90. 发明授权

US08916715B2 Process for 4-methyloxazole-5-carboxamide 有权
标题翻译： 4-甲基恶唑-5-甲酰胺的方法
公开(公告)号：US08916715B2
公开(公告)日：2014-12-23
申请号：US14127610
申请日：2012-05-31
申请人： Werner Bonrath , Jocelyn Fischesser , Hongyan Shen
发明人： Werner Bonrath , Jocelyn Fischesser , Hongyan Shen
IPC分类号： C07D263/34 , C07D213/69
CPC分类号： C07D263/34 , C07D213/69
摘要： A process for the preparation of 4-methyl-oxazole-5-carboxamide, an intermediate in the synthesis of pyridoxine, by reacting lower alkyl 4-methyl-oxazole-5-carboxy-late with a molar excess of anhydrous, liquid ammonia.
摘要翻译：通过将4-甲基 - 恶唑-5-羧基 - 低级烷基与摩尔过量的无水液氨反应，制备4-甲基 - 恶唑-5-甲酰胺（合成吡哆醇的中间体）的方法。

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