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    • 76. 发明授权
    • Transparent polycrystalline material and production process for the same
    • 透明多晶材料和生产工艺相同
    • US08470724B2
    • 2013-06-25
    • US13142132
    • 2009-12-25
    • Takunori TairaJun AkiyamaShigeo AsaiKunihiko Hara
    • Takunori TairaJun AkiyamaShigeo AsaiKunihiko Hara
    • C04B35/50
    • H01F41/0253B28B1/00B33Y40/00C04B35/447C04B35/50C04B35/6455C04B2235/3224C04B2235/6027C04B2235/605C04B2235/9653C30B28/00C30B29/22C30B29/30C30B30/04H01S3/1603H01S3/1611H01S3/1618H01S3/1671H01S3/1673H01S3/1685
    • Upon producing a transparent polycrystalline material, a suspension liquid (or slurry 1) is prepared, the suspension liquid being made by dispersing a raw-material powder in a solution, the raw-material powder including optically anisotropic single-crystalline particles to which a rare-earth element is added. A formed body is obtained from the suspension liquid by means of carrying out slip casting in a space with a magnetic field applied. On this occasion, while doing a temperature control so that the single-crystalline particles demonstrate predetermined magnetic anisotropy, one of static magnetic fields and rotary magnetic fields is selected in compliance with a direction of an axis of easy magnetization in the single-crystalline particles, and is then applied to them. A transparent polycrystalline material is obtained by sintering the formed body, the transparent polycrystalline material having a polycrystalline structure whose crystal orientation is controlled. In this calcination step, after subjecting the formed body to primary sintering at a temperature of 1,600-1,900 K, the resulting primarily-sintered body undergoes hot-isotropic-press sintering (or HIP processing) at a temperature of 1,600-1,900 K.
    • 在制备透明多晶材料时,制备悬浮液(或浆液1),悬浮液通过将原料粉末分散在溶液中而制成,原料粉末包括光学各向异性单晶颗粒,其中稀有 添加了地面元素。 通过在施加磁场的空间中进行滑移铸造,从悬浮液获得成形体。 在这种情况下,当进行温度控制使得单晶颗粒表现出预定的磁各向异性时,根据单晶颗粒中易磁化轴的方向选择静磁场和旋转磁场之一, 然后应用于它们。 通过烧结成形体获得透明多晶材料,该透明多晶材料具有晶体取向被控制的多晶结构。 在该烧成工序中,在1600〜1900K温度下对成型体进行一次烧结后,在1600〜1900K的温度下进行热均质压制烧结(或HIP加工)。