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    • 77. 发明申请
    • CELL WITH REUSABLE AND DISPOSABLE ASSEMBLIES FOR SIMULTANEOUS ELECTROCHEMICAL AND EPR MEASUREMENTS
    • 具有用于同时电化学和EPR测量的可重复和可弃置的组件的单元
    • US20150068899A1
    • 2015-03-12
    • US14023468
    • 2013-09-11
    • KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    • ABDEL-NASSER METWALLY ALY KAWDEMOHAMED ALY MORSY
    • G01N27/30H01M6/14G01N27/403
    • H01M14/00G01N24/10G01N27/403G01N27/416G01R33/30Y10T29/4911
    • A cell and method for simultaneous electrochemical and EPR measurements, including a disposable assembly, allows for a single device to produce data for both electroanalysis and EPR spectroscopy by generating a Redox reaction to form free radicals. The cell includes first and second hollow tubes, with the second tube being removably insertable into the first hollow tube. The interior of the first tube contains an insulating material, an electro-conductive material, and a wire connector extending from the electro-conductive material and out the first tube. The interior of the second tube contains an electrolytic solution, an analyte, a working electrode, and insulating material surrounding the working electrode. The second tube is inserted into the first tube and a reference electrode is placed into the second tube. The cell is placed within an EPR spectrometer. A potential is applied to the reference electrode to generate the Redox reaction of the analyte.
    • 用于同时电化学和EPR测量的电池和方法,包括一次性组件,允许单个装置通过产生氧化还原反应以形成自由基来产生电分析和EPR光谱的数据。 电池包括第一和第二中空管,第二管可拆卸地插入第一中空管中。 第一管的内部包含绝缘材料,导电材料和从导电材料延伸出第一管的导线连接器。 第二管的内部包含电解液,分析物,工作电极和围绕工作电极的绝缘材料。 将第二管插入第一管中,将参考电极放置在第二管中。 将该电池置于EPR光谱仪内。 对参比电极施加电位以产生分析物的氧化还原反应。