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71. 发明授权

US06830818B2 Polymer material and polymer film 失效
标题翻译：聚合物材料和聚合物膜
公开(公告)号：US06830818B2
公开(公告)日：2004-12-14
申请号：US10103129
申请日：2002-03-22
申请人： Katsuyuki Imoto , Hiroshi Tsushima , Emi Watanabe
发明人： Katsuyuki Imoto , Hiroshi Tsushima , Emi Watanabe
IPC分类号： B32B904
CPC分类号： C08L83/04 , C08G77/12 , C08G77/16 , C08G77/24 , C08G77/60 , C08L83/14 , Y10T428/31663 , C08L83/00
摘要： A silicone compound, either alone or in combination with a photoacid generator, is added to a branched polysilane compound. According to this constitution, highly reliable polymer material and polymer film can be realized which have excellent stability of refractive index against heat and high transparency and, when the photoacid generator is contained, can cause a change in refractive index upon exposure to ultraviolet light with high sensitivity and high resolution.
摘要翻译：将单独或与光酸产生剂组合的硅氧烷化合物加入支化聚硅烷化合物中。根据该构成，可以实现高折射率的聚合物材料和聚合物薄膜，其具有优异的折射率对热和高透明度的稳定性，并且当含有光致酸产生剂时，可以在暴露于具有高的紫外线的情况下引起折射率的变化灵敏度高，分辨率高。

72. 发明授权

US06759502B1 Synthesis of hyperbranched organometallic polymers and their use as precursors to advanced ceramic materials 失效
标题翻译：超支化有机金属聚合物的合成及其作为先进陶瓷材料的前体的用途
公开(公告)号：US06759502B1
公开(公告)日：2004-07-06
申请号：US10106752
申请日：2002-03-26
申请人： Ben Zhong Tang , Kaitian Xu , Han Peng , Jingdong Luo , Xixiang Zhang , Qunhui Sun , Wing Yip Lam , John A. K. Cha
发明人： Ben Zhong Tang , Kaitian Xu , Han Peng , Jingdong Luo , Xixiang Zhang , Qunhui Sun , Wing Yip Lam , John A. K. Cha
IPC分类号： C08G7760
CPC分类号： C08G77/60
摘要： Hyperbranched organometallic polymers, including poly [1,1′-ferrocenylenesilynes], poly [1,1′-ferrocenylene-(alkyl)silynes], poly [1,1′-ferrocenylene(alkenyl)silynes] and poly [1,1′-ferrocenylene(aromatic)silynes], are useful as precursors to certain ceramic materials. Processes for the preparation of such polymers and the preparation of ceramic materials from such polymers are described, as are the resulting ceramic materials and their use as ferromagnetic materials and electrically conductive materials.
摘要翻译：超支化有机金属聚合物，包括聚[1,1'-二茂铁基苯醚]，聚[1,1'-二茂铁基 - （烷基）硅藻土]，聚[1,1'-二茂铁基（烯基）硅藻]和聚[1,1' - 亚铁基（芳族）硅藻土]可用作某些陶瓷材料的前体。对这些聚合物的制备方法和由这些聚合物制备的陶瓷材料进行了描述，所得到的陶瓷材料及其作为铁磁材料和导电材料的用途也被描述。

73. 发明申请

US20020115836A1 Non-thrombogenic coating composition and methods for using same 有权
标题翻译：非血栓形成的涂层组合物及其使用方法
公开(公告)号：US20020115836A1
公开(公告)日：2002-08-22
申请号：US10047118
申请日：2002-01-14
发明人： Ray Tsang , Shigemasa Osaki
IPC分类号： A61K031/727 , C08B037/10
CPC分类号： A61L33/0029 , A61L27/28 , A61L31/08 , A61L33/0011 , A61L33/08 , C08B37/0063 , C08B37/0075 , C08G77/60 , C09D105/08 , C09D105/10 , C08L83/00
摘要： The present invention provides an anti-thrombogenic and cellular-adhesion coating composition for blood-contacting surfaces. The coating comprises a covalent complex of from 1 to 30 hydrophobic silyl moieties of Formula I: 1 wherein R1 is an C1-18 alkyl or C6-32 aryl group, each R2 is independently selected from the group consisting of C1-18 alkyl and C6-32 aryl, R3 is N or O, n is a number from 1 to 10, directly bound to a heparin molecule via covalent bonding, with an adhesive molecule directly bound to the heparin molecule. In one embodiment, the coating comprises benzyl-(1,2 dimethyl)disilyl heparin, wherein an adhesive molecule, such as fibronectin, is bound to the heparin.
摘要翻译：本发明提供了用于接触血液的表面的抗血栓形成和细胞粘附涂层组合物。该涂层包含1至30个式I的疏水性甲硅烷基部分的共价络合物：其中R1是C1-18烷基或C6-32芳基，每个R2独立地选自C1-18烷基和C6- 32芳基，R3是N或O，n是1至10的数，通过共价键直接与肝素分子结合，其中粘合分子与肝素分子直接结合。在一个实施方案中，涂层包含苄基 - （1,2二甲基）二甲硅烷基肝素，其中粘合剂分子例如纤连蛋白与肝素结合。

74. 发明授权

US06416855B1 Composite material containing fine particles of metal dispersed in polysilylenemethylene and process for the preparation thereof 失效
标题翻译：复合材料含有分散在聚亚甲基亚甲基中的金属微粒和其制备方法
公开(公告)号：US06416855B1
公开(公告)日：2002-07-09
申请号：US09351859
申请日：1999-07-13
申请人： Fabrice Rossignol , Masaaki Suzuki , Hideaki Nagai , Yoshinori Nakata , Takeshi Okutani , Nobuo Kushibiki , Masashi Murakami
发明人： Fabrice Rossignol , Masaaki Suzuki , Hideaki Nagai , Yoshinori Nakata , Takeshi Okutani , Nobuo Kushibiki , Masashi Murakami
IPC分类号： B32B516
CPC分类号： B82Y30/00 , C08G77/60 , C08K3/08 , G02B1/04 , Y10T428/25 , Y10T428/256 , Y10T428/26 , Y10T428/268 , C08L65/00 , C08L79/08 , C08L83/16
摘要： A composite material having a plurality of laminated polysilylenemethylene layers each having an inside region adjacent to a surface thereof in which nanoparticles of a metal of Au, Pt, Pd, Cu or Ag are dispersed. The composite material is produced by heating a layer of disilacyclobutane overlaid with a layer of nanoparticles of the above metal to polymerize the disilacyclobutane. The above procedure is repeated at least once more.
摘要翻译：一种复合材料，其具有多个叠层的聚亚甲基亚甲基层，各自具有与Au，Pt，Pd，Cu或Ag的金属的纳米颗粒分散的表面相邻的内部区域。复合材料通过加热覆盖有上述金属纳米颗粒层的二环丁烷层以聚合二环丁烷来制备。至少重复上述过程一次。

75. 发明申请

US20020058747A1 Carbosilane and polycarbosilane 有权
标题翻译：碳硅烷和聚碳硅烷
公开(公告)号：US20020058747A1
公开(公告)日：2002-05-16
申请号：US09801722
申请日：2001-06-05
发明人： Kazutoshi Ikenaga
IPC分类号： C08J003/00
CPC分类号： C07F7/2204 , C07F7/24 , C07F7/30 , C08G77/60
摘要： The present invention provides carbosilanes represented by the following general formula (1), polycarbosilanes synthesized therefrom by the polymerization reaction using an organic typical metal compound as an initiator, and the processes for producing the same. 1 wherein M represents an Sn, Ge or Pb atom; A represents an aliphatic group having 2-10 carbon atoms, a carbocyclic group or a heterocyclic group containing one or more atoms selected from silicon, oxygen, nitrogen and sulfur atoms, both groups having 6-30 carbon atoms; R1, R2, R3, R6, R7and R8 each independently represent an alkyl group having 1-20 carbon atoms, an alkenyl or alkynyl group having 2-20 carbon atoms, or an aryl group having 6-20 carbon atoms; R4, R5, R9 and R10 each independently represent an alkyl group having 1-20 carbon atoms, an alkenyl or alkynyl group having 2-20 carbon atoms, an alkenylalkyl or alkynylalkyl group having 3-20 carbon atoms, or an aryl group having 6-20 carbon atoms. These carbosilanes and polycarbosilanes per se are useful as industrial materials, but they are also usable as materials for polymers as a macromonomer.
摘要翻译：本发明提供由以下通式（1）表示的碳硅烷，使用有机典型金属化合物作为引发剂通过聚合反应合成的聚碳硅烷及其制备方法。其中M表示Sn，Ge或Pb原子; A表示具有2-10个碳原子的脂族基团，碳环基团或含有选自硅，氧，氮和硫原子的一个或多个原子的杂环基，两个基团具有6-30个碳原子; R1，R2，R3，R6，R7和R8各自独立地表示具有1-20个碳原子的烷基，具有2-20个碳原子的烯基或炔基或具有6-20个碳原子的芳基; R4，R5，R9和R10各自独立地表示具有1-20个碳原子的烷基，具有2-20个碳原子的烯基或炔基，具有3-20个碳原子的链烯基烷基或炔基烷基，或具有6个 -20个碳原子。这些碳硅烷和聚碳硅烷本身可用作工业材料，但它们也可用作聚合物作为大分子单体的材料。

76. 发明申请

US20020026026A1 Linear and branched chemoselective siloxane polymers and methods for use in analytical and purification applications 有权
标题翻译：线性和分支化学选择性硅氧烷聚合物和用于分析和纯化应用的方法
公开(公告)号：US20020026026A1
公开(公告)日：2002-02-28
申请号：US09895293
申请日：2001-07-02
发明人： Robert Andrew McGill , Eric J. Houser , Todd Misna
IPC分类号： C08G077/00
CPC分类号： C08G77/24 , B01J20/285 , C08G77/60 , C08L83/16 , Y10T428/31663 , Y10T436/163333 , Y10T436/17
摘要： This invention relates generally to a new class of chemoselective polymer materials. In particular, the invention relates to linear and branched polysiloxane compounds for use in various analytical applications involving sorbent polymer materials, including chromatography, chemical trapping, analyte collection, and chemical sensor applications. These polymers have pendant and terminal aryl, alkyl, alkenyl, and alkynyl groups that are functionalized with halogen substituted alcohol or halogen substituted phenol groups, having the general structure: 1 wherein: n is an integer greater than 1; wherein at least one of R1 and R2 includes an alkyl, alkenyl, alkynyl, or aryl group having at least one halogen substituted alcohol or halogen substituted phenol group attached thereto; wherein any said R1 and R2 aryl groups are attached to said nullSinullOnullnulln, the polymer backbone, directly or through a short hydrocarbon chain; wherein any remaining R1 or R2 group is an alkyl, alkenyl, alkynyl, or aryl group having between one and sixteen carbons; and Z is a polymer end group independently selected from the group consisting of saturated hydrocarbons, unsaturated hydrocarbons, alkyl silanes, aryl silanes, hydroxyl, hydride, alkoxides, halogen substituted alcohol, halogen substituted phenol, and combinations thereof. These polymeric materials are primarily designed to sorb hydrogen bond basic analytes such as organophosphonate esters (nerve agents and precursors) and nitro-substituted compounds (explosives).
摘要翻译：本发明一般涉及一类新的化学选择性聚合物材料。特别地，本发明涉及用于涉及吸收剂聚合物材料的各种分析应用中的直链和支链聚硅氧烷化合物，包括色谱法，化学捕获法，分析物收集法和化学传感器应用。这些聚合物具有用卤素取代的醇或卤素取代的酚基官能化的侧链和末端芳基，烷基，烯基和炔基，其具有以下通式：其中：n是大于1的整数; 其中R1和R2中的至少一个包括具有至少一个卤素取代的醇或卤素取代的苯酚基的烷基，烯基，炔基或芳基; 其中任何所述R 1和R 2芳基直接或通过短的烃链连接到所述[Si-O-] n，所述聚合物骨架上; 其中任何剩余的R 1或R 2基团是具有1至16个碳原子的烷基，烯基，炔基或芳基; Z是独立地选自饱和烃，不饱和烃，烷基硅烷，芳基硅烷，羟基，氢化物，醇盐，卤素取代的醇，卤素取代的酚及其组合的聚合物端基。这些聚合物材料主要设计用于吸附氢键碱性分析物，如有机膦酸酯（神经试剂和前体）和硝基取代的化合物（爆炸物）。

77. 发明授权

US06174982B1 Process for the preparation of polysilanes 有权
标题翻译：制备聚硅烷的方法
公开(公告)号：US06174982B1
公开(公告)日：2001-01-16
申请号：US09331441
申请日：1999-06-22
申请人： Ryoichi Nishida , Shinichi Kawasaki , Hiroaki Murase
发明人： Ryoichi Nishida , Shinichi Kawasaki , Hiroaki Murase
IPC分类号： C08G7708
CPC分类号： C08G77/60
摘要： A method for producing polysilanes comprising subjecting a dihalosilane of the general formula (wherein m is 1 to 3; R represents hydrogen atom, alkyl group, aryl group, alkoxy group, amino group or silyl group and two Rs are the same or different in case of m=1, four Rs are the same or at least two of them are different in case of m=2 and six Rs are the same or at least two of them are different in case of m=3; X represents halogen atom) to the action of Mg or Mg alloy in an aprotic solvent in the presence of Li salt and metal halide, thereby producing polysilane represented by the general formula (wherein R is as defined above corresponding to the starting material; n is 2 to 1000).
摘要翻译：一种制造聚硅烷的方法，包括使通式（其中m为1至3; R表示氢原子，烷基，芳基，烷氧基，氨基或甲硅烷基）的二卤代硅烷和两个R 2相同或不同， m = 1的情况下，在m = 2的情况下，4个Rs相同或至少2个不同，6个Rs相同或者在m = 3的情况下至少2个不同; X表示卤素原子）在Li盐和金属卤化物的存在下，在非质子溶剂中对Mg或Mg合金的作用，由此制备由通式表示的聚硅烷（其中R如上定义，对应于起始原料; n为2至1000）。

78. 发明授权

US06174615B1 Composite of polysilamine and strong acid 失效
标题翻译：聚酰胺和强酸复合
公开(公告)号：US06174615B1
公开(公告)日：2001-01-16
申请号：US09301845
申请日：1999-04-29
申请人： Naoya Ogata
发明人： Naoya Ogata
IPC分类号： H01M810
CPC分类号： H01M4/926 , C08G77/60 , C08G77/62 , H01M8/1004 , H01M8/103 , H01M8/1037 , H01M8/1048 , H01M8/1072 , Y02P70/56 , Y10T428/31663
摘要： A composite comprising a polysilamine having a repeating unit represented by the following formula [—N(R1)—A1—Si(R2)(R3)—B—] wherein R1, R2 and R3 are the same or different and each is a hydrogen atom or a lower alkyl group; A1 is a lower alkylene group which may be substituted by a lower alkyl group, a group represented by the formula —A2—N(R4)—A3— or a group represented by the formula —A2—N(R4)—A3—N(R5)—A4—, wherein A2, A3 and A4 are the same or different and each is a lower alkylene group which may be substituted by a lower alkyl group; R4 and R5 are the same or different and each is a hydrogen atom or lower alkyl groups; B is a lower alkylene group which may be substituted by a lower alkyl group; and n is an integer of not less than 2, and a strong acid is disclosed. This composite has proton conductivity and is thus suitably used as an electrolyte membrane of a fuel cell.
摘要翻译：包含具有由下列化学式由R 1，R 2和R 3表示的重复单元的聚酰胺的复合物相同或不同，各自为氢原子或低级烷基; A 1为可被低级烷基取代的低级亚烷基由式-A2-N（R4）-A3表示的基团或由式-A2-N（R4）-A3-N（R5）-A4-表示的基团，其中A2，A3和A4为相同或不同，各自为可被低级烷基取代的低级亚烷基; R4和R5相同或不同，分别为氢原子或低级烷基; B为低级亚烷基，可以被低级烷基; andn为不小于2的整数，并且公开了强酸。该复合体具有质子传导性，因此适合用作燃料电池的电解质膜。

79. 发明授权

US6140449A Crosslinkable silicon polymer compositions 失效
标题翻译：可交联硅聚合物组合物
公开(公告)号：US6140449A
公开(公告)日：2000-10-31
申请号：US236589
申请日：1999-01-26
申请人： Shigeru Mori , Eiichi Tabei
发明人： Shigeru Mori , Eiichi Tabei
IPC分类号： C08K5/10 , C08G77/60 , C08K5/14 , C08K5/23 , C08L83/16 , C09D183/16 , C08G77/08
CPC分类号： C08G77/60 , C09D183/16
摘要： A crosslinkable silicon polymer composition is provided comprising (A) a silicon polymer containing Si--Si bonds and Si--H groups and having a Mn of 500-500,000, (B) a polyfunctional aromatic carboxylic acid allyl ester, and (C) an organic peroxide or azo compound. The composition cures into a crosslinked polysilane film which is solvent insoluble, tough, and abrasion resistant.
摘要翻译：提供一种可交联的硅聚合物组合物，其包含（A）包含Si-Si键和Si-H基并具有500-500,000的Mn的硅聚合物，（B）多官能芳族羧酸烯丙基酯和（C）有机过氧化物或偶氮化合物。该组合物固化成溶剂不溶性，韧性和耐磨性的交联聚硅烷膜。

80. 发明授权

US6136940A Silacyclobutane compounds, methods of preparing same, and polymers formed therefrom 失效
标题翻译：硅环丁烷化合物，其制备方法和由其形成的聚合物
公开(公告)号：US6136940A
公开(公告)日：2000-10-24
申请号：US298389
申请日：1999-04-23
申请人： Norbert Auner , Martin Grasmann
发明人： Norbert Auner , Martin Grasmann
IPC分类号： C07F7/12 , C07F7/14 , C08G77/20 , C08G77/60 , C08G77/06
CPC分类号： C08G77/60 , C08G77/20
摘要： A silacyclobutane compound having the formula: ##STR1## wherein R.sup.1 and R.sup.2 are independently chloro, triorganosiloxy, organooxy, triorganosilyl, or a monovalent hydrocarbon group; R.sup.3 is a monovalent hydrocarbon group free of conjugated aliphatic unsaturation, triorganosilyl, or hydrogen; and R.sup.4 is a monovalent saturated hydrocarbon group; provided that when R.sup.3 is hydrogen, neither R.sup.1 nor R.sup.2 is chloro or organooxy. Methods of preparing the silacyclobutane compounds, silane polymers containing at least one silacyclobutane unit, and siloxane polymers containing at least one silacyclobutane unit.
摘要翻译：具有下式的硅环丁烷化合物：其中R 1和R 2独立地是氯，三有机甲硅烷氧基，有机氧基，三有机甲硅烷基或一价烃基; R3是不含共轭脂族不饱和键，三有机甲硅烷基或氢的一价烃基; R4是一价饱和烃基; 条件是当R 3是氢时，R 1和R 2都不是氯或有机氧基。制备硅环丁烷化合物的方法，含有至少一个硅环丁烷单元的硅烷聚合物和含有至少一个硅环丁烷单元的硅氧烷聚合物。

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