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71. 发明申请

US20080194887A1 SEPARATION OF FLUOROUS COMPOUNDS 审中-公开
标题翻译：氟化合物的分离
公开(公告)号：US20080194887A1
公开(公告)日：2008-08-14
申请号：US12047717
申请日：2008-03-13
申请人： DENNIS P. CURRAN , MASATO MATSUGI , MARVIN S. YU
发明人： DENNIS P. CURRAN , MASATO MATSUGI , MARVIN S. YU
IPC分类号： C07C17/013
CPC分类号： C07C17/263 , C07B39/00 , C07C17/38 , C07C21/18 , C07C22/08 , C07C67/56 , Y10T436/13 , Y10T436/19 , C07C69/63
摘要： A method of separating at least a first non-fluorous compound from a mixture of compounds including at least the first non-fluorous compound and a second fluorous compound includes: charging the of compounds to a non-fluorous solid (stationary) phase and eluting with a fluorous eluting fluid (mobile phase). In one embodiment, the non-fluorous solid phase is polar in nature. The method can further include a second phase elution with a suitable organic solvent. A method conducting a chemical reaction, includes: mixing at least a first fluorous compound and a second compound, the first fluorous compound differing in fluorous nature from the second compound; exposing the first mixture to conditions to convert at least one of the first fluorous compound and the second compound to give a second mixture containing at least a third compound, charging the second mixture to a non-fluorous solid phase; and eluting with a fluorous fluid
摘要翻译：从至少包含第一非氟化合物和第二氟化合物的化合物的混合物中分离至少第一非氟化合物的方法包括：将化合物装入非氟固体（固定）相，并用氟洗脱液（流动相）。在一个实施方案中，非氟固体本质上是极性的。该方法还可以包括用合适的有机溶剂进行第二相洗脱。进行化学反应的方法包括：将至少第一氟化合物和第二化合物混合，所述第一氟化合物与所述第二化合物不同; 将第一混合物暴露于转化至少一种第一种氟化合物和第二种化合物的条件以产生含有至少第三种化合物的第二混合物，将第二种混合物装入非氟固体; 并用氟液洗脱

72. 发明授权

US07364908B2 Separation of fluorous compounds 有权
标题翻译：氟化合物的分离
公开(公告)号：US07364908B2
公开(公告)日：2008-04-29
申请号：US10870514
申请日：2004-06-17
申请人： Dennis P. Curran , Masato Matsugi , Marvin S. Yu
发明人： Dennis P. Curran , Masato Matsugi , Marvin S. Yu
IPC分类号： G01N37/00 , G01N33/22 , C07C19/08 , C07C17/266
CPC分类号： C07C17/263 , C07B39/00 , C07C17/38 , C07C21/18 , C07C22/08 , C07C67/56 , Y10T436/13 , Y10T436/19 , C07C69/63
摘要： A method of separating at least a first non-fluorous compound from a mixture of compounds including at least the first non-fluorous compound and a second fluorous compound includes: charging the of compounds to a non-fluorous solid (stationary) phase and eluting with a fluorous eluting fluid (mobile phase). In one embodiment, the non-fluorous solid phase is polar in nature. The method can further include a second phase elution with a suitable organic solvent. A method conducting a chemical reaction, includes: mixing at least a first fluorous compound and a second compound, the first fluorous compound differing in fluorous nature from the second compound; exposing the first mixture to conditions to convert at least one of the first fluorous compound and the second compound to give a second mixture containing at least a third compound, charging the second mixture to a non-fluorous solid phase; and eluting with a fluorous fluid.
摘要翻译：从至少包含第一非氟化合物和第二氟化合物的化合物的混合物中分离至少第一非氟化合物的方法包括：将化合物装入非氟固体（固定）相并用氟洗脱液（流动相）。在一个实施方案中，非氟固体本质上是极性的。该方法还可以包括用合适的有机溶剂进行第二相洗脱。进行化学反应的方法包括：将至少第一氟化合物和第二化合物混合，所述第一氟化合物与所述第二化合物不同; 将第一混合物暴露于转化至少一种第一种氟化合物和第二种化合物的条件以产生含有至少第三种化合物的第二混合物，将第二种混合物装入非氟固体; 并用氟液洗脱。

73. 发明授权

US07288684B1 Process for the direct production of methanol from methane 有权
标题翻译：从甲烷直接生产甲醇的方法
公开(公告)号：US07288684B1
公开(公告)日：2007-10-30
申请号：US11560960
申请日：2006-11-17
申请人： Timothy A. Brandvold , Joseph A. Kocal
发明人： Timothy A. Brandvold , Joseph A. Kocal
IPC分类号： C07C27/12
CPC分类号： C07C29/48 , C07C29/095 , C07C29/80 , C07C67/035 , C07C69/63 , C07C31/04
摘要： A process for the production of methanol from methane has been developed. The process involves reacting methane with an oxidant such as oxygen or a peroxide in the presence of a catalyst and a solvent in a reaction zone to produce an effluent stream comprising a methanol product. The effluent stream is next separated into a gaseous stream comprising unreacted methane and carbon dioxide and a liquid stream comprising the methanol product and solvent. Next the gaseous stream is further separated to provide a methane stream which is recycled to the reaction zone. Finally, a methanol stream is isolated and a solvent stream is recycled to the reaction zone.
摘要翻译：已经开发了从甲烷生产甲醇的方法。该方法包括在反应区中在催化剂和溶剂存在下使甲烷与氧化剂如氧或过氧化物反应，以产生包含甲醇产物的流出物流。然后将流出物流分离成包含未反应的甲烷和二氧化碳的气流以及包含甲醇产物和溶剂的液体流。接下来，进一步分离气流以提供甲烷流，其被再循环到反应区。最后，分离甲醇流，将溶剂流再循环到反应区。

74. 发明授权

US07247747B2 Process for preparing R-(-)carnitine from S-(-)-chlorosuccinic acid or from a derivative thereof 失效
标题翻译：从S - （ - ） - 氯代琥珀酸或其衍生物制备R - （ - ）肉碱的方法
公开(公告)号：US07247747B2
公开(公告)日：2007-07-24
申请号：US11175356
申请日：2005-07-07
申请人： Piero Melloni , Alberto Cerri , Marco Santagostino
发明人： Piero Melloni , Alberto Cerri , Marco Santagostino
IPC分类号： C07C55/00 , C07C55/02
CPC分类号： C07C309/66 , C07B2200/07 , C07C51/377 , C07C51/48 , C07C51/56 , C07C69/63 , C07C227/08 , C07C227/32 , C07C55/32 , C07C229/22
摘要： An inner salt of L-carnitine is prepared by reduction, with a suitable reducing agent, of a compound of formu (I): where X1 and X2, which may be the same or different, are hydroxy, C1-C4 alkoxy, phenoxy, halogen, or X1 and X2, when taken together are an oxygen atom and the resulting compound is a derivative of succinic anhydride; Y is halogen, a mesyloxy or a tosyloxy group, and subsequent treatment with water, then with a base and then with trimethylamine.
摘要翻译：通过用合适的还原剂还原formu（I）化合物制备左旋肉碱的内盐，其中X 1和X 2可以是相同或不同，为羟基，C 1 -C 4烷氧基，苯氧基，卤素或X 1和X 2 当一起是氧原子并且所得化合物是琥珀酸酐的衍生物时; Y是卤素，甲磺酰氧基或甲苯磺酰氧基，然后用水处理，然后用碱，然后用三甲胺处理。

75. 发明授权

US07195752B2 Surfactant compounds and uses thereof 失效
标题翻译：表面活性剂化合物及其用途
公开(公告)号：US07195752B2
公开(公告)日：2007-03-27
申请号：US10485595
申请日：2002-08-02
申请人： Istvan Kaldor , Brian Edgar Looker , Christopher James Lunniss , Alison Judith Redgrave
发明人： Istvan Kaldor , Brian Edgar Looker , Christopher James Lunniss , Alison Judith Redgrave
IPC分类号： A61K9/12 , A61K9/14 , A61K31/05 , A61K31/56 , A61K47/00 , A61K47/06 , C07C59/00
CPC分类号： A61K9/008 , A61K31/137 , A61K31/56 , A61K47/12 , C07C59/135 , C07C69/63 , C07C69/708 , C09K3/30
摘要： A pharmaceutical aerosol formulation that includes a particulate medicament, one or more fluorocarbon or hydrogen-containing fluorocarbon propellants and a compound of the general formula (I) or a salt or solvate thereof is disclosed, wherein A represents a straight chain C1-16 alkylene substituted by n groups of formula B; n represents an integer 1 to 3; and B independently represents C1-4 fluoroalkylC0-6 alkylene-, C1-4 fluoroalkylC0-6 alkylene-O—, or C1-4 alkylC0-6 alkylene-O— wherein at least one substituent of formula B contains at least one fluorine atom and each C1-4 fluoroalkyl- moiety contains one or more fluorine atoms but not more than 3 consecutive perfluorinated carbon atoms. Compounds of formula (I) and uses of such compounds are also disclosed.
摘要翻译：一种药物气溶胶制剂，其包含颗粒药物，一种或多种含氟碳或含氢碳氟化合物推进剂和通式（I）的化合物，

76. 发明授权

US07193106B2 Halogenoacetoxyadamantane derivatives and process for production thereof 有权
标题翻译：卤代乙酰氧基金刚烷衍生物及其制备方法
公开(公告)号：US07193106B2
公开(公告)日：2007-03-20
申请号：US10511600
申请日：2003-04-28
申请人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
发明人： Kouichi Kodoi , Shinji Tanaka , Toshihide Yoshitome
IPC分类号： C07C69/03
CPC分类号： C07C69/63 , C07C67/14 , C07C2603/74
摘要： Provided are a novel halogenoacetoxyadamantane derivative which is useful as a modifying agent for a resin for a photoresist and a dry etching resistance-improving agent in the photolithography field, agricultural and medical intermediates and a compound for other various industrial products and a process for producing the same. To be specific, provided are a halogenoacetoxyadamantane derivative having a halogenoacetoxy group in an adamantane skeleton and a process for producing a halogenoacetoxyadamantane derivative, comprising the step of reacting a hydroxyl group of an adamantane skeleton with halogenoacetic halide or reacting the above hydroxyl group with a lithiation agent to derive it into a lithiumoxy group and then reacting halogenoacetic halide to introduce a halogenoacetoxy group.
摘要翻译：提供了一种新的卤代乙酰氧基金刚烷衍生物，其可用作光刻胶树脂中的改性剂和光刻领域中的耐干蚀刻性改进剂，农业和医疗中间体以及其它各种工业产品的化合物和用于制备相同。具体而言，提供在金刚烷骨架中具有卤代乙酰氧基的卤代乙酰氧基金刚烷衍生物和卤代乙酰氧基金刚烷衍生物的制造方法，包括使金刚烷骨架的羟基与卤代乙酰卤反应或使上述羟基与锂化反应的步骤将其衍生为锂氧基，然后使卤代乙酰卤反应引入卤代乙酰氧基。

77. 发明授权

US07161025B2 Method for producing a fluorinated ester compound 有权
标题翻译：氟化酯化合物的制造方法
公开(公告)号：US07161025B2
公开(公告)日：2007-01-09
申请号：US11105518
申请日：2005-04-14
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
IPC分类号： C07C69/63
CPC分类号： C07C67/287 , C07C41/06 , C07C51/60 , C07C67/14 , C07C67/297 , C07C53/50 , C07C53/46 , C07C59/135 , C07C69/708 , C07C69/63 , C07C43/178
摘要： The present invention provides a method for producing industrially useful fluorine-containing compounds such as a fluorinated ester compound and an acid fluoride compound.Namely, the present invention resides in a method for producing a fluorinated ester compound, which comprises fluorinating an ester compound which is an ester of a compound having hydroxyl group(s) with a compound having acyl fluoride group(s) and which has a structure which can be fluorinated, in a liquid phase to produce a fluorinated ester compound, wherein the fluorination is carried out in the form of a liquid mixture of the ester compound and the compound having acyl fluoride group(s).
摘要翻译：本发明提供了一种制造工业上有用的含氟化合物如氟化酯化合物和酰氟化合物的方法。即，本发明涉及氟化酯化合物的制造方法，其特征在于，将具有羟基的化合物的酯化合物与具有酰氟基的化合物氟化，并且具有结构其可以在液相中被氟化以产生氟化酯化合物，其中氟化是以酯化合物和具有酰氟基团的化合物的液体混合物的形式进行的。

78. 发明授权

US07145035B2 Methods of ortho alkylation 失效
标题翻译：邻位烷基化方法
公开(公告)号：US07145035B2
公开(公告)日：2006-12-05
申请号：US10468637
申请日：2002-03-14
申请人： Gary David Annis , Richard James Brown , Albert Loren Casalnuovo , Stephen Ernest Jacobson , Philip Osborne Moss
发明人： Gary David Annis , Richard James Brown , Albert Loren Casalnuovo , Stephen Ernest Jacobson , Philip Osborne Moss
IPC分类号： C07C313/00 , C07D211/72
CPC分类号： C07D213/73 , C07C67/297 , C07C68/06 , C07C209/68 , C07C211/52 , C07C213/08 , C07C227/16 , C07C231/12 , C07C231/14 , C07C233/25 , C07C317/28 , C07C319/14 , C07C323/29 , C07C381/10 , C07D213/64 , C07D213/68 , C07D213/75 , C07D213/76 , C07C69/017 , C07C69/24 , C07C69/96 , C07C233/15 , C07C69/63 , C07C69/157 , C07C69/16
摘要： The present invention pertains to methods for preparing a compound of Formula (I), wherein A is O or N-L; each L is independently H or an acyl group; K is, together with the two contiguous linking carbon atoms, a phenyl ring, a 5- or 6-membered heteroaromatic ring or an aromatic 8-, 9- or 10-membered fused carbobicyclic or heterobicyclic ring system wherein each ring or ring system is optionally substituted; R1 is H, C1 to C4 alkyl or CO2R3; R2 is H or C1 to C4 alkyl; and R3 is C1 to C4 alkyl; comprising hydrogenating a compound of Formula (II), wherein n is 0, 1 or 2 in the presence of a catalyst comprising palladium to form the compound of Formula (I). This invention further pertains to methods for preparing compounds of Formula (II) useful for preparing compounds of Formula (I). This invention also pertains to compounds used in these methods
摘要翻译：本发明涉及制备式（I）化合物的方法，其中A为O或N-L; 每个L独立地是H或酰基; K与两个相邻的连接碳原子连同苯环，5或6元杂芳环或芳族8,9-或10元稠合的碳双环或杂双环系统，其中每个环或环系是任选取代; R 1是H，C 1至C 4烷基或CO 2 R 3 O 3 >; R 2是H或C 1至C 4烷基; 且R 3是C 1至C 4烷基的C 1至C 4。包括在包含钯的催化剂存在下氢化式（II）化合物，其中n为0,1或2，以形成式（I）化合物。本发明还涉及制备可用于制备式（I）化合物的式（II）化合物的方法。本发明还涉及用于这些方法的化合物

79. 发明申请

US20060116527A1 Method for fabricating a high specific surface area mesoporous alumina 有权
标题翻译：高比表面积中孔氧化铝的制造方法
公开(公告)号：US20060116527A1
公开(公告)日：2006-06-01
申请号：US11242836
申请日：2005-10-05
申请人： Tz-Bang Du , Yung-Chan Lin , Bor-Wen Chen , Shyue-Ming Jang
发明人： Tz-Bang Du , Yung-Chan Lin , Bor-Wen Chen , Shyue-Ming Jang
IPC分类号： C01F7/36 , C07C69/34
CPC分类号： C07C69/63 , C01F7/36 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要： A method for fabricating a high specific surface area mesoporous alumina is disclosed, which includes the following steps: (a) providing a water solution containing an aluminum salt and a fluoro-surfactant; (b) adding concentrated hydrochloric acid to adjust the PH value of the solution to about 6.0 to 8.0; (c) aging the solution at 70° C. to 110° C. for 12 to 20 hours; (d) washing the precipitate with water; (e) washing the precipitate with an organic solvent; (f) drying the precipitate; and (g) sintering the precipitate in a furnace of 500° C. to 1000° C.
摘要翻译：公开了一种制造高比表面积中孔氧化铝的方法，其包括以下步骤：（a）提供含有铝盐和氟表面活性剂的水溶液; （b）加入浓盐酸将溶液的PH值调节至6.0〜8.0左右; （c）将溶液在70℃至110℃下老化12至20小时; （d）用水洗涤沉淀物; （e）用有机溶剂洗涤沉淀; （f）干燥沉淀物; 和（g）在500℃至1000℃的炉中烧结沉淀物

80. 发明授权

US07053238B2 Process for producing fluorinated polyvalent carbonyl compound 失效
公开(公告)号：US07053238B2
公开(公告)日：2006-05-30
申请号：US10891155
申请日：2004-07-15
申请人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
发明人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
IPC分类号： C07C69/63
CPC分类号： C07C67/14 , C07C45/54 , C07C51/60 , C07C67/287 , C07C67/29 , C07C67/297 , C07C67/307 , C07C59/21 , C07C53/46 , C07C69/63
摘要： A fluorinated polyvalent carbonyl compound is produced by an economically advantageous method from inexpensive materials without requiring a complicated synthetic process step. Namely, the present invention comprises reacting a polyvalent alcohol having at least two kinds of alcohol skeletons selected among a primary alcohol, a secondary alcohol and a tertiary alcohol, with an acid halide to obtain a polyvalent ester compound, fluorinating it in a liquid phase to obtain a perfluorinated polyvalent ester compound, and cleaving the ester bonds derived from primary and secondary alcohols in the perfluoropolyvalent ester compound to obtain a fluorinated polyvalent carbonyl compound.

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