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61. 发明授权

US09945008B2 Treatment method of chlorine-containing zinc oxide secondary material 有权
公开(公告)号：US09945008B2
公开(公告)日：2018-04-17
申请号：US14907579
申请日：2014-07-03
申请人： YUNNAN XIANGYUNFEILONG RESOURCES RECYCLING TECHNOLOGY CO., LTD.
发明人： Yuzhang Shu , Qi Zhang , Guifen Yang , Baohua Sun , Linkui Wei
IPC分类号： C22B26/00 , C22B26/10 , C22B19/30 , C22B7/00 , C22B3/00 , C25C1/16 , C22B3/38
CPC分类号： C22B26/10 , C22B3/005 , C22B7/007 , C22B19/22 , C22B19/30 , C25C1/16 , Y02P10/234
摘要： The invention discloses a treatment method of a chlorine-containing zinc oxide secondary material, which comprises the following steps: 1) leaching the chlorine-containing zinc oxide secondary material I through an acid solution; 2) selectively extracting zinc through di-(2-ethylhexyl)phosphoric acid (P204)-kerosene solvent; 3) implementing stripping-electrolysis zinc recovery; 4) repeating steps 1)-4); 5) taking out the raffinate obtained from the Step (4), mixing the residual taken out raffinate with chlorine-containing zinc oxide secondary material II when balance on chlorine ion input and taking out is achieved; carrying out liquid-solid separation; leaching the separated deposit through acid raffinate of the step 1); 6) after separated solution achieves preset conditions, purifying the chlorine-containing aqueous phase; 7) evaporating and concentrating to crystallize out KCl and NaCl products. The invention is environment-friendly and energy-saving, and free from process wastewater emission; production cost is greatly reduced and secondary pollution of the current dechloridation process is eliminated thoroughly.

62. 发明授权

US07753987B2 High vacuum in-situ refining method for high-purity materials and an apparatus thereof 失效
标题翻译：用于高纯度材料的高真空原位精制方法及其装置
公开(公告)号：US07753987B2
公开(公告)日：2010-07-13
申请号：US12067835
申请日：2006-04-11
申请人： Xiaolong Du , Zhaoquan Zeng , Hongtao Yuan , Handong Li , Qikun Xue , Jinfeng Jia
发明人： Xiaolong Du , Zhaoquan Zeng , Hongtao Yuan , Handong Li , Qikun Xue , Jinfeng Jia
IPC分类号： C22B9/04 , C22B9/05 , C22B26/00 , C22B30/04
CPC分类号： C22B9/02 , C22B9/04 , C22B9/14 , C22B19/12 , C22B19/18 , F27B14/04 , F27B14/20 , Y02P10/234
摘要： The present invention concerns a high vacuum in-situ refining method for high-purity and superhigh-purity materials and the apparatus thereof, characterized in heating the upper part and lower part of crucible separately using double-heating-wires diffusion furnace under vacuum, thereby forming the temperature profile which is high at upper part and low at lower part of crucible, or in reverse during different stages; then heating the crucible in two steps to remove impurities with high saturation vapor pressure and low saturation vapor pressure respectively in efficiency; and obtaining high-purity materials eventually. The whole procedure is isolated from atmosphere, reducing contamination upon stuff remarkably. The present invention could provide products with high-quality and high production capacity, which are stable in performance, therefore is reliable and free from contamination. The present invention is appropriate for manufacture of high-purity and superhigh-purity materials, particularly for manufacture of high-activity high-purity materials.
摘要翻译：本发明涉及一种用于高纯度和超高纯度材料的高真空原位精制方法及其装置，其特征在于使用双重加热丝扩散炉在真空下分别加热坩埚的上部和下部，由此形成坩埚上部和下部较高的温度分布，或在不同阶段形成相反的温度分布; 然后分两步加热坩埚以分别以高饱和蒸气压和低饱和蒸气压去除杂质; 并最终获得高纯度材料。整个过程与大气隔离，减少了污染物的显着。本发明可以提供具有高质量和高生产能力的产品，性能稳定，因此可靠，无污染。本发明适用于制造高纯度和超高纯度材料，特别是用于制造高活性高纯度材料。

63. 发明申请

US20080000647A1 Non-Ferrous Metal Cover Gases 审中-公开
标题翻译：有色金属盖气
公开(公告)号：US20080000647A1
公开(公告)日：2008-01-03
申请号：US11691296
申请日：2007-03-26
申请人： Matthew H. Luly , Rajiv R. Singh
发明人： Matthew H. Luly , Rajiv R. Singh
IPC分类号： A62C3/06 , C09K21/10 , C22B21/00 , C22B26/00
CPC分类号： C22B9/006 , A62D1/0092 , C22B21/064 , C22B26/22 , Y02P10/122
摘要： Disclosed are cover gas compositions comprising at least one pentafluoropropane for impeding the oxidation of molten nonferrous metals and alloys, such as magnesium.
摘要翻译：公开了包含至少一种用于阻止熔融的有色金属和合金如镁的氧化的五氟丙烷的覆盖气体组合物。

64. 发明申请

US20070071665A1 Use of a derivative of aspartic acid as a collector in froth flotation processes 失效
标题翻译：在泡沫浮选过程中使用天冬氨酸的衍生物作为收集剂
公开(公告)号：US20070071665A1
公开(公告)日：2007-03-29
申请号：US10578106
申请日：2004-11-05
申请人： Ludwig Eisenhuth , Elisabeth Henriksson , Anders Klingberg
发明人： Ludwig Eisenhuth , Elisabeth Henriksson , Anders Klingberg
IPC分类号： C22B26/00
CPC分类号： B03D1/021 , B03D1/0043 , B03D1/01 , B03D1/06 , B03D2201/02 , B03D2203/06 , C07C229/24
摘要： A derivative of aspartic acid is used as a collector for a phosphate containing mineral, such as apatite, in a froth flotation process. According to the invention the collector has a high selectivity for phosphate containing minerals even in the presence of carbonate minerals, such as calcite. The derivative has the formula (1) where RI is a hydrophobic group containing a hydrocarbon group of 6-24 carbon atoms; RII is an alkyl group with 1-7 carbon atoms or a group of the formula (B)yH, in which B is an alkyleneoxy group with 24 carbon atoms and y is a number from 1 to 10; and M is a group selected from the group consisting of a cation or hydrogen. Methods for producing the derivative are also described.
摘要翻译：在泡沫浮选过程中，天冬氨酸的衍生物用作含磷酸盐矿物如磷灰石的收集剂。根据本发明，即使在碳酸盐矿物如方解石的存在下，收集器也对含磷酸盐的矿物具有高选择性。该衍生物具有式（1），其中R 1是具有6-24个碳原子的烃基的疏水基团; R II是具有1-7个碳原子的烷基或式（B）的基团，其中B是具有24个碳原子的亚烷基氧基，和 y是从1到10的数字; 并且M是选自阳离子或氢的基团。还描述了衍生物的制备方法。

65. 发明申请

US20050276737A1 Mineralization of alkali metals, sulfur, and halogens 有权
标题翻译：碱金属，硫和卤素的矿化
公开(公告)号：US20050276737A1
公开(公告)日：2005-12-15
申请号：US10374293
申请日：2003-02-26
申请人： J. Mason
发明人： J. Mason
IPC分类号： A62D3/20 , C01G1/00 , C22B7/00 , C22B7/02 , C22B7/04 , C22B26/00
CPC分类号： C04B7/24 , C22B7/001 , C22B7/002 , C22B7/02 , C22B7/04 , C22B26/00 , Y02P10/214 , Y02P40/145
摘要： A system and method for conversion of alkali metals, heavy metals, halogens, and sulfur into mineral products. The system includes a single reaction vessel. To begin the process, co-reactants such as lime and clay are mixed with waste feeds containing alkali metals, heavy metals, halogens, and sulfur. This mixture is then introduced into the reaction vessel. The reaction vessel is operated under reducing conditions. After the mineral products are allowed to form, they are collected from the reaction vessel.
摘要翻译：将碱金属，重金属，卤素和硫转化成矿物产品的系统和方法。该系统包括单个反应容器。为了开始该过程，将诸如石灰和粘土的共反应物与含有碱金属，重金属，卤素和硫的废料混合。然后将该混合物引入反应容器中。反应容器在还原条件下运行。允许矿物形成后，从反应容器中收集。

66. 发明申请

US20050211955A1 Cesium and strontium extraction using a mixed extractant solvent including crown ether and calixarene extractants 失效
标题翻译：使用包括冠醚和杯芳烃萃取剂的混合萃取剂溶剂进行铯和锶萃取
公开(公告)号：US20050211955A1
公开(公告)日：2005-09-29
申请号：US10808039
申请日：2004-03-23
申请人： David Meikrantz , Terry Todd , Catherine Riddle , Jack Law , Dean Peterman , Bruce Mincher , Christopher McGrath , John Baker
发明人： David Meikrantz , Terry Todd , Catherine Riddle , Jack Law , Dean Peterman , Bruce Mincher , Christopher McGrath , John Baker
IPC分类号： C22B3/26 , C22B26/00 , C22B60/02 , C23G5/00
CPC分类号： C22B3/002 , C22B26/00 , Y02P10/234
摘要： A mixed extractant solvent including calix[4]arene-bis-(tert-octylbenzo)-crown-6 (“BOBCalixC6”), 4′,4′,(5′)-di-(t-butyldicyclo-hexano)-18-crown-6 (“DtBu18C6”), and at least one modifier dissolved in a diluent. The mixed extractant solvent may be used to remove cesium and strontium from an acidic solution. The DtBu18C6 may be present from approximately 0.01 M to approximately 0.4M, such as from approximately 0.086 M to approximately 0.108 M. The modifier may be 1-(2,2,3,3-tetrafluoropropoxy)-3-(4-sec-butylphenoxy)-2-propanol (“Cs-7SB”) and may be present from approximately 0.01M to approximately 0.8M. In one embodiment, the mixed extractant solvent includes approximately 0.15M DtBu18C6, approximately 0.007M BOBCalixC6, and approximately 0.75M Cs-7SB modifier dissolved in an isoparaffinic hydrocarbon diluent. The mixed extractant solvent may form an organic phase in an extraction system that also includes an aqueous phase. Methods of extracting cesium and strontium as well as strontium alone are also disclosed.
摘要翻译：混合萃取剂溶剂包括杯[4]芳烃双 - （叔辛基苯并） - 起始-6（“BOBCalixC6”），4'，4'，（5'） - 二 - （叔丁基二环己基） -crown-6（“DtBu18C6”）和溶解在稀释剂中的至少一种改性剂。混合的萃取剂溶剂可用于从酸性溶液中除去铯和锶。 DtBu18C6可以为约0.01M至约0.4M，例如约0.086M至约0.108M。改性剂可为1-（2,2,3,3-四氟丙氧基）-3-（4-仲 - 丁基苯氧基）-2-丙醇（“Cs-7SB”），并且可以以约0.01M至约0.8M存在。在一个实施方案中，混合萃取剂溶剂包括溶解在异链烷烃稀释剂中的约0.15M DtBu18C6，约0.007M BOBCalixC6和约0.75M Cs-7SB改性剂。混合的萃取剂溶剂可以在还包含水相的萃取系统中形成有机相。还公开了提取铯和锶以及单独的锶的方法。

67. 发明授权

US06846417B2 Co-retarding agents for preparing purified brine 有权
标题翻译：用于制备纯净盐水的助滞剂
公开(公告)号：US06846417B2
公开(公告)日：2005-01-25
申请号：US10216530
申请日：2002-08-09
申请人： Mateo Jozef Jacques Mayer , René Lodewijk Maria Demmer
发明人： Mateo Jozef Jacques Mayer , René Lodewijk Maria Demmer
IPC分类号： C01D3/06 , C01D3/16 , B01D11/02 , C22B26/00
CPC分类号： C01D3/16 , C01D3/06
摘要： The invention relates to a process to produce brine of improved purity by dissolving salt that contains a calcium sulfate source in water, in the presence of a retarding agent, while using one or more co-retardants to bind contaminants that could interfere with the retarding agents.
摘要翻译：本发明涉及通过在阻滞剂的存在下将含有硫酸钙源的盐溶解在水中来制备具有改进纯度的盐水的方法，同时使用一种或多种助阻剂来结合可能干扰阻滞剂的污染物。

68. 发明授权

US6051196A Purification of phosphorus containing scheelite ore 失效
标题翻译：含磷白钨矿的纯化
公开(公告)号：US6051196A
公开(公告)日：2000-04-18
申请号：US247745
申请日：1999-02-09
申请人： Raj P. Singh , Michael J. Miller , Thomas A. Wolfe
发明人： Raj P. Singh , Michael J. Miller , Thomas A. Wolfe
IPC分类号： C01B25/32 , C01F1/00 , C01F11/24 , C01G41/00 , C22B26/00
CPC分类号： C22B26/00 , C01F11/24
摘要： A method for purifying a phosphorus containing scheelite ore is described wherein the calcite phase is selectively dissolved prior to dissolution of the apatite phase. Selective dissolution of the calcite produces several benefits: (1) a usable calcium solution, (2) enhanced apatite dissolution, and (3) lower volumes of toxic acid solution for disposal.
摘要翻译：描述了一种纯化含磷白钨矿的方法，其中在磷灰石相溶解之前方解石相选择性溶解。方解石的选择性溶解产生几个好处：（1）可用的钙溶液，（2）增强的磷灰石溶解，和（3）较少量的有毒酸溶液的处理。

69. 发明授权

US6010672A Process for producing sodium carbonate from trona ore 失效
标题翻译：从天然碱矿石生产碳酸钠的方法
公开(公告)号：US6010672A
公开(公告)日：2000-01-04
申请号：US61363
申请日：1998-04-15
申请人： Allan L. Turner
发明人： Allan L. Turner
IPC分类号： C01D7/12 , C01D7/00 , C22B26/00
CPC分类号： C01D7/126
摘要： Disclosed is a process for the production of sodium carbonate monohydrate crystals from uncalcined trona ore. The process include contacting trona ore with a saturated sodium carbonate solution at a temperature of at least about 117.degree. C. to form a brine solution comprising anhydrous sodium carbonate crystals. The temperature of the brine solution is reduced to form sodium carbonate monohydrate crystals and the crystals are separated from the brine solution. The process can include maintaining the concentration of bicarbonate in the brine solution at a low level to promote the formation of only anhydrous sodium carbonate at temperatures above about 117.degree. C. and to promote the formation of sodium carbonate monohydrate at temperatures below about 109.degree. C.
摘要翻译：公开了一种从未煅烧的天然碱矿石生产碳酸钠一水合物晶体的方法。该方法包括在至少约117℃的温度下将天然碱与饱和碳酸钠溶液接触以形成包含无水碳酸钠晶体的盐水溶液。将盐水溶液的温度降低以形成碳酸钠一水合物晶体，并将晶体与盐水溶液分离。该方法可以包括将盐水溶液中碳酸氢盐的浓度维持在低水平，以促进在高于约117℃的温度下仅形成无水碳酸钠，并在低于约109℃的温度促进形成碳酸钠一水合物。

70. 发明授权

US5762680A Distribution system for molten magnesium 失效
标题翻译：熔融镁分配系统
公开(公告)号：US5762680A
公开(公告)日：1998-06-09
申请号：US717773
申请日：1996-09-24
申请人： Olav Holta , H.ang.kon Westengen
发明人： Olav Holta , H.ang.kon Westengen
IPC分类号： B22D45/00 , B22D17/30 , C22B26/00
CPC分类号： B22D17/30
摘要： An apparatus for distribution of magnesium or magnesium alloys from a central melting unit (2) into a casting shop with one or more casting machines (3) has a tube furnace (1) extending from a central melting unit (2) into the casting shop. The tube furnace (1) is equipped with outlets (6) at the top for the mounting of a transfer tube (7) for the supply of metal to one or more holding furnaces (4) arranged at each casting machine. The tube furnace is preferably placed inside a steel cover (8) and is positioned just beneath the metal level in the holding furnace (4). The tube furnace (1) and transfer tubes (7) are provided with heating elements (11) with an outer insulation (12). The transfer tubes (7) have an air inlet (9). Two or more tube furnaces could be placed in the steel cover (8). The metal is transferred by the act of gravity.
摘要翻译：将镁或镁合金从中央熔化单元（2）分配到具有一个或多个铸造机（3）的铸造车间中的装置具有从中心熔化单元（2）延伸到铸造车间的管式炉（1）。管式炉（1）在顶部配备有用于安装用于将金属供给到布置在每个浇铸机上的一个或多个保温炉（4）的输送管（7）的出口（6）。管式炉优选放置在钢盖（8）的内部并且位于保持炉（4）内的金属层的正下方。管式炉（1）和输送管（7）设置有具有外绝缘层（12）的加热元件（11）。输送管（7）具有空气入口（9）。两个或多个管式炉可以放置在钢盖（8）中。金属被重力作用转移。

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