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61. 发明授权

US06577802B1 Application of silane-enhanced adhesion promoters for optical fibers and fiber ribbons 有权
标题翻译：硅烷增强粘合促进剂在光纤和纤维带上的应用
公开(公告)号：US06577802B1
公开(公告)日：2003-06-10
申请号：US09616103
申请日：2000-07-13
申请人： Ching-Kee Chien
发明人： Ching-Kee Chien
IPC分类号： G02B602
CPC分类号： C03C25/1065 , C03C25/105
摘要： The present invention is directed to methods of applying an adhesion-promoting intermediary layer to an optical fiber using a carrier gas. The present invention is also directed to optical fibers and ribbons which have polymeric coatings with improved adhesion characteristics. The optical fibers comprise an adhesion-promoting intermediary layer between the cladding and primary polymeric coating which comprises a silane.
摘要翻译：本发明涉及使用载气将粘合促进中间层施加到光纤的方法。本发明还涉及具有改进的粘附特性的聚合物涂层的光纤和带。光纤在包层和初级聚合物涂层之间包含粘合促进中间层，其包含硅烷。

62. 发明授权

US06563996B1 Optical fibers prepared with a primary coating composition including a monomer with a pendant hydroxyl functional group 有权
标题翻译：用包含具有侧羟基官能团的单体的初级涂料组合物制备的光纤
公开(公告)号：US06563996B1
公开(公告)日：2003-05-13
申请号：US09712565
申请日：2000-11-14
申请人： Michael J. Winningham
发明人： Michael J. Winningham
IPC分类号： G02B602
CPC分类号： C09D4/00 , C03C25/106 , C03C25/1065 , C09D4/06 , C08F220/28 , C08F222/20 , C08F290/067
摘要： The present invention relates to an optical fiber including a glass fiber and a primary coating encapsulating and in contact with the glass fiber, the primary coating being the cured product of a polyrnerizable composition which includes a monomer with a pendant hydroxyl functional group which can bond with a surface of the optical fiber and is present in an amount effective to promote adhesion. The present invention also relates to methods of making such optical fibers.
摘要翻译：本发明涉及包含玻璃纤维和初级涂层的光纤，其包封并与玻璃纤维接触，初级涂层是可聚合组合物的固化产物，其包含具有侧基羟基官能团的单体，其可与光纤的表面并且以有效促进粘附的量存在。本发明还涉及制造这种光纤的方法。

63. 发明申请

US20030059188A1 Optical fibers possessing a primary coating with a higher degree of cure and methods of making 有权
标题翻译：具有较高固化程度的初级涂层和制造方法的光纤
公开(公告)号：US20030059188A1
公开(公告)日：2003-03-27
申请号：US10086109
申请日：2002-02-27
发明人： Linda S. Baker , John S. Peanasky
IPC分类号： G02B006/16
CPC分类号： C03C25/1065
摘要： An optical fiber including: a fiber including at least a core; a primary coating substantially encapsulating the fiber, the primary coating being the cured product of a first polymerizable composition including a first photoinitiator which absorbs light within a range of the UV spectrum; and a secondary coating substantially encapsulating the primary coating on the fiber, the secondary coating being the cured product of a second polymerizable composition including a second photoinitiator which also absorbs light within the range of the UV spectrum, wherein an average integrated intensity for the second photoinitiator is 95% or less of the average integrated intensity for the primary photoinitiator over at least a portion of the range of the UV spectrum. Also disclosed are fiber optic ribbons including the optical fibers, methods of making the optical fibers, and methods of increasing the degree of cure for a primary coating on an optical fiber.
摘要翻译：一种光纤，包括：至少包含芯的纤维; 初级涂层基本上包封纤维，初级涂层是第一可聚合组合物的固化产物，其包含在UV光谱范围内吸收光的第一光引发剂; 以及基本上将所述主涂层包封在所述纤维上的二次涂层，所述第二涂层是包含第二光引发剂的第二可聚合组合物的固化产物，所述第二光引发剂也吸收在所述UV光谱范围内的光，其中所述第二光引发剂的平均积分强度在UV光谱的范围的至少一部分上为初级光引发剂的平均积分强度的95％或更小。还公开了包括光纤的光纤带，制造光纤的方法以及增加光纤上的初级涂层的固化程度的方法。

64. 发明授权

US06531522B1 Fast curing primary optical fiber coating 失效
标题翻译：快速固化主光纤涂层
公开(公告)号：US06531522B1
公开(公告)日：2003-03-11
申请号：US09712603
申请日：2000-11-14
申请人： Michael J. Winningham
发明人： Michael J. Winningham
IPC分类号： C08F246
CPC分类号： C09D175/16 , C03C25/106 , C03C25/1065 , C09D4/00 , C09D4/06 , Y10T428/2938 , Y10T428/2942 , Y10T428/2967 , Y10T428/2987 , Y10T428/31551 , C08F220/32 , C08F222/20 , C08F290/147
摘要： The present invention relates to a coating for an optical fiber. The coating includes a monomer. The monomer includes an oxyglycidyl (meth)acrylate component. A coating with the monomeric component has exhibited an excellent polymerization rate. The present invention also relates to methods of making such optical fibers coated in accordance with the invention and the coated glass article.
摘要翻译：本发明涉及一种光纤用涂层。涂层包括单体。单体包括（甲基）丙烯酸羟基缩水甘油酯组分。具有单体组分的涂层具有优异的聚合速率。本发明还涉及制造根据本发明涂覆的这种光纤和涂覆的玻璃制品的方法。

65. 发明申请

US20030044140A1 COMPOSITION CONTAINING TACKIFIER AND METHOD OF MODIFYING TIME-SENSITIVE RHEOLOGICAL PROPERTIES OF OPTICAL FIBER COATING 失效
标题翻译：包含加热器的组合物和改性光纤涂层的时间敏感性流变性能的方法
公开(公告)号：US20030044140A1
公开(公告)日：2003-03-06
申请号：US09747044
申请日：2000-12-21
发明人： Edward J. Fewkes , Gregory F. Jacobs , Kenneth R. Jones , Huan-Hung Sheng , Frederic C. Wagner , Michael J. Winningham
IPC分类号： C08G002/00
CPC分类号： C09D4/00 , C03C25/106 , C03C25/1065 , C09D4/06 , Y10T428/2938 , C08F290/067
摘要： The present invention relates to a composition for preparing optical fiber coatings, the composition including a polymerizable base composition, containing at least one monomer and optionally at least one oligomer, wherein the polymerizable base composition is substantially free of unsaturated epoxidized diene polymers, and a tackifier present in an amount effective to modify a time-sensitive rheological property of a polymerization product of the composition. Another aspect of the present invention relates to a method of modifying a time-sensitive theological property of an optical fiber coating by introducing into a polymerizable composition a tackifier in an amount effective to modify a time-sensitive rheological property of the polymerization product of the polymerizable composition. Also disclosed are an optical fiber, a fiber optic ribbon, and a fiber bundle that contain coating(s) prepared from a composition of the present invention.
摘要翻译：本发明涉及一种用于制备光纤涂层的组合物，该组合物包括含有至少一种单体和任选的至少一种低聚物的可聚合基础组合物，其中可聚合基础组合物基本上不含不饱和环氧化二烯聚合物，和增粘剂以有效地改变组合物的聚合产物的时间敏感性流变性的量存在。本发明的另一方面涉及一种通过向可聚合组合物中引入增粘剂以有效改变可聚合的聚合物的聚合产物的时间敏感性流变性能的方式来改变光纤涂层的时间敏感的神学性质的方法组成。还公开了包含由本发明的组合物制备的涂层的光纤，光纤带和纤维束。

66. 发明申请

US20020183415A1 RADIATION-CURABLE, OPTICAL FIBER PRIMARY COATING SYSTEM 有权
标题翻译：辐射可固化，光纤主要涂层系统
公开(公告)号：US20020183415A1
公开(公告)日：2002-12-05
申请号：US09353658
申请日：1999-07-15
发明人： DAVID M. SZUM , CHANDER P. CHAWLA , JAMES R. PETISCE , GEORGE PASTERNACK , TIMOTHY E. BISHOP , PAUL E. SNOWWHITE , EDWARD P. ZAHORA
IPC分类号： C08K003/00
CPC分类号： C03C25/1065 , Y10T428/2938 , Y10T428/2942 , Y10T428/2947 , Y10T428/2962 , Y10T428/2967
摘要： Optical fiber primary coating systems are disclosed having excellent ribbon stripping and adhesion behavior. The coatings are radiation-curable. The excellent stripping and adhesion behavior can be inner piramry coating composition having a slip enhancing component and a high modulus outer primary coating composition. Combination of means can be employed. Stripping behavior can be measured by crack propagation and fiber friction measurements.
摘要翻译：公开了具有优异的带剥离和粘合行为的光纤一次涂覆系统。涂层是可辐射固化的。良好的剥离和粘合行为可以是具有滑爽增强组分和高模量外部初级涂料组合物的内部薄膜涂料组合物。可以组合手段。剥离行为可以通过裂纹扩展和纤维摩擦测量来测量。

67. 发明申请

US20020168520A1 Coated optical fiber 有权
标题翻译：涂层光纤
公开(公告)号：US20020168520A1
公开(公告)日：2002-11-14
申请号：US10056565
申请日：2002-01-25
发明人： James R. Toler , Edward J. Fewkes
IPC分类号： D02G003/00
CPC分类号： G02B6/2558 , C03C25/106 , C03C25/1065 , G02B6/4402 , Y10T428/2933 , Y10T428/2964
摘要： The disclosed coated optical fiber includes a core surrounded by a cladding. At least a segment of the fiber is coated with a photopolymerizable coating composition. The photopolymerizable coating composition is a mixture of at least about 60% of a first polyurethane acrylate coating having a Young's modulus of at least about 400 MPa and about 5-40% of a second polyurethane coating having a Young's modulus of no more than about 50 MPa. The invention further includes a method of making the coated optical fiber. The method includes the steps of blending the photopolymerizable coating composition as recited above and splicing an end section of a first optical fiber having a core and a cladding to an end section of a second optical fiber having a core and a cladding, thereby forming a resultant optical fiber. The aforementioned photopolymerizable composition is applied to the end section of the first optical fiber and the end section of the second optical fiber after the resultant fiber is formed and the composition is cured.
摘要翻译：公开的涂覆光纤包括被包层包围的芯。纤维的至少一段用可光聚合的涂料组合物涂覆。可光聚合涂料组合物是至少约60％的具有至少约400MPa的杨氏模量和约5-40％的杨氏模量不超过约50的第二聚氨酯涂层的第一聚氨酯丙烯酸酯涂层的混合物 MPa。本发明还包括制造涂覆光纤的方法。该方法包括以下步骤：将上述可光聚合涂层组合物混合并将具有芯和包层的第一光纤的端部与将芯和包层的第二光纤的端部拼接，从而形成结果光纤。在形成所得纤维并将组合物固化后，将上述可光聚合组合物施加到第一光纤的端部和第二光纤的端部。

68. 发明授权

US06438306B1 Radiation curable resin composition 有权
标题翻译：辐射固化树脂组合物
公开(公告)号：US06438306B1
公开(公告)日：2002-08-20
申请号：US09544209
申请日：2000-04-07
申请人： Timothy E. Bishop , Paul E. Snowwhite , Tyson Norlin , James J. Schouten , John Southwell , Anthony Toussaint
发明人： Timothy E. Bishop , Paul E. Snowwhite , Tyson Norlin , James J. Schouten , John Southwell , Anthony Toussaint
IPC分类号： G02B602
CPC分类号： C09D4/06 , C03C25/106 , C03C25/1065 , C08F2/50 , C08F220/32 , C08F2220/346 , C09D4/00 , C08F290/14 , C08F290/06 , C08F2220/1875
摘要： The present invention relates to a coated optical fiber comprising a glass optical fiber with a single protective coating or a combination of an inner and an outer primary coating applied thereon and optionally with a colored coating subsequently applied thereon wherein the inner primary coating or at least a portion of the single coating is prepared from a radiation curable composition which when cured as a capillary film with a 100 W medium pressure mercury lamp has a percentage reacted acrylate unsaturation of at least about 54% after exposure to a dose of about 4.4 mJ/cm2 or wherein the outer primary coating is prepared from a radiation curable composition which when cured as a capillary film with a 100 W medium pressure mercury lamp has a percentage reacted acrylate unsaturation of at least about 56% after exposure to a dose of about 4.4 mJ/cm2. The invention further relates to a radiation curable composition having a high cure speed.
摘要翻译：本发明涉及一种涂覆光纤，其包括具有单一保护涂层的玻璃光纤或其上施加有内部和外部初级涂层的组合，并且可选地随后涂覆有着色涂层，其中所述内部初级涂层或至少一个单一涂层的一部分由可辐射固化组合物制备，当用100W中压汞灯固化时，其暴露于约4.4mJ / cm 2的剂量后具有至少约54％的丙烯酸酯不饱和度的百分比或其中外部初级涂层由可辐射固化组合物制备，当用100W中压汞灯固化时，其具有至少约56％反应的丙烯酸酯不饱和度的百分比，暴露于约4.4mJ / cm2。本发明还涉及具有高固化速度的可辐射固化组合物。

69. 发明申请

US20020106173A1 ULTRAVIOLET CURABLE COATINGS FOR OPTICAL FIBER FOR WET-ON-WET APPLICATION 审中-公开
标题翻译：用于光纤光纤的超紫外线固化涂层
公开(公告)号：US20020106173A1
公开(公告)日：2002-08-08
申请号：US09739677
申请日：2000-12-20
发明人： Peter Stupak , Igor Khudyakov
IPC分类号： G02B006/22 , C08F002/50
CPC分类号： C03C25/12 , C03C25/1065 , G02B6/02033
摘要： The present invention is a method of making an optical fiber, and the fiber itself, where the primary and secondary coatings are cured simultaneously with Uv radiation. The method of making the optical fiber comprises applying the primary coating on a glass fiber (optical fiber) where the primary coating has a first photoinitiator which allows the primary coating to be cured by a first wavelength range of UV light, applying the secondary coating over the primary coating where the secondary coating contains a second photoinitiator whose UV reaction spectra is substantially different from the first photoinitiator in the primary coating and which allows the secondary coating to be cured through exposure to UV radiation in a second wavelength range of UV light, and finally by exposing the optical fiber, having the two coatings, to a UV light source which contains wavelengths in both wavelength ranges of the first and second photoinitiators, so that the primary and secondary coatings cure simultaneously. The present invention is directed to eliminating the problems of uncontrollable post-cure hardening of the coatings, that exist in present manufacturing methods, while at the same time greatly reducing the time and costs involved in making optical fibers by reducing the height of the draw tower and increasing production speeds, without compromising the quality or durability of the fiber coatings.
摘要翻译：本发明是制造光纤的方法和纤维本身，其中初级和次级涂层与Uv辐射同时固化。制造光纤的方法包括将第一涂层施加在玻璃纤维（光纤）上，其中初级涂层具有第一光引发剂，其允许初级涂层通过UV光的第一波长范围固化，施加二次涂层其中第二涂层含有第二光引发剂，其UV反应光谱与初级涂层中的第一光引发剂基本上不同，并且允许二次涂层通过在UV光的第二波长范围内暴露于UV辐射而固化，以及最后通过将具有两个涂层的光纤暴露于包含第一和第二光引发剂的两个波长范围内的波长的UV光源，使得初级和次级涂层同时固化。本发明旨在消除当前制造方法中存在的涂层不可控后固化硬化的问题，同时通过降低拉制塔的高度大大减少制造光纤所涉及的时间和成本并提高生产速度，而不损害纤维涂层的质量或耐久性。

70. 发明申请

US20020102077A1 Protective materials for optical fibers which do not substantially discolor 审中-公开
标题翻译：基本不变色的光纤保护材料
公开(公告)号：US20020102077A1
公开(公告)日：2002-08-01
申请号：US09975549
申请日：2001-10-12
发明人： David M. Szum , Adrianus G.M. Abel
IPC分类号： G02B006/44
CPC分类号： C03C25/106 , C03C25/1065 , G02B6/4403 , G02B6/4404 , G02B6/443 , G02B6/4475 , G02B6/448 , G02B6/4495 , G02B6/4498
摘要： Radiation-curable compositions are disclosed which, after cure, are substantially non-yellowing. The compositions are particularly tailored for coating and bundling of optical fibers. A first preferred composition is based on a polyether-type of oligomer diluted with reactive diluents. Isocyanurate structures are included in the composition to raise Tg. A second preferred composition is based on fatty oil comprising (meth)acrylate groups and bisphenol A derivatives comprising (meth)acrylate groups. Photoinitiators can be included to increase cure speed. The formulations do not include material amounts of ingredients which tend to cause yellowing or, in theory, extended conjugation in the cured compositions.
摘要翻译：公开了可固化的组合物，其在固化后基本上不变黄。该组合物特别适用于光纤的涂布和捆扎。第一优选的组合物是基于用活性稀释剂稀释的聚醚型低聚物。组合物中包含异氰酸酯结构以提高Tg。第二优选组合物是基于包含（甲基）丙烯酸酯基团的脂肪油和包含（甲基）丙烯酸酯基团的双酚A衍生物。可以加入光引发剂以提高固化速度。制剂不包括倾向于引起变黄的成分的物质量，或理论上在固化的组合物中延长的缀合。

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