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61. 发明申请

US20060129004A1 Process for preparing alcohols from olefins by hydroformylation and hydrogenation 有权
标题翻译：通过加氢甲酰化和氢化由烯烃制备醇的方法
公开(公告)号：US20060129004A1
公开(公告)日：2006-06-15
申请号：US11296310
申请日：2005-12-08
申请人： Hans-Gerd Lueken , Alred Kaizik , Wilfried Bueschken , Andreas Stenert
发明人： Hans-Gerd Lueken , Alred Kaizik , Wilfried Bueschken , Andreas Stenert
IPC分类号： C07C29/16 , C07C29/14
CPC分类号： C07C45/50 , C07C29/141 , C07C31/125 , C07C47/02
摘要： A process for preparing aliphatic alcohols that includes cobalt-catalyzed hydroformylation of olefins, treatment of a hydroformylation mixture with oxygen-containing gases in the presence of acidic, aqueous cobalt(II) salt solutions, separation of a mixture into an aqueous phase comprising cobalt salts and an organic phase comprising the aliphatic aldehydes, and hydrogenation of an aldehyde-containing organic phase wherein the organic phase and treatment with an adsorbent to separate off cobalt compounds prior to hydrogenation.
摘要翻译：一种制备脂族醇的方法，其包括钴催化的烯烃加氢甲酰化，在酸性的钴（II）盐溶液存在下用含氧气体处理加氢甲酰化混合物，将混合物分离成包含钴盐的水相和包含脂族醛的有机相，和含醛有机相的氢化，其中有机相和用吸附剂处理以在氢化之前分离出钴化合物。

62. 发明授权

US06657090B2 Process for preparing highly pure raffinate II and Methyl tert-butyl ether 有权
标题翻译：制备高纯度萃余液II和甲基叔丁基醚的方法
公开(公告)号：US06657090B2
公开(公告)日：2003-12-02
申请号：US09981985
申请日：2001-10-19
申请人： Armin Rix , Gerda Grund , Wilfried Bueschken
发明人： Armin Rix , Gerda Grund , Wilfried Bueschken
IPC分类号： C07C4109
CPC分类号： B01D3/009 , C07C7/14891 , C07C11/09 , C07C41/06 , C07C41/42 , C07C2531/08 , C10L1/023 , Y02P20/127 , C07C43/046
摘要： The present invention provides a process, which includes: contacting at least one C4-hydrocarbon stream which includes isobutene with methanol over at least one acid catalyst and preparing methyl tert-butyl ether (MTBE) and a substantially isobutene-free C4-hydrocarbon mixture; wherein in a first stage in one or more first reactors, the isobutene reacts with the methanol over an acid catalyst to form an equilibrium mixture which includes MTBE, remaining isobutene and methanol; the equilibrium mixture is fed to a second stage which includes a reactive distillation column; and in the reactive distillation column, the remaining isobutene reacts with methanol over an acid ion exchange resin to form MTBE; wherein the reactive distillation column is operated at a pressure ranging from 3 to 15 bar abs., a reaction zone temperature ranging from 55° C. to 75° C., and a reflux ratio of less than 1. The present invention also provides a method of making gasoline, which includes the above process and contacting the MTBE with a fuel.
摘要翻译：本发明提供了一种方法，其包括：使至少一种包含异丁烯的C 4烃流与甲醇在至少一种酸催化剂上接触并制备甲基叔丁基醚（MTBE）和基本上不含异丁烯的C 4烃混合物; 其中在一个或多个第一反应器中的第一阶段中，异丁烯通过酸催化剂与甲醇反应形成包括MTBE，剩余的异丁烯和甲醇的平衡混合物;将平衡混合物进料到第二阶段，该第二阶段包括反应性蒸馏塔 ; 在反应蒸馏塔中，剩余的异丁烯通过酸离子交换树脂与甲醇反应以形成MTBE;其中反应蒸馏塔在3至15巴绝对压力的范围内操作，反应区温度为55℃ 至75℃，回流比小于1.本发明还提供一种制备汽油的方法，其包括上述方法并使MTBE与燃料接触。

63. 发明授权

US06340778B1 Process for catalytic aldol condensations by means of a multiphase reaction 有权
标题翻译：通过多相反应催化醛醇缩合的方法
公开(公告)号：US06340778B1
公开(公告)日：2002-01-22
申请号：US09694350
申请日：2000-10-24
申请人： Wilfried Bueschken , Klaus-Diether Wiese , Guido Protzmann , Juergen Koch
发明人： Wilfried Bueschken , Klaus-Diether Wiese , Guido Protzmann , Juergen Koch
IPC分类号： C07C4572
CPC分类号： B01J8/06 , B01J2208/00265 , C07C45/74 , C07C47/21
摘要： The invention relates to a process for the catalytic aldol condensation of aldehydes by means of a multiphase reaction in a tube reactor, wherein the catalyst is present in the continuous phase and at least one aldehyde is present in a dispersed phase and the loading factor B of the tube reactor is equal to or greater than 0.8; the aldol condensation products obtained in this way can be used for preparing alcohols or carboxylic acids.
摘要翻译：本发明涉及在管式反应器中通过多相反应催化醛醛缩合的方法，其中催化剂存在于连续相中，并且至少一种醛存在于分散相中，负载因子B为管式反应器等于或大于0.8; 以这种方式获得的醛醇缩合产物可用于制备醇或羧酸。

64. 发明授权

US5728891A Process for the preparation of 3,3,5-trimethylcyclohexanone 失效
标题翻译：制备3,3,5-三甲基环己酮的方法
公开(公告)号：US5728891A
公开(公告)日：1998-03-17
申请号：US668356
申请日：1996-06-26
申请人： Wilfried Bueschken , Juergen Hummel
发明人： Wilfried Bueschken , Juergen Hummel
IPC分类号： B01J23/44 , C07B61/00 , C07C45/62 , C07C49/403 , C07C49/303
CPC分类号： C07C45/62
摘要： A process for the preparation of 3,3,5-trimethylcyclohexanone by catalytic hydrogenation of isophorone, wherein the hydrogenation is carried out in a plurality of two or more series-connected loops, wherein each loop involves the use of one reactor, which comprises: (a) feeding isophorone and hydrogen to an upper part of a reactor to catalytically hydrogenate said isophorone to produce a hydrogenation product, (b) recycling a portion of said hydrogenation product back into said upper part of said reactor, (c) feeding the remainder of said hydrogenation product from said reactor to an upper part of a subsequent reactor wherein isophorone is catalytically hydrogenated to produce a subsequent hydrogenation product, and wherein a portion of said subsequent hydrogenation product has been recycled and is fed with said remainder of said hydrogenation product to said upper part of said subsequent reactor, (d) repeating step (c) until the subsequent reactor is the last reactor, (e) recovering the remainder of said subsequent hydrogenation product from said last reactor, and (f) obtaining 3,3,5-trimethylcyclohexanone from the product of step (e).
摘要翻译：通过异佛尔酮的催化氢化制备3,3,5-三甲基环己酮的方法，其中氢化在多个两个或更多个串联连接的环中进行，其中每个环包括使用一个反应器，其包含：（a）将异佛尔酮和氢气加入到反应器的上部以催化氢化所述异佛尔酮以产生氢化产物，（b）将所述氢化产物的一部分再循环回所述反应器的上部，（c）的所述氢化产物从所述反应器到后续反应器的上部，其中异佛尔酮被催化氢化以产生随后的氢化产物，并且其中所述后续氢化产物的一部分已被再循环并与所述剩余的所述氢化产物一起加入所述后续反应器的所述上部，（d）重复步骤（c），直到随后的反应器为最后的反应器，（e）回收t 剩余的来自所述最后一个反应器的所述随后的氢化产物，和（f）从步骤（e）的产物获得3,3,5-三甲基环己酮。

65. 发明授权

US4885397A Process for the preparation of cyclic ketones by isomerization of epoxides 失效
标题翻译：通过环氧化物异构化制备环酮的方法
公开(公告)号：US4885397A
公开(公告)日：1989-12-05
申请号：US244070
申请日：1988-09-14
申请人： Wilfried Bueschken
发明人： Wilfried Bueschken
IPC分类号： B01J27/08 , B01J27/138 , C07B61/00 , C07C45/00 , C07C45/58 , C07C49/385 , C07C49/587 , C07C67/00
CPC分类号： C07C45/58
摘要： A process for preparing a cyclic ketone from a cyclic epoxide, comprising the step of:contacting a cyclic epoxide with an alkali or alkaline-earth halide salt in the presence of a polar solvent at a temperature ranging from 120.degree. to 250.degree. C., wherein said cyclic epoxide is unsubstituted or substituted with one or more C.sub.1-5 alkyl or alkenyl groups, and wherein said cyclic epoxide comprises 7-20 ring carbon atoms, and contains up to 5 carbon-carbon multiple bonds.
摘要翻译：一种由环状环氧化物制备环酮的方法，包括以下步骤：在极性溶剂存在下，在120-250℃的温度下使环状环氧化物与碱金属或碱土卤化物盐接触，其中所述环状环氧化物是未取代的或被一个或多个C 1-5烷基或烯基取代，并且其中所述环状环氧化物包含7-20个环碳原子，并且含有多至5个碳 - 碳多键。

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