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61. 发明授权

US07935760B2 Process of making a heterogeneous polymer blend 失效
标题翻译：制造非均相聚合物共混物的方法
公开(公告)号：US07935760B2
公开(公告)日：2011-05-03
申请号：US11296830
申请日：2005-12-07
申请人： Peijun Jiang , Aspy K. Mehta , Armenag H. Dekmezian , Sunny Jacob , Andrew G. Narvaez , Pradeep P. Shirodkar
发明人： Peijun Jiang , Aspy K. Mehta , Armenag H. Dekmezian , Sunny Jacob , Andrew G. Narvaez , Pradeep P. Shirodkar
IPC分类号： C08L23/00 , C08L23/04
CPC分类号： C08L23/10 , C08F110/06 , C08F210/06 , C08L23/145 , C08L2308/00 , C08L2312/00 , C08L2312/02 , C08L2314/06 , C08F2/001 , C08L2666/06 , C08F210/18 , C08F236/20 , C08F2500/20
摘要： In a process for producing a heterogeneous polymer blend, at least one first monomer is polymerized in a first reaction zone in the presence of a supported catalyst to produce a thermoplastic first polymer having a crystallinity of at least 30%. At least part of said first polymer is then contacted with at least one second monomer and at least one polyene in a second reaction zone under conditions sufficient to polymerize said second monomer to produce a second polymer having a crystallinity of less than 20%. The second polymer is at least partially cross-linked in the second reaction zone such that at least a fraction of the second polymer is insoluble in xylene and such that the first and second polymers form different phases of the blend.
摘要翻译：在制备非均相聚合物共混物的方法中，至少一种第一单体在负载型催化剂的存在下在第一反应区中聚合以产生具有至少30％的结晶度的热塑性第一聚合物。然后在足以使所述第二单体聚合以产生结晶度小于20％的第二聚合物的条件下，将至少部分所述第一聚合物与至少一种第二单体和至少一种多烯在第二反应区中接触。第二聚合物在第二反应区域中至少部分交联，使得至少一部分第二聚合物不溶于二甲苯并使得第一和第二聚合物形成共混物的不同相。

62. 发明授权

US07867433B2 Polyolefin-based crosslinked articles 有权
标题翻译：聚烯烃基交联物品
公开(公告)号：US07867433B2
公开(公告)日：2011-01-11
申请号：US12130745
申请日：2008-05-30
申请人： Sunny Jacob , Alistair D. Westwood , Tonson Abraham
发明人： Sunny Jacob , Alistair D. Westwood , Tonson Abraham
IPC分类号： C08L23/10 , B29C47/00
CPC分类号： C08L23/10 , C08K5/005 , C08K5/14 , C08K5/34924 , C08L23/16 , C08L75/00 , C08L2312/00 , C08L2666/02
摘要： Methods for making a crosslinked elastomeric composition and articles made of the same are provided. In at least one specific embodiment, an elastomeric composition comprising at least one propylene-based polymer is blended with at least one component selected from the group consisting of multifunctional acrylates, multifunctional methacrylates, functionalized polybutadiene resins, functionalized cyanurate, and allyl isocyanurate; and blended with at least one component selected from the group consisting of hindered phenols, phosphites, and hindered amines. The propylene-based polymer can include propylene derived units and one or more dienes, and have a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g. The blended composition can then be extruded and crosslinked. The extruded polymer can be crosslinked using electron beam radiation having an e-beam dose of about 100 KGy or less. The crosslinked polymers are particularly useful for making fibers and films.
摘要翻译：提供制备交联弹性体组合物的方法和由其制成的制品。在至少一个具体实施方案中，包含至少一种基于丙烯的聚合物的弹性体组合物与至少一种选自多官能丙烯酸酯，多官能甲基丙烯酸酯，官能化聚丁二烯树脂，官能化氰尿酸酯和异氰脲酸烯丙酯的组分共混; 并与至少一种选自受阻酚，亚磷酸酯和受阻胺的组分共混。基于丙烯的聚合物可以包括丙烯衍生的单元和一种或多种二烯，并且具有50％至99％的三单元组立构规整度和小于80J / g的熔融热。然后可以将共混组合物挤出和交联。挤出的聚合物可以使用约100KGy或更小的电子束剂量的电子束辐射进行交联。交联聚合物特别适用于制造纤维和薄膜。

63. 发明授权

US07803875B2 Curing of rubbers and thermoplastic vulcanizates in the absence of halogen donors 失效
标题翻译：在没有卤素供体的情况下固化橡胶和热塑性硫化橡胶
公开(公告)号：US07803875B2
公开(公告)日：2010-09-28
申请号：US11823250
申请日：2007-06-27
申请人： Sunny Jacob , Rodney May
发明人： Sunny Jacob , Rodney May
IPC分类号： C08L61/10 , C08L9/00
CPC分类号： C08L23/16 , C08K3/011 , C08K3/22 , C08K5/0025 , C08K5/098 , C08L21/00 , C08L23/12 , C08L61/04 , C08L2666/06 , C08L2666/16
摘要： Aspects of the invention include a method of curing a rubber composition comprising providing a rubber; intimately contacting a curative agent with the rubber; wherein the curative agent consists essentially of a phenol formaldehyde resin, a metal oxide and a carboxylic acid metal salt. Another aspect of the present invention is to a method of curing a rubber composition comprising providing a rubber; intimately contacting a curative agent with the rubber; wherein the curative agent comprises a phenol formaldehyde resin and carboxylic acid metal salt; and wherein halogen-donating species are absent from the rubber and curative agent.
摘要翻译：本发明的方面包括固化橡胶组合物的方法，包括提供橡胶; 使治疗剂与橡胶紧密接触; 其中所述固化剂基本上由酚甲醛树脂，金属氧化物和羧酸金属盐组成。本发明的另一方面是一种固化橡胶组合物的方法，包括提供橡胶; 使治疗剂与橡胶紧密接触; 其中所述固化剂包含苯酚甲醛树脂和羧酸金属盐; 并且其中卤素供体物质不存在于橡胶和固化剂中。

64. 发明申请

US20090298964A1 Polyolefin-Based Crosslinked Articles 有权
标题翻译：聚烯烃交联制品
公开(公告)号：US20090298964A1
公开(公告)日：2009-12-03
申请号：US12130745
申请日：2008-05-30
申请人： Sunny Jacob , Alistair D. Westwood , Tonson Abraham
发明人： Sunny Jacob , Alistair D. Westwood , Tonson Abraham
IPC分类号： B29C71/04
CPC分类号： C08L23/10 , C08K5/005 , C08K5/14 , C08K5/34924 , C08L23/16 , C08L75/00 , C08L2312/00 , C08L2666/02
摘要： Methods for making a crosslinked elastomeric composition and articles made of the same are provided. In at least one specific embodiment, an elastomeric composition comprising at least one propylene-based polymer is blended with at least one component selected from the group consisting of multifunctional acrylates, multifunctional methacrylates, functionalized polybutadiene resins, functionalized cyanurate, and allyl isocyanurate; and blended with at least one component selected from the group consisting of hindered phenols, phosphites, and hindered amines. The propylene-based polymer can include propylene derived units and one or more dienes, and have a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g. The blended composition can then be extruded and crosslinked. The extruded polymer can be crosslinked using electron beam radiation having an e-beam dose of about 100 KGy or less. The crosslinked polymers are particularly useful for making fibers and films.
摘要翻译：提供制备交联弹性体组合物的方法和由其制成的制品。在至少一个具体实施方案中，包含至少一种基于丙烯的聚合物的弹性体组合物与至少一种选自多官能丙烯酸酯，多官能甲基丙烯酸酯，官能化聚丁二烯树脂，官能化氰尿酸酯和异氰脲酸烯丙酯的组分共混; 并与至少一种选自受阻酚，亚磷酸酯和受阻胺的组分共混。基于丙烯的聚合物可以包括丙烯衍生的单元和一种或多种二烯，并且具有50％至99％的三单元组立构规整度和小于80J / g的熔化热。然后可以将共混组合物挤出和交联。挤出的聚合物可以使用约100KGy或更小的电子束剂量的电子束辐射进行交联。交联聚合物特别适用于制造纤维和薄膜。

65. 发明申请

US20090258209A1 Translucent Propylene-Based Elastomeric Compositions 有权
标题翻译：半透明丙烯弹性组合物
公开(公告)号：US20090258209A1
公开(公告)日：2009-10-15
申请号：US12103346
申请日：2008-04-15
申请人： Sunny Jacob , Gary K. Lawrence , Edward John Blok , Ralph E. Raulie
发明人： Sunny Jacob , Gary K. Lawrence , Edward John Blok , Ralph E. Raulie
IPC分类号： B32B27/32 , C08L23/10 , C08L23/06 , B29C45/00 , B29C47/00 , B29C49/00
CPC分类号： C08L23/10 , B29C47/0004 , B29C47/0021 , B29C47/0023 , B29C49/0005 , B29C51/002 , B29K2023/12 , C08L23/16 , C08L2666/06
摘要： A composition is described in one aspect as comprising one or more propylene-α-olefin terpolymers; wherein the propylene-α-olefin terpolymer(s) possess a melting temperature (Tm) within the range of from less than 105° C., and a heat of fusion (Hf) within the range of from less than 75 J/g; one or more polyolefin(s); and oil; wherein fillers are present, if at all, at a level that maintains a Haze value of 65% or less for the composition. The terpolymer in one embodiment is a polymer comprising at least 65 wt %, by weight of the terpolymer, of propylene-derived units, within the range of from 5 to 35 wt % of ethylene or other α-olefin and a diene such as ethylidiene norbornene, and in certain embodiments having a Mooney Viscosity (ML(1+4)@125° C.) within the range of from 10 to 50 (ASTM D1646). The compositions can be cured to form transparent or translucent articles such as sheets that are also flexible.
摘要翻译：组合物在一个方面描述为包含一种或多种丙烯-α-烯烃三元共聚物; 其中所述丙烯-α-烯烃三元共聚物的熔融温度（Tm）在小于105℃的范围内，熔融热（Hf）在小于75J / g的范围内; 一种或多种聚烯烃; 和油; 其中如果有的话，填料的含量维持组合物的雾度值为65％或更低。在一个实施方案中，三元共聚物是包含至少65重量％的三元共聚物，丙烯衍生的单元，在乙烯或其它α-烯烃的5-35重量％范围内和二烯如亚乙基降冰片烯，在某些具有门尼粘度（ML（1 + 4）@ 125℃）的实施方案中，在10至50的范围内（ASTM D1646）。组合物可以固化以形成也是柔性的透明或半透明制品，例如片材。

66. 发明授权

US07445846B2 Thermoplastic vulcanizates and laminates made therewith 失效
标题翻译：热塑性硫化胶和由其制成的层压板
公开(公告)号：US07445846B2
公开(公告)日：2008-11-04
申请号：US11097434
申请日：2005-04-01
申请人： Sunny Jacob , William Gary Stevenson
发明人： Sunny Jacob , William Gary Stevenson
IPC分类号： B32B25/08 , B32B25/14 , B32B25/16
CPC分类号： C08L23/10 , B32B25/04 , B32B25/08 , B32B25/16 , B32B25/18 , B32B27/08 , B32B27/18 , B32B27/32 , B32B2250/02 , B32B2250/24 , B32B2270/00 , B32B2274/00 , B32B2307/546 , B32B2307/554 , B32B2307/558 , B32B2307/56 , B32B2307/746 , B32B2419/00 , B32B2479/00 , B32B2605/08 , C08L23/16 , C08L23/22 , Y10T428/3154 , Y10T428/31544 , Y10T428/31913 , Y10T428/31917 , Y10T428/31924 , Y10T428/31931 , Y10T428/31938 , C08L2666/06
摘要： A thermoplastic vulcanizate comprising a) a dynamically vulcanized rubber, b) a thermoplastic resin, and c) optionally a synthetic oil, where the thermoplastic vulcanizate is substantially devoid of mineral oils.
摘要翻译：一种热塑性硫化橡胶，其包含a）动态硫化橡胶，b）热塑性树脂，和c）任选的合成油，其中热塑性硫化橡胶基本上不含矿物油。

67. 发明申请

US20070284787A1 Process for preparing articles 失效
标题翻译：制备文章的过程
公开(公告)号：US20070284787A1
公开(公告)日：2007-12-13
申请号：US11787855
申请日：2007-04-18
申请人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
发明人： Weiqing Weng , Sunny Jacob , Peijun Jiang , Armenag H. Dekmezian , Aspy K. Mehta , Peter W. Manders , Pradeep Shirodkar , Palanisamy Arjunan
IPC分类号： C08L23/00 , B29C43/00
CPC分类号： B29C43/003 , C08L21/00 , C08L23/04 , C08L23/10 , C08L23/16 , C08L61/06 , C08L67/00 , C08L69/00 , C08L2312/04 , C08L2666/06 , C08L2666/08 , C08L2666/02
摘要： The present invention relates to a process for preparing a thermoplastic vulcanizate (TPV) comprising: contacting a thermoplastic polymer, a cross-linkable elastomer, at least one curative, and at least one cure activator in a solvent to form Composition A. The solvent is then removed, and thereafter the cross-linkable elastomer is at least partially cured. The average particle size of the cross-linkable elastomer is 10 microns or less after the solvent is removed.
摘要翻译：本发明涉及一种制备热塑性硫化橡胶（TPV）的方法，包括：使热塑性聚合物，可交联弹性体，至少一种固化剂和至少一种固化活化剂在溶剂中接触以形成组合物A.溶剂是然后除去，然后可交联弹性体至少部分固化。除去溶剂后，可交联弹性体的平均粒径为10微米以下。

68. 发明申请

US20070083007A1 Microcellular foams of thermoplastic vulcanizates 有权
标题翻译：热塑性硫化胶的微孔泡沫
公开(公告)号：US20070083007A1
公开(公告)日：2007-04-12
申请号：US11246772
申请日：2005-10-07
申请人： Sunny Jacob
发明人： Sunny Jacob
IPC分类号： C08L53/00 , B29C44/34
CPC分类号： C08L23/16 , C08J9/0061 , C08J2323/10 , C08J2421/00 , C08J2451/00 , C08L23/10 , C08L23/12 , C08L23/14 , C08L23/142 , C08L23/283 , C08L51/06 , C08L51/08 , C08L53/02 , C08L53/025 , C08L91/00 , C08L2205/02 , C08L2205/035 , C08L2205/22 , C08L2207/07 , C08L2312/00 , C08L2666/02 , C08L2666/24 , C08L2666/08 , C08L2666/06 , C08L2666/14
摘要： The invention described relates to formed profiles comprising microcellular TPE foam compositions, and articles therefrom, wherein the TPE are thermoplastic vulcanizates. The foamed thermoplastic elastomer profile comprises a foamable thermoplastic elastomer composition having a) a cross-linkable hydrocarbon rubber in the presence of b) a thermoplastic polyolefin resin having a Tm greater than 120° C. wherein said composition further comprising: a) 25 to 30 wt % of a partially or fully vulcanized reaction product of said cross-linkable hydrocarbon rubber with a cross-linking agent, said reaction product being present as a dispersed phase; b) 7 to 12 wt % of said thermoplastic resin as a continuous phase; c) 8-22 wt % of an elastomeric thermoplastic modifier comprising 1) 3-7 wt. % copolymers of propylene with one or more of ethylene and C4-C10 alpha-olefins, said copolymers having a Tm greater than 20° C. and less than 120° C., and, 2) 5-15 wt. % hydrogenated, triblock styrenic copolymers from styrene and isoprene; and, optionally, d) 3-12 wt. % solid filler; and/or e) 35-45 wt. % of non-aromatic hydrocarbon oil; wherein said wt. % amounts are based upon the total weight of the composition, and where the composition has been prepared by a process comprising dynamically vulcanizing said composition. The foamed thermoplastic elastomer profiles having smooth surfaces, improved low water absorption, improved compression set and compression load deflection.
摘要翻译：所描述的本发明涉及包含微孔TPE泡沫组合物的成型型材及其制品，其中TPE是热塑性硫化橡胶。发泡热塑性弹性体轮廓包括可发泡的热塑性弹性体组合物，其具有a）可交联烃橡胶，其存在b）具有Tm大于120℃的热塑性聚烯烃树脂。其中所述组合物还包含：a）25至30 所述可交联烃橡胶与交联剂的部分或完全硫化的反应产物的wt％，所述反应产物以分散相存在; b）作为连续相的7〜12重量％的所述热塑性树脂; c）8-22重量％的弹性体热塑性改性剂，其包含1）3-7重量％丙烯与乙烯和C 4 -C 10α-烯烃中的一种或多种的共聚物，所述共聚物的Tm大于20℃且小于120℃ C.，和2）5-15wt。％苯乙烯和异戊二烯的氢化三嵌段苯乙烯共聚物; 和任选地，d）3-12重量％％固体填料; 和/或e）35-45wt。％的非芳香烃油; 其中所述wt。％的量基于组合物的总重量，并且其中组合物通过包括动态硫化所述组合物的方法制备。发泡热塑性弹性体轮廓具有光滑的表面，改善的低吸水率，改进的压缩永久变形和压缩载荷偏转。

69. 发明申请

US20060293460A1 Heterogeneous polymer blend with continuous elastomeric phase and process of making the same 失效
标题翻译：具有连续弹性相的非均相聚合物共混物和制备相同的方法
公开(公告)号：US20060293460A1
公开(公告)日：2006-12-28
申请号：US11295927
申请日：2005-12-07
申请人： Sunny Jacob , Peijun Jiang , Aspy Mehta , Pradeep Shirodkar , Armenag Dekmezian
发明人： Sunny Jacob , Peijun Jiang , Aspy Mehta , Pradeep Shirodkar , Armenag Dekmezian
IPC分类号： C08L23/04
CPC分类号： C08L23/16 , C08L23/10 , C08L2312/00 , C08L2666/06
摘要： A heterogeneous polymer blend comprises a dispersed phase comprising a thermoplastic first polymer having a crystallinity of at least 30% and a continuous phase comprising a second polymer different from the first polymer. The second polymer has a crystallinity of less than 20% and is at least partially cross-linked.
摘要翻译：非均相聚合物共混物包含分散相，其包含结晶度至少为30％的热塑性第一聚合物和包含不同于第一聚合物的第二聚合物的连续相。第二聚合物具有小于20％的结晶度并且至少部分交联。

70. 发明授权

US06787607B2 Thermoplastic elastomers having enhanced foaming and physical properties 失效
标题翻译：具有增强发泡和物理性能的热塑性弹性体
公开(公告)号：US06787607B2
公开(公告)日：2004-09-07
申请号：US10203323
申请日：2002-10-28
申请人： Abdelhadi Sahnoune , Terry M. Finerman , Sunny Jacob , Sydney Ham
发明人： Abdelhadi Sahnoune , Terry M. Finerman , Sunny Jacob , Sydney Ham
IPC分类号： C08F800
CPC分类号： C08J9/0061 , C08J2323/16 , C08J2427/00 , C08L23/02 , C08L23/04 , C08L23/10 , C08L23/16 , C08L27/18 , C08L33/06 , C08L2203/14 , C08L2205/22 , C08L2666/04 , C08L2666/06
摘要： An olefinic thermoplastic elastomer composition which includes an acrylic-modified polytetrafluoroethylene. When foamed, such compositions produce a very soft foam with improved processing properties and physical characteristics. A process of foaming and foamed articles are also disclosed.
摘要翻译：一种包含丙烯酸改性聚四氟乙烯的烯烃类热塑性弹性体组合物。当发泡时，这种组合物产生非常柔软的泡沫，具有改进的加工性能和物理特性。还公开了发泡和发泡制品的方法。

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