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    • 61. 发明授权
    • Ion beam sample preparation apparatus and methods
    • 离子束样品制备装置及方法
    • US08283642B2
    • 2012-10-09
    • US13082373
    • 2011-04-07
    • Steven Thomas CoyleJohn Andrew Hunt
    • Steven Thomas CoyleJohn Andrew Hunt
    • G21K5/10H01J37/08H01J37/30H01J37/31
    • G01N1/44G01N1/32H01J37/023H01J37/31H01J2237/0245H01J2237/2007H01J2237/3118
    • Disclosed are embodiments of an ion beam sample preparation apparatus and methods for using the embodiments. The apparatus comprises a tilting ion beam irradiating means in a vacuum chamber that may direct ions toward a sample, a shield blocking a portion of the ions directed toward the sample, and a shield retention stage with shield retention means that replaceably and removably holds the shield in a position. The shield has datum features which abut complementary datum features on the shield retention stage when the shield is held in the shield retention stage. The shield has features which enable the durable adhering of the sample to the shield for processing the sample with the ion beam. The complementary datum features on both shield and shield retention stage enable accurate and repeatable positioning of the sample in the apparatus for sample processing and reprocessing. The tilting ion beam irradiating means may direct ions at the sample from more than one tilt angle. A rotating shield retention stage is also disclosed which works in concert with the tilting ion beam irradiating means to improve the flexibility and efficiency of the apparatus in preparing samples for microscopic observation.
    • 公开了用于使用实施例的离子束样品制备装置和方法的实施方案。 该装置包括在真空室中的倾斜离子束照射装置,其可将离子引向样品,屏蔽阻挡朝向样品的一部分离子的屏蔽保护台,以及具有屏蔽保持装置的屏蔽保持装置,其可替换地和可移除地保持屏蔽 在一个位置 当屏蔽保持在屏蔽保持阶段时,屏蔽具有与屏蔽保持平台上的辅助基准特征相交的基准特征。 屏蔽件具有能够将样品耐久地粘附到屏蔽件的特征,以用离子束处理样品。 屏蔽和屏蔽保持阶段的补充基准特征使得样品能够准确和可重复地定位在用于样品处理和再处理的设备中。 倾斜离子束照射装置可以从多于一个倾斜角度引导样品处的离子。 还公开了旋转屏蔽保持阶段,其与倾斜离子束照射装置协调工作,以在制备用于显微镜观察的样品中提高装置的灵活性和效率。
    • 62. 发明申请
    • Ion Beam Sample Preparation Apparatus and Methods
    • 离子束样品制备装置及方法
    • US20120085939A1
    • 2012-04-12
    • US13082373
    • 2011-04-07
    • Steven Thomas CoyleJohn Andrew Hunt
    • Steven Thomas CoyleJohn Andrew Hunt
    • G21K5/10
    • G01N1/44G01N1/32H01J37/023H01J37/31H01J2237/0245H01J2237/2007H01J2237/3118
    • Disclosed are embodiments of an ion beam sample preparation apparatus and methods for using the embodiments. The apparatus comprises a tilting ion beam irradiating means in a vacuum chamber that may direct ions toward a sample, a shield blocking a portion of the ions directed toward the sample, and a shield retention stage with shield retention means that replaceably and removably holds the shield in a position. The shield has datum features which abut complementary datum features on the shield retention stage when the shield is held in the shield retention stage. The shield has features which enable the durable adhering of the sample to the shield for processing the sample with the ion beam. The complementary datum features on both shield and shield retention stage enable accurate and repeatable positioning of the sample in the apparatus for sample processing and reprocessing. The tilting ion beam irradiating means may direct ions at the sample from more than one tilt angle. A rotating shield retention stage is also disclosed which works in concert with the tilting ion beam irradiating means to improve the flexibility and efficiency of the apparatus in preparing samples for microscopic observation.
    • 公开了用于使用实施例的离子束样品制备装置和方法的实施方案。 该装置包括在真空室中的倾斜离子束照射装置,其可将离子引向样品,屏蔽阻挡朝向样品的一部分离子的屏蔽保护台,以及具有屏蔽保持装置的屏蔽保持装置,其可替换地和可移除地保持屏蔽 在一个位置 当屏蔽保持在屏蔽保持阶段时,屏蔽具有与屏蔽保持平台上的辅助基准特征相交的基准特征。 屏蔽件具有能够将样品耐久地粘附到屏蔽件的特征,以用离子束处理样品。 屏蔽和屏蔽保持阶段的补充基准特征使得样品能够准确和可重复地定位在用于样品处理和再处理的设备中。 倾斜离子束照射装置可以从多于一个倾斜角度引导样品处的离子。 还公开了旋转屏蔽保持阶段,其与倾斜离子束照射装置协调工作,以在制备用于显微镜观察的样品中提高装置的灵活性和效率。
    • 67. 发明授权
    • Rotatable wide angle camera and prism assembly for electron microscopes
    • 可旋转广角相机和电子显微镜的棱镜组件
    • US5536941A
    • 1996-07-16
    • US392242
    • 1995-02-22
    • Peter R. Swann
    • Peter R. Swann
    • H01J37/22H01J37/244
    • H01J37/224H01J2237/244H01J2237/26
    • An apparatus for recording electron images and diffraction patterns which can be automatically controlled via a computer, has improved precision, and has greater flexibility in acquiring and displaying specimen images is provided. The apparatus includes an electron microscope having a projection chamber, an electron scintillator in the projection chamber for converting a projected electron image into a light image, and a camera positioned adjacent to the projection chamber for acquiring the light image. The camera is rotatable about its optical (horizontal) axis so that desired features of the acquired image may be brought into alignment with the display device used to view them, such as for example, a CRT screen. By positioning the camera outside of the vacuum of the electron microscope projection chamber, problems associated with prior internally-mounted devices are avoided and the camera may be readily manually or automatically adjusted.
    • 用于记录可以通过计算机自动控制的电子图像和衍射图案的设备具有提高的精度,并且在获取和显示样本图像方面具有更大的灵活性。 该装置包括具有投影室的电子显微镜,投影室中的电子闪烁体,用于将投射的电子图像转换成光图像;以及位于投影室附近的照相机,用于获取光图像。 照相机可绕其光学(水平)轴线旋转,使得所获取的图像的期望特征可以与用于观看它们的显示装置(例如CRT屏幕)对齐。 通过将相机定位在电子显微镜投影室的真空之外,避免了与现有内置装置相关的问题,并且可以容易地手动或自动调节照相机。
    • 68. 发明授权
    • Specimen elevator for an ion milling machine
    • US4272682A
    • 1981-06-09
    • US65579
    • 1979-08-10
    • Peter R. Swann
    • Peter R. Swann
    • G01N1/32H01J37/305H01L21/687
    • H01L21/68742H01J37/3053H01L21/68792G01N1/32
    • An ion milling machine specimen elevator comprising a vertically oriented piston which supports a specimen holder at its top and is movable between a lowered operating position and a raised viewing position. When the piston is in the lowered operating position, it is slowly rotated about its vertical axis by a suitable drive. The elongated piston passes through an O-ring seal into an evacuated ion milling or work chamber. At the bottom of the work chamber is disposed a pneumatic control cylinder into which the piston extends. The piston can be moved up or down by altering the pressure in the pneumatic cylinder. During ion milling the piston is at its lowest position in the evacuated work chamber and is held there by pressurized gas in the pneumatic control cylinder. A second small chamber is provided above the work chamber for specimen viewing and specimen exchange. The disclosed specimen elevator can move the specimen into the second chamber and at the same time provide a seal so the work chamber does not lose vacuum during specimen viewing or exchange. If it is desired to remove the specimen from the work chamber without disturbing its vacuum, the pressure in the pneumatic control cylinder is released and the elongated piston is automatically forced to its highest position by the exerted atmospheric pressure. As the elongated piston rises to its upper position the top of the piston passes through a second O-ring seal, at the top of the work chamber, then into the small second chamber. As the piston moves into the small second chamber, it seals the work chamber from the small second chamber so air admitted to the second chamber does not enter the work chamber. The small chamber can be lifted from the larger work chamber after the internal pressure of the small chamber is raised to atmospheric. Removing the small chamber exposes the specimen holder, allowing the specimen to be removed or closely examined to study the progress of the ion milling operation. The specimen is reinserted into the work chamber by replacing and then evacuating the small chamber and then by repressurizing the pneumatic control cylinder. This forces the piston to move through the seal between the work chamber and the small chamber to its lowest position. The piston has a beveled gear attached thereto which engages a driven bevel gear when the piston is in the lowered operating position to slowly rotate the specimen in the work chamber.