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51. 发明申请

US20210154653A1 METHOD FOR PREPARING A NICKEL- AND COPPER-BASED BIMETALLIC CATALYST FOR HYDROGENATING AROMATIC COMPOUNDS 有权
公开(公告)号：US20210154653A1
公开(公告)日：2021-05-27
申请号：US17048223
申请日：2019-04-05
申请人： IFP Energies Nouvelles
发明人： Malika BOUALLEG , Anne-Agathe QUOINEAUD
IPC分类号： B01J37/02 , B01J23/72 , B01J23/755 , B01J6/00 , C10G45/48 , B01J37/20 , B01J37/18 , B01J37/08
摘要： Method for preparing a catalyst comprising a bimetallic active phase made of nickel and copper, and a support comprising a refractory oxide, comprising the following steps:
a step of bringing the support into contact with a solution containing a nickel precursor is carried out;
a step of bringing the support into contact with a solution containing a copper precursor is carried out;
a step of drying the catalyst precursor at a temperature lower than 250° C. is carried out;
the catalyst precursor obtained is supplied to a hydrogenation reactor, and a step of reduction by bringing said precursor into contact with a reducing gas at a temperature lower than 200° C. for a period greater than or equal to 5 minutes and less than 2 hours is carried out.

52. 发明授权

US10745628B2 Hydrogenation catalyst for aromatic hydrocarbon and hydrotreatment method using the catalyst 有权
公开(公告)号：US10745628B2
公开(公告)日：2020-08-18
申请号：US15700089
申请日：2017-09-09
申请人： CHIYODA CORPORATION
发明人： Kenichi Imagawa , Haruto Kobayashi , Akihiro Muto , Shinichi Inoue
IPC分类号： C10G45/48 , B01J23/755 , C07C5/10 , C07C13/18 , C01G23/08 , B01J21/04 , B01J35/10 , B01J37/02 , B01J21/06 , C01G53/04 , B01J37/18 , C01F7/02 , C01F7/34 , C01G23/04 , G01N23/20
摘要： A hydrogenation catalyst with a small amount of supported metal that is excellent in stability and inhibition of side reactions is provided. The catalyst hydrogenates an aromatic hydrocarbon compound into an alicyclic hydrocarbon compound, and a Group X metal represented by nickel is supported in a composite support including at least alumina and titania. The composite support preferably includes at least an alumina substrate coated with titania. It is also preferable that the Group X metal is prereduced by hydrogen. In the case that the Group X metal is nickel, the nickel content is preferably 5-35 wt % as nickel oxide in the catalyst. The substrate includes, for example, a porous structure formed by a plurality of needle-shaped or column-shaped intertwined three-dimensionally.

53. 发明申请

US20190330536A1 CONVERSION PROCESS FOR AN ORGANIC MATERIAL 审中-公开
公开(公告)号：US20190330536A1
公开(公告)日：2019-10-31
申请号：US16427218
申请日：2019-05-30
申请人： BEIJING SANJU ENVIRONMENTAL PROTECTION & NEW MATERIALS CO., LTD
发明人： Ke LIN , Lixin GUO , Yongjun CUI , Shengfeng LI , Dongmei CUI
IPC分类号： C10G1/00 , C10J3/72 , C10G1/06 , C10G45/40 , C10G45/36 , C10G45/52 , C10G45/54 , C10G45/48 , C10G2/00 , B01J23/745
摘要： Provided is a conversion process for an organic oil, relating to the field of biomass utilization, energy and chemical industry. The conversion process is carried out in presence of an aqueous slurry and a catalyst selected from the group consisting of an iron oxide compound, a waste agent resulting from use of an iron oxide compound as desulfurizer, and a regeneration product of the waste agent, under a controlled molar ratio of iron element to sulfur element. It is found that free radical condensation polymerization of organic oil during cracking process can be blocked effectively by using carbonylation, and hydrogenation is achieved with active hydrogen produced from the conversion of CO and water. In the conversion process, organic material, especially biomass solid, can be directly converted without dehydration, and water can be additionally added to the biomass liquid or the mineral oil.

54. 发明授权

US10350580B2 Catalyst with a mesoporous and macroporous co-mixed nickel active phase having a median macropore diameter in the range 50 to 300 NM, and its use in hydrogenation 有权
公开(公告)号：US10350580B2
公开(公告)日：2019-07-16
申请号：US15317839
申请日：2015-06-09
申请人： IFP Energies nouvelles
发明人： Malika Boualleg , Anne-Claire Dubreuil , Emily Maille , Cecile Thomazeau
IPC分类号： B01J21/04 , B01J23/755 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/02 , B01J37/03 , B01J37/04 , B01J37/08 , C07C5/03 , C07C5/05 , C07C5/10 , C10G45/36 , C10G45/48 , B01J23/835 , B01J23/89 , B01J27/185 , B01J35/00 , B01J37/20 , B01J33/00
摘要： A catalyst comprising a calcined oxide matrix which is mainly alumina and an active phase comprising nickel, said active phase being at least partially co-mixed within said calcined oxide matrix which is mainly alumina, the nickel content being in the range 5% to 65% by weight of said element with respect to the total mass of catalyst, said active phase not comprising any metal from group VIB, the nickel particles having a diameter of less than 15 nm, said catalyst having a median mesopore diameter in the range 12 nm to 25 nm, a median macropore diameter in the range 50 to 300 nm, a mesopore volume, measured by mercury porosimetry, of 0.40 mL/g or more and a total pore volume, measured by mercury porosimetry, of 0.45 mL/g or more. The process for the preparation of said catalyst, and its use in a hydrogenation process.

55. 发明授权

US10273419B2 Method for producing naphthenic process oils by hydrogenation 有权
公开(公告)号：US10273419B2
公开(公告)日：2019-04-30
申请号：US15157556
申请日：2016-05-18
申请人： KLAUS DAHLEKE KG
发明人： Nils Hansen
IPC分类号： C08L9/06 , C09D5/00 , C09D11/02 , C10G45/44 , C10G45/46 , C10G45/48 , C10G45/50 , B01J23/883 , C10M101/02
摘要： The object of the invention is a method for producing naphthenic process oils that have a high content of naphthenic carbon atoms of 20-60 wt % and a low content of polycyclic aromatics of less than 3 wt %, determined in accordance with IP 346, by the hydrogenation of a process oil educt that has a high content of polycyclic aromatics. The method in accordance with the invention enables secondary extracts, such as are formed in the production of label-free process oils, even in a mixture with primary extracts, to be utilized in an economically meaningful way. The resulting process oils are likewise label-free, so that the use of PCA-containing process oils can be reduced and less of these substances will get into the environment. Through this the environment and in particular health are less stressed. In addition, the starting substances in this way can lead to a different use and no longer have to be added to heating oil. By avoiding heating oil, CO2 emissions are also reduced. Also, through the direct hydrogenation of DAE, high value naphthenic process oils are obtained by the method in accordance with the invention. The process oils that are obtained contain surprisingly high amounts of naphthenic hydrocarbon compounds. In addition, an object of the invention is the use of the process oils produced in accordance with the invention as a plasticizer or extender oil for natural and synthetic rubber mixtures or thermoplastic elastomers.

56. 发明授权

US09528052B2 Two stage diesel aromatics saturation process using base metal catalyst 有权
标题翻译：使用贱金属催化剂的二阶段柴油芳烃饱和方法
公开(公告)号：US09528052B2
公开(公告)日：2016-12-27
申请号：US14281425
申请日：2014-05-19
申请人： SHELL OIL COMPANY
发明人： John Anthony Smegal , Aristides Macris
IPC分类号： C10G65/08 , C10G45/50 , C10G65/00 , C10G65/02 , C10G65/04 , C10G45/44 , C10G45/46 , C10G45/48
CPC分类号： C10G65/08 , C10G45/50
摘要： A process that provides for the improvement of the properties of a distillate feedstock that has significant concentrations of nitrogen and polyaromatic compounds. The process includes a first reaction zone that uses a base metal catalyst and is operated under high pressure conditions to provide for the hydrodenitrogenation of organic nitrogen and saturation of polyaromatic compounds contained in the distillate feedstock. The first reaction zone treated effluent is separated into a heavy fraction and a lighter fraction with the heavy fraction being charged to a second reaction zone that also uses a base metal catalyst and is operated under high pressure conditions to provide for the saturation of monaromatic compounds that are contained in the heavy fraction. The inventive process provides for a high quality, low-sulfur and low-nitrogen diesel product that has a significantly lower aromatics content than the distillate feedstock and having a high value for its high Cetane Index.
摘要翻译：提供具有显着浓度的氮和多芳族化合物的馏出物原料的性质的改进的方法。该方法包括使用贱金属催化剂并在高压条件下操作以提供有机氮的加氢脱氮和馏出物原料中所含的多芳族化合物的饱和的第一反应区。将第一反应区处理的流出物分离成重馏分和轻馏分，将重馏分装入第二反应区，第二反应区也使用贱金属催化剂，并在高压条件下操作以提供饱和的单芳族化合物，包含在重馏分中。本发明方法提供了高质量，低硫和低氮柴油产品，其具有比馏出物原料显着更低的芳族化合物含量，并且对于其高十六烷指数具有高值。

57. 发明授权

US09315755B2 Catalytic system for preparation of high branched alkane from olefins 有权
标题翻译：用于从烯烃制备高支链烷烃的催化体系
公开(公告)号：US09315755B2
公开(公告)日：2016-04-19
申请号：US14118172
申请日：2012-04-23
申请人： Yong Tang , Wenjie Tao , Xiuli Sun , Junfang Li , Zheng Wang
发明人： Yong Tang , Wenjie Tao , Xiuli Sun , Junfang Li , Zheng Wang
IPC分类号： C10M105/04 , B01J31/22 , B01J31/18 , C07C323/45 , C07C251/08 , C07C251/20 , C10G45/48 , C10G45/52 , C10G50/00 , C10G69/12 , C08F10/00 , C07F15/04 , C07C251/24
CPC分类号： C10M105/04 , B01J31/1805 , B01J31/2295 , B01J2231/20 , B01J2531/824 , B01J2531/847 , B01J2540/225 , B01J2540/30 , C07C251/08 , C07C251/20 , C07C251/24 , C07C323/45 , C07C2603/20 , C07C2603/26 , C07F15/04 , C07F15/045 , C08F8/04 , C08F10/00 , C08F110/02 , C08F110/08 , C10G45/48 , C10G45/52 , C10G50/00 , C10G50/02 , C10G69/126 , C10G2300/1088 , C10G2300/302 , C10G2300/304 , C10G2400/10 , C10M107/10 , C10M177/00 , C10M2205/028 , C10M2205/0285 , C10N2270/00 , C08F4/7006 , C08F2500/02 , C08F2500/10 , C08F2500/17 , C08F110/06
摘要： The present invention discloses a catalytic system for preparing highly branched alkane from olefin, which contains novel nickel or palladium complexes. In the presence of the catalytic system, highly branched oily alkane mixture can be efficiently obtained from olefins (such as ethylene) under mild conditions. The alkane mixture has a low bromine number, and can be used as a processing aid(s) and lubricant base oil with high-performance. Provides also was a method for preparing the catalyst and a method for preparing an oily olefin polymer.
摘要翻译：本发明公开了一种由烯烃制备高分支烷烃的催化体系，其中含有新的镍或钯络合物。在催化体系的存在下，在温和条件下，可以从烯烃（如乙烯）中有效地获得高度支化的油状烷烃混合物。烷烃混合物具有低溴值，可用作加工助剂和具有高性能的润滑剂基础油。也提供了制备催化剂的方法和制备油性烯烃聚合物的方法。

58. 发明授权

US09212323B2 Liquid-full hydrotreating and selective ring opening processes 有权
标题翻译：全液相加氢处理和选择性开环方法
公开(公告)号：US09212323B2
公开(公告)日：2015-12-15
申请号：US14335058
申请日：2014-07-18
申请人： E I DU PONT DE NEMOURS AND COMPANY
发明人： Hasan Dindi , Thanh Gia Ta
IPC分类号： C10G45/02 , C10G45/08 , C10G45/22 , C10G45/48 , C10G45/58 , C10G45/60 , C10G65/08 , C10G65/12 , C10G69/02 , C10G45/50 , C10G45/54 , C10G65/04
CPC分类号： C10G45/02 , C10G45/08 , C10G45/22 , C10G45/48 , C10G45/50 , C10G45/54 , C10G45/58 , C10G45/60 , C10G65/043 , C10G65/08 , C10G65/12 , C10G69/02 , C10G2300/202 , C10G2300/307 , C10G2300/308 , C10G2300/4018 , C10G2300/4081 , C10G2300/802 , C10G2400/04
摘要： This disclosure relates to liquid-full processes for hydroprocessing a light cycle oil (LCO). The processes involve hydrotreatment followed by selective ring opening in the presence of hydrotreating catalyst and selective ring opening catalyst respectively. The selective ring opening catalyst can be either zeolite ring opening catalyst or amorphous ring opening catalyst. In aspects of zeolite ring opening catalyst, the volume ratio of the total amount of the zeolite ring opening catalyst to the total amount of the hydrotreating catalyst is from about 0.2 to about 1.5. In aspects of amorphous ring opening catalyst, the volume ratio of the total amount of the amorphous ring opening catalyst to the total amount of the hydrotreating catalyst is from about 0.2 to about 3.
摘要翻译：本公开涉及用于加氢处理轻质循环油（LCO）的液体充分方法。该方法包括加氢处理，然后在加氢处理催化剂和选择性开环催化剂存在下选择性开环。选择性开环催化剂可以是沸石开环催化剂或无定形开环催化剂。在沸石开环催化剂方面，沸石开环催化剂的总量与加氢处理催化剂总量的体积比为约0.2至约1.5。无定形开环催化剂方面，无定形开环催化剂的总量与加氢处理催化剂总量的体积比为约0.2至约3。

59. 发明授权

US08992768B2 Method for the desulfurization of fuels and highly active nickel carrier catalyst based on aluminum oxide suitable for said method 有权
标题翻译：基于适用于所述方法的氧化铝的燃料脱硫和高活性镍载体催化剂的方法
公开(公告)号：US08992768B2
公开(公告)日：2015-03-31
申请号：US12531540
申请日：2008-03-13
申请人： Jürgen Ladebeck , Tiberius Regula , Klaus Wanninger , Wolfgang Gabriel , Frank Grossmann , Jürgen Koy
发明人： Jürgen Ladebeck , Tiberius Regula , Klaus Wanninger , Wolfgang Gabriel , Frank Grossmann , Jürgen Koy
IPC分类号： C10G25/00 , C10G45/06 , B01J20/08 , B01J20/28 , B01J23/755 , B01J23/78 , B01J23/89 , B01J35/10 , B01J37/03 , B82Y30/00 , C10G45/48 , C10G45/52 , B01J35/00 , B01J37/00
CPC分类号： C10G25/003 , B01J20/08 , B01J20/28007 , B01J20/28014 , B01J20/2803 , B01J20/28057 , B01J20/28069 , B01J20/28078 , B01J23/755 , B01J23/78 , B01J23/892 , B01J35/0053 , B01J35/006 , B01J35/10 , B01J35/1019 , B01J35/1038 , B01J35/108 , B01J37/0009 , B01J37/03 , B82Y30/00 , C10G45/06 , C10G45/48 , C10G45/52 , C10G2300/202 , C10G2300/701 , C10G2400/02
摘要： A highly active nickel carrier catalyst based on aluminium oxide has a nickel content of approximately 20 to 70 wt.-% (as Ni) and optionally comprises a bonding agent and optionally a promoter, selected from the compounds of Mg, Ti, Pb, Pt, Ba, Ca and/or Cu, wherein the size of the Ni crystallites in the reduced state is in the range of approximately 3.5 to 4.5 nm and the distortion factor of the Ni crystallites is approximately 2 to 5%. In a method for the reduction of the content of sulphur compounds in hydrocarbon-based fuels by selective adsorption of the sulphur compounds on a nickel catalyst, a nickel catalyst based on aluminium oxide is used, particularly the nickel catalyst described above. A nickel catalyst based on aluminium oxide may be used for reducing the sulphur compound content in hydrocarbon-based fuels by selective adsorption of the sulphur compounds on said catalyst and/or for the hydrogenation of aromatic compounds.
摘要翻译：基于氧化铝的高活性镍载体催化剂的镍含量为约20至70重量％（如Ni），并且任选地包含粘合剂和任选的助催化剂，其选自Mg，Ti，Pb，Pt ，Ba，Ca和/或Cu，其中处于还原态的Ni微晶的尺寸在约3.5至4.5nm的范围内，并且Ni微晶的变形系数约为2％至5％。在通过硫化合物选择性吸附在镍催化剂上来降低烃基燃料中硫化合物含量的方法中，使用基于氧化铝的镍催化剂，特别是上述镍催化剂。基于氧化铝的镍催化剂可用于通过选择性吸附所述催化剂上的硫化合物和/或芳族化合物的氢化来还原烃基燃料中的硫化合物含量。

60. 发明授权

US08912377B2 Method for producing high value aromatics and olefin from light cycle oil produced by a fluidized catalytic cracking process 有权
标题翻译：由流化催化裂化工艺生产的轻循环油生产高价值芳烃和烯烃的方法
公开(公告)号：US08912377B2
公开(公告)日：2014-12-16
申请号：US13124406
申请日：2009-10-07
申请人： Cheol Joong Kim , Tae Jin Kim , Do Woan Kim , Sung Won Kim , Sang Hun Oh , Sam Ryong Pakr , Seung Hoon Oh , Yoon Kyung Lee , Gyung Rok Kim , Hong Seok Jung , Eun Kyoung Kim , Byoung In Lee , Dae Hyun Choo
发明人： Cheol Joong Kim , Tae Jin Kim , Do Woan Kim , Sung Won Kim , Sang Hun Oh , Sam Ryong Pakr , Seung Hoon Oh , Yoon Kyung Lee , Gyung Rok Kim , Hong Seok Jung , Eun Kyoung Kim , Byoung In Lee , Dae Hyun Choo
IPC分类号： C10G11/02 , C07C4/06 , C10G11/18 , C10G11/04 , C10G11/05 , C10G45/44 , C10G45/46 , C10G45/48 , C10G69/04 , C10G69/06
CPC分类号： C10G11/18 , C10G11/02 , C10G11/04 , C10G11/05 , C10G45/44 , C10G45/46 , C10G45/48 , C10G69/04 , C10G69/06 , C10G2300/4081 , C10G2400/20 , C10G2400/30
摘要： The present invention relates to a method of producing aromatic products (benzene/toluene/xylene) and olefin products from petroleum fractions obtained by fluid catalytic cracking, and, more particularly, to a method of producing products comprising high-concentration aromatic products and high value-added light olefin products from light cycle oil obtained by fluid catalytic cracking.
摘要翻译：本发明涉及通过流化催化裂化得到的石油馏分中的芳香族产物（苯/甲苯/二甲苯）和烯烃产物的制造方法，更具体地说，涉及一种生产高浓度芳香族产物和高价值物质的方法 - 通过流化催化裂化获得的轻循环油的添加轻质烯烃产物。

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