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51. 发明授权

US4886895A Phosphate-containing and phosphonate-containing phosphate esters 失效
标题翻译：含磷酸盐和膦酸酯的磷酸酯
公开(公告)号：US4886895A
公开(公告)日：1989-12-12
申请号：US306113
申请日：1989-02-06
申请人： Thomas A. Hardy , Edward N. Walsh
发明人： Thomas A. Hardy , Edward N. Walsh
IPC分类号： C07F9/09 , C07F9/40 , C08K5/521 , C08K5/5333 , D06M13/292
CPC分类号： D06M13/292 , C07F9/091 , C07F9/093 , C07F9/4006 , C08K5/521 , C08K5/5333 , C23F11/1673
摘要： There are disclosed multiphosphorus-containing compounds comprising phosphonate-containing or phosphate-containing phosphate esters. The compounds can be prepared by: (a) reacting a phosphonate-containing or phosphate-containing alcohol with phosphorus pentoxide following by reaction with an epoxide, (b) reacting a phosphonate-containing or phosphate-containing alcohol with a phosphorus oxyhalide, hydrolyzing any phosphorus halogen bonds and then reacting the resulting phosphoric acid derivative with an epoxide, (c) transesterifying a phosphonate-containing or phosphate-containing alcohol with a dialkyl phosphite, oxidizing the resulting compound to yield a phosphoric acid derivative and reacting the phosphoric acid derivative with an epoxide. The compounds are useful as flame retardant additives for polyurethanes and textiles.
摘要翻译：公开了包含含膦酸酯或磷酸酯的磷酸酯的含有多磷的化合物。化合物可以通过以下方法制备：（a）通过与环氧化物反应，使含膦酸酯或含磷酸酯的醇与五氧化二磷反应，（b）使含膦酸酯或含磷酸盐的醇与磷酰卤反应，将任何磷卤素键，然后使所得磷酸衍生物与环氧化物反应，（c）将含膦酸酯或含磷酸酯的醇与亚磷酸二烷基酯酯交换，氧化所得化合物以产生磷酸衍生物，并使磷酸衍生物与环氧化物。该化合物可用作聚氨酯和纺织品的阻燃添加剂。

52. 发明授权

US4845271A Process for the preparation of omega-unsaturated carboxylic acids 失效
标题翻译：制备ω-不饱和羧酸的方法
公开(公告)号：US4845271A
公开(公告)日：1989-07-04
申请号：US7041
申请日：1987-01-27
申请人： Stanley B. Mirviss
发明人： Stanley B. Mirviss
IPC分类号： C07C17/16 , C07C51/347 , C07C51/353
CPC分类号： C07C51/347 , C07C17/16 , C07C51/353
摘要： An improved method for the synthesis of omega-unsaturated carboxylic acids is disclosed which precludes double bond migration or hydrogenation in order to prepare a high purity product necessary for high resolution in forming a resist by electron beam microlithography. This result can be obtained by a coupling reaction between a Grignard reagent of an unsaturated organochloride compound as defined in the application with a halo magnesium salt of a long chain organic acid.
摘要翻译：公开了一种用于合成ω-不饱和羧酸的改进方法，其排除双键迁移或氢化，以便通过电子束微光刻法制备高分辨率形成抗蚀剂所需的高纯度产物。该结果可以通过本申请中定义的不饱和有机氯化物化合物的格氏试剂与长链有机酸的卤代镁盐的偶联反应获得。

53. 发明授权

US4844006A Apparatus to provide a vaporized reactant for chemical-vapor deposition 失效
标题翻译：提供用于化学气相沉积的汽化反应物的装置
公开(公告)号：US4844006A
公开(公告)日：1989-07-04
申请号：US164677
申请日：1988-03-07
申请人： Theron V. Page, Jr. , Thomas F. Boydston , John G. Posa
发明人： Theron V. Page, Jr. , Thomas F. Boydston , John G. Posa
IPC分类号： C23C16/448
CPC分类号： C23C16/4481
摘要： An apparatus to provide a vaporized reactant for chemical-vapor deposition is disclosed. The apparatus employs a heated quartz reactant reservoir, quartz lines, a quartz valve and, optionally, a purge system. The apparatus may also include a quartz refill reservoir and heating means for the quartz lines. The purge system may be a vacuum purge system.
摘要翻译：公开了提供用于化学气相沉积的汽化反应物的装置。该装置采用加热的石英反应物储存器，石英管线，石英阀和任选的清洗系统。该装置还可以包括用于石英管线的石英填充储存器和加热装置。吹扫系统可以是真空吹扫系统。

54. 发明授权

US4765866A Energy ray curing of arylsiloxane/silicate compositions and subsequent etching thereof 失效
标题翻译：芳基硅氧烷/硅酸盐组合物的能量射线固化和其后的蚀刻
公开(公告)号：US4765866A
公开(公告)日：1988-08-23
申请号：US101522
申请日：1987-09-28
申请人： George E. Whitwell , John H. Deatcher , Andrea Leone-Bay
发明人： George E. Whitwell , John H. Deatcher , Andrea Leone-Bay
IPC分类号： C09D183/04 , H01L21/311 , H01L21/312 , B44C1/22 , B29C37/00
CPC分类号： H01L21/3121 , C09D183/04 , H01L21/31111
摘要： The etching of cured arylsiloxane/silicate resin coatings with HF is improved if the curing of said coatings, prior to etching, comprises curing with energy ray irradiation.
摘要翻译：如果在蚀刻之前所述涂层的固化包括用能量射线照射固化，则用HF蚀刻固化的芳基硅氧烷/硅酸盐树脂涂层得到改善。

55. 发明授权

US4764634A Preparation of organic phosphinites 失效
标题翻译：有机亚磷酸盐的制备
公开(公告)号：US4764634A
公开(公告)日：1988-08-16
申请号：US900948
申请日：1986-08-27
申请人： Jeffrey E. Telschow
发明人： Jeffrey E. Telschow
IPC分类号： B01J31/00 , B01J31/02 , C07B61/00 , C07F9/46
CPC分类号： C07F9/46
摘要： The instant invention is directed to a process for producing organic phosphinites by a process wherein a disubstituted halophosphine is reacted with a primary, secondary, or tertiary alcohol or phenol in the presence of a tertiary amine base wherein the reaction is conducted at a temperature of from about ambient. The invention is particularly directed to the preparation of isopropyl diphenylphosphinite.
摘要翻译：本发明涉及通过一种方法制备有机亚磷酸盐的方法，其中二取代的卤代膦在叔胺碱的存在下与伯，仲或叔醇或酚反应，其中反应在关于环境。本发明特别涉及二苯基磷酸异丙酯的制备。

56. 发明授权

US4758620A Blend of solvent and arylsiloxane interlayer dielectric materials 失效
标题翻译：溶剂和芳基硅氧烷层间电介质材料的混合
公开(公告)号：US4758620A
公开(公告)日：1988-07-19
申请号：US69087
申请日：1987-07-02
申请人： George E. Whitwell , John H. Deatcher
发明人： George E. Whitwell , John H. Deatcher
IPC分类号： C08J3/09 , C09D183/04 , C08K5/01
CPC分类号： C08J3/092 , C08K5/01 , C09D183/04 , C08J2383/04
摘要： Striation-free interlayer dielectric films of good reflectivity are formed by spin-coating a solution comprising 1,2,4-trimethylbenzene solvent containing a dissolved arylsiloxane oligomer or polymer capable of forming an interlayer dielectric film.
摘要翻译：通过旋涂包含含有能够形成层间电介质膜的溶解的芳基硅氧烷低聚物或聚合物的1,2,4-三甲基苯溶剂的溶液来形成良好的反射率的无条纹层间绝缘膜。

57. 发明授权

US4751009A Fabric softeners comprising stable single phase clear solutions of anionic and cationic surfactants 失效
标题翻译：织物柔软剂包括阴离子和阳离子表面活性剂的稳定的单相澄清溶液
公开(公告)号：US4751009A
公开(公告)日：1988-06-14
申请号：US81924
申请日：1987-08-05
申请人： Gene R. Damaso , Eugene R. Carr
发明人： Gene R. Damaso , Eugene R. Carr
IPC分类号： C11D1/14 , C11D1/18 , C11D1/22 , C11D1/28 , C11D1/62 , C11D1/65 , C11D3/00 , D06M13/44
CPC分类号： C11D3/0015 , C11D1/65 , C11D1/14 , C11D1/18 , C11D1/22 , C11D1/28 , C11D1/62
摘要： A fabric softener composition comprising a stable, clear single phase solution of an anionic surfactant having an alkyl radical containing at least eight carbon atoms, a cationic surfactant, water and an effective amount of propylene glycol and an alkali metal salt of benzene, toluene or xylene sulfonate. The fabric softener may be highly concentrated and has the property that when added to a detergent solution it imparts a fabric softening effect but does not lessen the detergency of the solution.
摘要翻译：一种织物柔软剂组合物，其包含具有至少8个碳原子的烷基的阴离子表面活性剂的稳定且透明的单相溶液，阳离子表面活性剂，水和有效量的丙二醇和苯，甲苯或二甲苯的碱金属盐磺酸盐。织物柔软剂可以是高度浓缩的，并且具有当添加到洗涤剂溶液中时赋予织物柔软效果但不降低溶液的去污力的性质。

58. 发明授权

US4713489A Preparation of N-substituted arylsulfonamides 失效
标题翻译： N-取代芳基磺酰胺的制备
公开(公告)号：US4713489A
公开(公告)日：1987-12-15
申请号：US820876
申请日：1986-01-16
申请人： Gail H. Birum , Richard F. Jansen
发明人： Gail H. Birum , Richard F. Jansen
IPC分类号： C07C311/15 , C07C143/79
CPC分类号： C07C311/15
摘要： N-substituted arylsulfonamides which comprises the steps of (a) reacting an aryl hydrocarbon with chlorosulfonic acid to form a crude chlorosulfonation reaction product, (b) adding said crude reaction product to a mixture comprising an aliphatic amine, an alkali or alkaline earth metal hydroxide and water to form an amidation reaction mixture, (c) maintaining the temperature of the amidation reaction mixture at between about 50.degree. C. and 100.degree. C. and the pH at above about 7 with stirring for a period of time of up to about 2 hours, and optionally (d) separating the resulting N-substituted arylsulfonamide from the amidation reaction product.
摘要翻译： N-取代的芳基磺酰胺，其包括以下步骤：（a）使芳基烃与氯磺酸反应以形成粗氯磺化反应产物，（b）将所述粗反应产物加入到包含脂族胺，碱金属或碱土金属氢氧化物和水以形成酰胺化反应混合物，（c）将酰胺化反应混合物的温度保持在约50℃至100℃，pH高于约7，同时搅拌一段时间至多约 2小时，任选地（d）从酰胺化反应产物中分离得到的N-取代的芳基磺酰胺。

59. 发明授权

US2687358A Stabilized soil and a process of stabilizing it 失效
标题翻译：稳定土壤和稳定土壤的过程
公开(公告)号：US2687358A
公开(公告)日：1954-08-24
申请号：US20048450
申请日：1950-12-12
申请人： ICI LTD
发明人： ALLBERRY EDWARD C , HAWKINS STANLEY W
IPC分类号： C09K17/14
CPC分类号： C09K17/14 , Y10S106/90 , Y10S260/14

60. 发明授权

US5089303A Blend of solvent and photocurable arylsiloxane materials 失效
标题翻译：溶剂与光固化芳基硅氧烷材料的混合
公开(公告)号：US5089303A
公开(公告)日：1992-02-18
申请号：US342150
申请日：1989-04-24
申请人： John H. Deatcher , Eric W. Burkhardt
发明人： John H. Deatcher , Eric W. Burkhardt
IPC分类号： C08J3/09 , C09D183/04 , H01L23/532
CPC分类号： C08J3/095 , C09D183/04 , H01L23/5329 , C08J2383/04 , H01L2924/0002
摘要： Good quality films can be formed on a substrate by coating a substrate with a solution comprising an alkoxy alkanol solvent containing a dissolved photocurable arylsiloxane oligomer or polymer. Phenyl siloxane/silicate compositions can be used to form photocurable films on substrates for use as dielectric films, protective coatings, and the like.
摘要翻译：通过用包含溶解的可光固化的芳基硅氧烷低聚物或聚合物的烷氧基烷醇溶剂的溶液涂布基材，可以在基材上形成优质的膜。苯基硅氧烷/硅酸盐组合物可用于在用作介电膜，保护涂层等的基材上形成光固化膜。

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