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51. 发明申请

US20140309462A1 CATALYTIC FLUORINATION PROCESS OF MAKING HYDROHALOALKANE 有权
标题翻译：催化氟化氢的制备方法
公开(公告)号：US20140309462A1
公开(公告)日：2014-10-16
申请号：US14357345
申请日：2012-11-09
申请人： Mario Joseph NAPPA , Andrew JACKSON , Daniel C. MERKEL
发明人： Mario Joseph Nappa , Andrew Jackson , Daniel C. Merkel
IPC分类号： C07C17/087 , C07C17/25 , C07C17/38
CPC分类号： C07C17/38 , B01J27/12 , B01J27/135 , B01J37/26 , C07C17/087 , C07C17/206 , C07C17/25 , C07C19/10 , C07C21/18
摘要： The present disclosure provides a fluorination process which involves reacting a hydrohaloalkene of the formula RfC—Cl═CH2 with HF in a reaction zone in the presence of a fluorination catalyst selected from the group consisting of TaF5 and TiF4 to produce a product mixture containing a hydrohaloalkane of the formula RfCFClCH3, wherein Rf is a perfluorinated alkyl group.
摘要翻译：本公开提供了一种氟化方法，其涉及在选自TaF 5和TiF 4的氟化催化剂的存在下，在反应区中使式RfC-Cl = CH 2的氢卤代烯烃与HF反应，以产生含有氢卤代烷烃的产物混合物式RfCFClCH 3，其中Rf是全氟化烷基。

52. 发明授权

US08633339B2 Blowing agents for forming foam comprising unsaturated fluorocarbons 有权
标题翻译：用于形成包含不饱和碳氟化合物的泡沫的发泡剂
公开(公告)号：US08633339B2
公开(公告)日：2014-01-21
申请号：US11591400
申请日：2006-11-01
申请人： Joseph Anthony Creazzo , Mario Joseph Nappa , Allen Capron Sievert , Ekaterina N. Swearingen
发明人： Joseph Anthony Creazzo , Mario Joseph Nappa , Allen Capron Sievert , Ekaterina N. Swearingen
IPC分类号： C07C21/18
CPC分类号： C08J9/146 , B01F17/0085 , C03C23/0075 , C07C21/18 , C08G18/4208 , C08G18/4883 , C08G2101/0025 , C08J9/0019 , C08J9/144 , C08J2205/05 , C08J2205/052 , C08J2325/06 , C08J2375/06 , C08J2375/08 , C10M105/52 , C10M107/38 , C10M147/04 , C10M169/04 , C10M169/041 , C10M177/00 , C10M2211/022 , C10M2211/06 , C10M2213/04 , C10M2213/06 , C10N2230/06 , C10N2230/22 , C10N2240/20 , C10N2240/204 , C10N2250/121 , C10N2270/00 , C11D3/245 , C11D3/43 , C11D7/5018 , C11D11/0023 , C11D11/0029 , C11D11/0035 , C11D11/0047 , C23G5/02803 , C23G5/02825 , G11B5/71 , G11B5/725 , G11B5/8408 , G11B23/505
摘要： Disclosed herein are blowing agents comprising fluorocarbons and/or hydrofluorocarbons useful in foamable compositions. Also disclosed are methods for forming a foam comprising the aforementioned blowing agents.
摘要翻译：本文公开了包含可用于可发泡组合物的碳氟化合物和/或氢氟烃的发泡剂。还公开了形成包含上述发泡剂的泡沫体的方法。

53. 发明授权

US08535555B2 Epoxide and fluorinated epoxide stabilizers for fluoroolefins 有权
公开(公告)号：US08535555B2
公开(公告)日：2013-09-17
申请号：US12377454
申请日：2007-08-31
申请人： Andrew Edward Feiring , Viacheslav A. Petrov , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Thomas J. Leck , Jon Lee Howell
发明人： Andrew Edward Feiring , Viacheslav A. Petrov , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Thomas J. Leck , Jon Lee Howell
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/10 , C09K2205/102 , C09K2205/104 , C09K2205/11 , C09K2205/126 , C09K2205/132 , C09K2205/134 , C09K2205/24 , F25B39/02
摘要： The present invention relates to compositions comprising at least one fluoroolefin and an effective amount of stabilizer that may be an epoxide, fluorinated epoxide or oxetane, or a mixture thereof with other stabilizers. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers, and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.

54. 发明授权

US08487145B2 Catalysts and process to manufacture 2,3,3,3-tetrafluoropropene 有权
标题翻译：催化剂和制备2,3,3,3-四氟丙烯的方法
公开(公告)号：US08487145B2
公开(公告)日：2013-07-16
申请号：US13417582
申请日：2012-03-12
申请人： Mario Joseph Nappa , Andrew Jackson
发明人： Mario Joseph Nappa , Andrew Jackson
IPC分类号： C07C17/00
CPC分类号： C07C17/25 , B01J23/26 , B01J35/1019 , C07C21/18
摘要： Disclosed is a process for the manufacture of 2,3,3,3-tetrafluoropropene comprising: (a) contacting 1,1,1,2,3-pentafluoropropane with a catalyst comprised of chromium (III) oxide having a surface area of at least 150 m2/g and having an alkali metal loading of at least 7 milligrams of alkali metal per 100 square meters of catalyst surface area, to produce a product mixture comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride; and (b) recovering said 2,3,3,3-tetrafluoropropene from the product mixture produced in (a).
摘要翻译：公开了一种制备2,3,3,3-四氟丙烯的方法，包括：（a）将1,1,1,2,3-五氟丙烷与由表面积为至少150m2 / g，并且每100平方米的催化剂表面积具有至少7毫克碱金属的碱金属负荷，以产生包含2,3,3,3-四氟丙烯和氟化氢的产物混合物; 和（b）从（a）中制备的产物混合物回收所述2,3,3,3-四氟丙烯。

55. 发明授权

US08394286B2 Thiol and thioether stabilizers for fluoroolefins 失效
标题翻译：用于氟烯烃的硫醇和硫醚稳定剂
公开(公告)号：US08394286B2
公开(公告)日：2013-03-12
申请号：US12377708
申请日：2007-08-31
申请人： Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli
发明人： Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/126
摘要： The present disclosure relates to compositions comprising at least one fluoroolefin and an effective amount of a stabilizer comprising at least one thiol or thioether, or mixtures thereof. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.
摘要翻译：本公开涉及包含至少一种氟烯烃和有效量的包含至少一种硫醇或硫醚的稳定剂或其混合物的组合物。稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。

56. 发明授权

US08349213B2 Solvent compositions comprising unsaturated fluorinated hydrocarbons 有权
标题翻译：包含不饱和氟化烃的溶剂组合物
公开(公告)号：US08349213B2
公开(公告)日：2013-01-08
申请号：US13153599
申请日：2011-06-06
申请人： Mario Joseph Nappa , Melodie A. Schweitzer , Allen Capron Sievert , Ekaterina N. Swearingen
发明人： Mario Joseph Nappa , Melodie A. Schweitzer , Allen Capron Sievert , Ekaterina N. Swearingen
IPC分类号： B01F1/00 , B05D5/08
CPC分类号： C08J9/146 , B01F17/0085 , C03C23/0075 , C07C21/18 , C08G18/4208 , C08G18/4883 , C08G2101/0025 , C08J9/0019 , C08J9/144 , C08J2205/05 , C08J2205/052 , C08J2325/06 , C08J2375/06 , C08J2375/08 , C10M105/52 , C10M107/38 , C10M147/04 , C10M169/04 , C10M169/041 , C10M177/00 , C10M2211/022 , C10M2211/06 , C10M2213/04 , C10M2213/06 , C10N2230/06 , C10N2230/22 , C10N2240/20 , C10N2240/204 , C10N2250/121 , C10N2270/00 , C11D3/245 , C11D3/43 , C11D7/5018 , C11D11/0023 , C11D11/0029 , C11D11/0035 , C11D11/0047 , C23G5/02803 , C23G5/02825 , G11B5/71 , G11B5/725 , G11B5/8408 , G11B23/505
摘要： This invention relates to cleaning compositions comprising unsaturated fluorinated hydrocarbons. The invention further relates to use of said cleaning compositions in methods to clean, degrease, deflux, dewater, and deposit fluorolubricant. The invention further relates to novel unsaturated fluorinated hydrocarbons and their use as cleaning compositions and in the methods listed above.
摘要翻译：本发明涉及包含不饱和氟化烃的清洁组合物。本发明还涉及所述清洁组合物在清洗，脱脂，除油，脱水和沉积氟橄榄油的方法中的用途。本发明还涉及新型不饱和氟化烃及其作为清洁组合物和上述方法的用途。

57. 发明申请

US20120318828A1 AEROSOL PROPELLANTS COMPRISING UNSATURATED FLUOROCARBONS 有权
标题翻译：包含不饱和氟化物的航空动力燃料
公开(公告)号：US20120318828A1
公开(公告)日：2012-12-20
申请号：US13594007
申请日：2012-08-24
申请人： Mario Joseph Nappa , Joseph Anthony Creazzo , Allen Capron Sievert , Ekaterina N. Swearingen
发明人： Mario Joseph Nappa , Joseph Anthony Creazzo , Allen Capron Sievert , Ekaterina N. Swearingen
IPC分类号： B65D83/14
CPC分类号： C09K3/30 , A61K9/124
摘要： Disclosed herein are propellants comprising fluorocarbons and/or hydrofluorocarbons. Also disclosed are sprayable compositions comprising the propellants.
摘要翻译：本文公开了包含碳氟化合物和/或氢氟烃的推进剂。还公开了包含推进剂的可喷雾组合物。

58. 发明申请

US20120172638A1 SYNTHESIS OF 1234YF BY SELECTIVE DEHYDROCHLORINATION OF 244BB 有权
标题翻译：通过244BB的选择性脱氢合成合成1234YF
公开(公告)号：US20120172638A1
公开(公告)日：2012-07-05
申请号：US13172987
申请日：2011-06-30
申请人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
发明人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
IPC分类号： C07C17/23 , C07C21/18
CPC分类号： C07C17/25 , B01J23/26 , B01J37/0036 , B01J37/038 , C07C21/18
摘要： Disclosed is a process for the manufacture of 2,3,3,3-tetrafluoropropene comprising: (a) contacting 1,1,1,2,tetrafluoro-2-chloropropane with a catalyst comprised of chromium (III) oxide, and at least 1% of an alkali metal, to produce a product mixture comprising 2,3,3,3-tetrafluoropropene; and (b) recovering said 2,3,3,3-tetrafluoropropene from the product mixture produced in step (a) above.
摘要翻译：公开了一种制备2,3,3,3-四氟丙烯的方法，其包括：（a）将1,1,1,2，四氟-2-氯丙烷与由氧化铬（III）组成的催化剂和至少 1％的碱金属，以制备包含2,3,3,3-四氟丙烯的产物混合物; 和（b）从上述步骤（a）中制备的产物混合物中回收所述2,3,3,3-四氟丙烯。

59. 发明申请

US20120085110A1 TERPENE, TERPENOID, AND FULLERENE STABILIZERS FOR FLUOROOLEFINS 有权
标题翻译： TERPENE，TERPENOID和富勒烯稳定剂
公开(公告)号：US20120085110A1
公开(公告)日：2012-04-12
申请号：US13325966
申请日：2011-12-14
申请人： JON LEE HOWELL , Velliyur Nott Mallikarjuna Rao , Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Ekaterina N. Swearingen , Andrew Edward Feiring
发明人： JON LEE HOWELL , Velliyur Nott Mallikarjuna Rao , Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Ekaterina N. Swearingen , Andrew Edward Feiring
IPC分类号： F25D31/00 , F28D15/00 , C07C21/18 , C09K5/04 , B82Y30/00
CPC分类号： C09K5/045 , C09K2205/126
摘要： The present invention relates to compositions comprising at least one fluoroolefin and an effective amount of stabilizer that may be a terpene, terpenoid or fullerene; or a mixture of a terpene, terpenoid or fullerene with other stabilizers. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers, and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.
摘要翻译：本发明涉及包含至少一种氟烯烃和有效量的可以是萜烯，萜烯或富勒烯的稳定剂的组合物; 或萜烯，萜烯或富勒烯与其他稳定剂的混合物。稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。

60. 发明授权

US07982073B2 Catalytic production processes for making tetrafluoropropenes and pentafluoropropenes 有权
标题翻译：用于制备四氟丙烯和五氟丙烯的催化生产方法
公开(公告)号：US07982073B2
公开(公告)日：2011-07-19
申请号：US12373594
申请日：2007-07-11
申请人： Mario Joseph Nappa , Velliyur Nott Mallikarjuna Rao
发明人： Mario Joseph Nappa , Velliyur Nott Mallikarjuna Rao
IPC分类号： C07C17/25
CPC分类号： B01J27/132 , B01J23/26 , B01J35/1014 , B01J37/26 , C07C17/25 , Y02P20/582 , C07C21/18
摘要： A process is disclosed for making CF3CF═CHF. The process involves contacting at least one hexafluoropropane selected from the group consisting of CF3CF2CH2F and CF3CHFCHF2 with a chromium oxyfluoride catalyst in a reactor to obtain a product mixture comprising CF3CF═CHF, and recovering CF3CF═CHF from the product mixture.A process is disclosed for making CF3CH═CHF. The process involves contacting CF3CH2CHF2 with a chromium oxyfluoride catalyst in a reactor to obtain a product mixture comprising CF3CH═CHF, and recovering CF3CH═CHF from the product mixture.A process is disclosed for making CF3CF═CH2. The process involves contacting CF3CF2CH3 with a chromium oxyfluoride catalyst in a reactor to obtain a product mixture comprising CF3CF═CH2, and recovering CF3CF═CH2 from the product mixture.
摘要翻译：公开了一种制备CF 3 CF = CHF的方法。该方法包括在反应器中使至少一种选自CF 3 CF 2 CH 2 F和CF 3 CHFCHF 2的六氟丙烷与氟氧化铬催化剂接触，以获得包含CF 3 CF = CHF的产物混合物，并从产物混合物中回收CF 3 CF = CHF。公开了一种制造CF3CH = CHF的方法。该方法包括在反应器中将CF 3 CH 2 CHF 2与氟氧化铬催化剂接触以获得包含CF 3 CH = CHF的产物混合物，并从产物混合物中回收CF 3 CH = CHF。公开了制备CF 3 CF = CH 2的方法。该方法包括在反应器中将CF 3 CF 2 CH 3与氟氧化铬催化剂接触以获得包含CF 3CF≡CH2的产物混合物，并从产物混合物中回收CF 3 CF = CH 2。

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