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51. 发明申请

US20110034743A1 BASE OIL COMPOSITION COMPRISING OLIGOMERIZED OLEFINS 有权
标题翻译：包含低聚烯烃的基础油组合物
公开(公告)号：US20110034743A1
公开(公告)日：2011-02-10
申请号：US12538752
申请日：2009-08-10
申请人： Saleh Elomari , Stephen J. Miller
发明人： Saleh Elomari , Stephen J. Miller
IPC分类号： C07C11/00
CPC分类号： C10M107/06 , C10G50/02 , C10G2300/1092 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2400/10 , C10M107/10 , C10M2205/0245 , C10N2220/022 , C10N2220/023 , C10N2270/00 , C10M2205/0285
摘要： We provide a base oil, comprising one or more oligomerized olefins, wherein the base oil has: d. a kinematic viscosity at 100° C. greater than 2.9 mm2/s; d. a viscosity index from 25 to 90; and f. a cloud point less than −55° C. We provide a base oil made by oligomerizing propylene in an ionic liquid catalyst, where the base oil has a viscosity index from 25 to 90 and the base oil is colorless.We also provide a base oil made by oligomerizing an olefin feed comprising propylene in an acidic alkyl-pyridinium chloroaluminate ionic liquid, wherein the base oil has a viscosity index at 100° C. greater than 2.9 mm2/s, a viscosity index from 25 to 90, and a cloud point less than −55° C.
摘要翻译：我们提供一种基础油，其包含一种或多种低聚烯烃，其中所述基础油具有：d。在100℃下的运动粘度大于2.9mm 2 / s; d。粘度指数为25〜90; 和f。浊点小于-55℃。提供通过在离子液体催化剂中使丙烯低聚而制得的基础油，其中基础油的粘度指数为25至90，基础油为无色。我们还提供通过在酸性烷基 - 氯铬酸吡啶鎓离子液体中将包含丙烯的烯烃进料低聚制得的基础油，其中基油在100℃下的粘度指数大于2.9mm 2 / s，粘度指数为25至 90，浊点小于-55℃

52. 发明申请

US20110034742A1 TUNING AN OLIGOMERIZING STEP TO PRODUCE A BASE OIL WITH SELECTED PROPERTIES 有权
标题翻译：调整低成本步骤生产具有选定属性的基础油
公开(公告)号：US20110034742A1
公开(公告)日：2011-02-10
申请号：US12538746
申请日：2009-08-10
申请人： Saleh Elomari , Stephen J. Miller
发明人： Saleh Elomari , Stephen J. Miller
IPC分类号： C07C2/08 , C07C2/16 , C07C2/02 , C07C11/00
CPC分类号： C10G50/02 , C10G2300/1088 , C10G2300/1092 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2300/80 , C10G2400/10
摘要： A process, comprising: a. selecting a kinematic viscosity; b. feeding an olefin feed comprising a propylene to an oligomerization zone; c. tuning an oligomerizing step to produce a base oil having the kinematic viscosity and a viscosity index from 20 to 90. A process, comprising: a. selecting a kinematic viscosity that is greater than 20 mm2/s; b. feeding a feed comprising propylene to an oligomerization zone; and c. adding a Brönsted acid to produce a base oil. A process, comprising tuning a step in an oligomerization zone comprising a propylene and an ionic liquid catalyst to produce a base oil having: a. a high kinematic viscosity; b. a viscosity index from 25 to 90; and c. a low pour point. A base oil, comprising oligomerized olefins, wherein the base oil has: a. a high kinematic viscosity; b. a viscosity index from 25 to 90; and c. a low pour point.
摘要翻译：一个过程，包括：a。选择运动粘度; b。将包含丙烯的烯烃进料进料到低聚区; C。调节低聚步骤以产生具有20至90的运动粘度和粘度指数的基础油。一种方法，包括：a。选择大于20 mm2 / s的运动粘度; b。将含有丙烯的进料进料到低聚区; 和c。加入布朗斯台德酸生产基础油。一种方法，包括调整包含丙烯和离子液体催化剂的低聚区中的步骤以产生具有以下成分的基础油：a。高运动粘度; b。粘度指数为25〜90; 和c。低倾点。一种基础油，其包含低聚烯烃，其中所述基础油具有：a。高运动粘度; b。粘度指数为25〜90; 和c。低倾点。

53. 发明授权

US07824658B2 Method of making ultrasmall crystal MTT molecular sieves 有权
标题翻译：制造超小晶体MTT分子筛的方法
公开(公告)号：US07824658B2
公开(公告)日：2010-11-02
申请号：US11945001
申请日：2007-11-26
申请人： Stephen J. Miller
发明人： Stephen J. Miller
IPC分类号： C01B39/04
CPC分类号： C01B39/48 , C01B37/00 , C01B37/02
摘要： A method for preparing a crystalline molecular sieve having MTT framework topology and crystallite sizes of about 150 to about 600 Angstroms, comprising: a. preparing a reaction mixture comprising, in terms of mole ratios, the following. YO2/W2O330-40 R+/YO20.06-0.12 OH−/YO20.20-0.26 K+/YO20.09-0.15 and an amount of water not substantially in excess of the amount required to cause and maintain crystallization, wherein Y is silicon, germanium or mixtures thereof; W is aluminum, boron, gallium, iron or mixtures thereof; and R+ is a diisopropylimidazolium cation, and b. heating said reaction mixture at crystallization conditions and in the absence of an external liquid phase for sufficient time to form a crystallized material containing crystals of the molecular sieve. Also, a method to make the shaped ultrasmall crystal MTT molecular sieve, and a method to form the molecular sieve using a particular order of addition of components.
摘要翻译：一种制备具有约150至约600埃的MTT框架拓扑结构和微晶尺寸的结晶分子筛的方法，包括：a。制备以摩尔比计的下列反应混合物。 YO 2 / W 2 O 3 30-40 R + / YO 2 0.06-0.12 OH- / YO 2 0.20-0.26 K + / YO 2 0.09-0.15和基本上不超过引起和保持结晶所需量的水的量，其中Y是硅，锗或其混合物; W是铝，硼，镓，铁或其混合物; 和R +是二异丙基咪唑鎓阳离子，和b。在结晶条件下和在不存在外部液相的条件下加热所述反应混合物足够的时间以形成含有分子筛晶体的结晶物质。另外，制造成形超小晶体MTT分子筛的方法，以及使用特定添加成分的顺序形成分子筛的方法。

54. 发明授权

US07723556B2 Process to make base oil from thermally cracked waxy feed using ionic liquid catalyst 有权
标题翻译：使用离子液体催化剂从热裂解蜡质进料制备基础油的方法
公开(公告)号：US07723556B2
公开(公告)日：2010-05-25
申请号：US12498254
申请日：2009-07-06
申请人： Saleh Elomari , Russell R. Krug , Stephen J. Miller
发明人： Saleh Elomari , Russell R. Krug , Stephen J. Miller
IPC分类号： C07C2/68 , C07C2/70 , C07C2/60
CPC分类号： C10G50/02 , C07C2527/125 , C07C2531/02 , C10G2400/10 , C10M105/04 , C10M109/02 , C10M127/02 , C10M177/00 , C10M2205/0285 , C10N2220/022 , C10N2220/023 , C10N2230/02 , C10N2270/00 , C10M2203/0206
摘要： We provide a process for making a base oil, comprising: a) selecting an olefin feed produced by thermal cracking of a waxy feed; b) oligomerizing the olefin feed in an ionic liquid oligomerization zone at a set of oligomerization conditions to form an oligomer; and c) alkylating the oligomer in the presence of an isoparaffin, in an ionic liquid alkylation zone, at a set of alkylation conditions to form an alkylated oligomeric product having a kinematic viscosity at 100° C. of 6.9 mm2/s or greater, a VI of at least 134, and a Bromine Number of less than 4. We provide a process to make base oil from an olefin feed produced in a FCC unit. We also provide a process to make two or more viscosity grades of base oil from an olefin feed produced by thermal cracking of a waxy feed.
摘要翻译：我们提供一种制备基础油的方法，包括：a）选择通过蜡质进料的热裂解产生的烯烃原料; b）在一组低聚条件下使离子液体低聚区中的烯烃进料低聚以形成低聚物; 和c）在异烷烃存在下，在离子液体烷基化区中，在一组烷基化条件下烷基化低聚物以形成在100℃下的运动粘度为6.9mm 2 / s或更大的烷基化低聚产物， VI至少为134，溴值小于4.我们提供了一种从FCC装置中生产的烯烃原料制备基础油的方法。我们还提供一种通过蜡质进料的热裂解产生的烯烃原料制备两种或更多种粘度等级的基础油的方法。

55. 发明申请

US20100029998A1 Synthesis of a Crystalline Silicoaluminophosphate 审中-公开
标题翻译：结晶硅铝磷酸盐的合成
公开(公告)号：US20100029998A1
公开(公告)日：2010-02-04
申请号：US12181652
申请日：2008-07-29
申请人： Stephen J. Miller
发明人： Stephen J. Miller
IPC分类号： C07C5/02 , C01B25/36 , B01J27/185
CPC分类号： B01J29/85 , B01J23/42 , B01J35/002 , B01J2229/18 , C01B37/08 , C01B39/54 , C10G45/60 , C10G47/16 , C10G49/08 , C10G65/12 , C10G2300/1014 , C10G2300/1022 , C10G2300/1037 , C10G2400/10 , Y02P30/20
摘要： The present invention is a method for synthesizing non-zeolitic molecular sieves which have a three dimensional microporous framework comprising [AlO2] and [PO2] units. In preparing the reaction mixture, a surfactant is used, coupled with non-aqueous impregnation to prevent acid sites from being destroyed by water during Pt impregnation. The superior SAPO exhibits higher activity and selectivity especially in catalytic hydroisomerization of waxy feeds, due to the presence of medium-sized silica islands distributed throughout the SAPO.
摘要翻译：本发明是一种合成非沸石分子筛的方法，其具有包含[AlO 2]和[PO 2]单元的三维微孔骨架。在制备反应混合物时，使用表面活性剂，与非水性浸渍相结合，以防止在Pt浸渍过程中酸性部位被水破坏。特别是在蜡质进料的催化加氢异构化中，上层SAPO表现出更高的活性和选择性，这是由于分布在整个SAPO中的中等尺寸二氧化硅岛的存在。

56. 发明申请

US20090084026A1 Production of Biofuels and Biolubricants From a Common Feedstock 有权
公开(公告)号：US20090084026A1
公开(公告)日：2009-04-02
申请号：US11862704
申请日：2007-09-27
申请人： Stephen J. Miller
发明人： Stephen J. Miller
IPC分类号： C10L1/19 , B01J14/00
CPC分类号： C10G3/46 , C10G3/50 , C10G45/58 , C10G2300/1011 , C10G2300/1014 , C11C3/003 , C11C3/006 , Y02P30/20
摘要： The present invention is directed to methods and systems for processing triglyceride-containing, biologically-derived oils, wherein such processing comprises conversion of triglycerides to free fatty acids and the separation of these fatty acids by saturation type. Such separation by type enables the efficient preparation of both lubricants and transportation fuels from a common source using a single integrated method and/or system.

57. 发明授权

US07374657B2 Production of low sulfur, moderately aromatic distillate fuels by hydrocracking of combined Fischer-Tropsch and petroleum streams 失效
标题翻译：通过联合费托和石油流的加氢裂化生产低硫，中等芳烃馏分燃料
公开(公告)号：US07374657B2
公开(公告)日：2008-05-20
申请号：US11019455
申请日：2004-12-23
申请人： Stephen J. Miller , Dennis J. O'Rear
发明人： Stephen J. Miller , Dennis J. O'Rear
IPC分类号： C10L1/04 , C10G42/02
CPC分类号： C10L1/08 , C10G2/32 , C10G45/02 , C10G47/00 , C10G47/12 , C10G65/12 , C10G2300/1022 , C10G2300/1037 , C10G2300/202 , C10G2300/30 , C10G2300/301 , C10G2300/302 , C10G2300/307 , C10G2300/308 , C10G2300/4018 , C10G2400/04
摘要： The present invention relates to distillate fuels or distillate fuel blend stocks comprising a blend of a Fischer-Tropsch derived product and a petroleum derived product that is hydrocracked under conditions to preserve aromatics. The resulting distillate fuel product is a low sulfur, moderately aromatic distillate fuel. The resulting distillate fuel or distillate fuel blend stock exhibits excellent properties, including good seal swell, density, and thermal stability. The present invention also relates to processes for making these distillate fuels or distillate fuel blend stocks.
摘要翻译：本发明涉及馏出物燃料或馏出物燃料共混物原料，其包含费 - 托衍生产物和石油衍生产物的混合物，其在保持芳族化合物的条件下进行加氢裂化。所得的馏出物燃料产物是低硫，中等芳香族馏分燃料。所得的馏出物燃料或馏出物燃料共混物料具有优异的性能，包括良好的密封膨胀，密度和热稳定性。本发明还涉及制备这些馏出物燃料或馏出燃料混合原料的方法。

58. 发明授权

US07268094B2 Mixed matrix membrane with super water washed silica containing molecular sieves and methods for making and using the same 有权
标题翻译：含有分子筛的超级水洗二氧化硅的混合基质膜及其制备和使用方法
公开(公告)号：US07268094B2
公开(公告)日：2007-09-11
申请号：US10643555
申请日：2003-08-18
申请人： Stephen J. Miller , Lun-Teh Yuen
发明人： Stephen J. Miller , Lun-Teh Yuen
IPC分类号： B01J35/02
CPC分类号： B01J20/28026 , B01D67/0079 , B01D67/0088 , B01D69/148 , B01D71/024 , B01D71/027 , B01D71/028 , B01D2325/26 , B01J20/28033
摘要： The present invention provides a method for preparing silica containing molecular sieves which may be mixed with an organic polymer to create a mixed matrix membrane. Further, this invention includes a method of making such a mixed matrix membrane and the membrane itself. A process for separating component gases from a mixture using the subject mixed matrix membrane is also described. The method for preparing silica containing molecular sieves comprises super water washing silica containing molecular sieves to produce water washed molecular sieves which are substantially free of surface remnants. Super water washing also ideally lowers the concentration of alkali metals in the molecular sieves. The water washed sieves are sufficiently free of surface remnants such that when the water washed sieves are subjected to a Sieve Wash Conductivity Test, a wash filtrate is produced having a conductivity of less than 110 micro mhos/cm, more preferably less than 80 micro mhos/cm, even more preferably less than 50 micro mhos/cm, and most preferably less than 30 micro mhos/cm. It is believed that super washing the sieves to this degree will enhance, compared to conventional preparation techniques, the ability of the molecular sieves to bond with an organic polymer to form a highly selective and permeable mixed matrix membrane.
摘要翻译：本发明提供了一种制备含二氧化硅的分子筛的方法，该方法可与有机聚合物混合以产生混合基质膜。此外，本发明包括制造这种混合基质膜和膜本身的方法。还描述了使用主题混合基质膜从混合物中分离组分气体的方法。制备含二氧化硅的分子筛的方法包括含有分子筛的超级水洗二氧化硅，以产生基本上没有表面残留物的水洗分子筛。超级水洗也有利于降低分子筛中碱金属的浓度。水洗筛足够地没有表面残留物，使得当洗涤过的筛子进行筛洗电导率测试时，产生电导率小于110微摩尔/厘米，更优选小于80微摩尔的洗涤滤液 / cm，甚至更优选小于50微摩尔/厘米，最优选小于30微摩尔/厘米。据认为，与常规制备技术相比，超级洗涤这种程度的筛子将增强分子筛与有机聚合物结合以形成高选择性和可渗透的混合基质膜的能力。

59. 发明授权

US06755900B2 Crosslinked and crosslinkable hollow fiber mixed matrix membrane and method of making same 有权
标题翻译：交联和交联中空纤维混合基质膜及其制备方法
公开(公告)号：US06755900B2
公开(公告)日：2004-06-29
申请号：US10323090
申请日：2002-12-18
申请人： William J. Koros , David Wallace , John D. Wind , Stephen J. Miller , Claudia Staudt-Bickel , De Q. Vu
发明人： William J. Koros , David Wallace , John D. Wind , Stephen J. Miller , Claudia Staudt-Bickel , De Q. Vu
IPC分类号： B01D6908
CPC分类号： B01D67/0093 , B01D53/22 , B01D53/228 , B01D63/02 , B01D63/021 , B01D69/08 , B01D69/141 , B01D71/64 , B01D71/82 , B01D2313/18 , B01D2323/30 , Y02C20/20 , Y10S55/05
摘要： A composition of and a method of making high performance mixed matrix hollow fiber membranes is described. The membranes have a high resistance to plasticization by use of a predetermined amount of crosslinking. The preferred polymer material for the membrane is a polyimide polymer continuous phase comprising ester crosslinks and a molecular sieve material dispersed within the polymer continuous phase. The resultant mixed matrix hollow fiber membrane exhibits a high permeance of CO2 in combination with a high CO2/CH4 selectivity. Another embodiment provides a method of making the mixed matrix hollow fiber membrane from a monesterified polymer followed by final crosslinking after hollow fiber formation.
摘要翻译：描述了制备高性能混合基质中空纤维膜的组合物和方法。膜通过使用预定量的交联具有高的增塑性。用于膜的优选聚合物材料是包含酯交联的聚酰亚胺聚合物连续相和分散在聚合物连续相中的分子筛材料。所得到的混合基质中空纤维膜表现出高的CO 2渗透性和高CO 2 / CH 4选择性。另一个实施方案提供了从单酯化聚合物制备混合基质中空纤维膜，然后在中空纤维形成之后进行最终交联的方法。

60. 发明授权

US06723889B2 Process for producing a highly paraffinic diesel fuel having a high iso-paraffin to normal paraffin mole ratio 失效
标题翻译：具有高异链烷烃与正常石蜡摩尔比的高度链烷烃类柴油燃料的方法
公开(公告)号：US06723889B2
公开(公告)日：2004-04-20
申请号：US09765585
申请日：2001-01-22
申请人： Stephen J. Miller , Arthur John Dahlberg , Kamala R. Krishna , Russell R. Krug
发明人： Stephen J. Miller , Arthur John Dahlberg , Kamala R. Krishna , Russell R. Krug
IPC分类号： C07C522
CPC分类号： C10L1/08 , C10G2400/04 , Y10S208/95
摘要： A process for producing a diesel fuel having at least 70% C10+ paraffins, wherein the iso-paraffin to normal paraffin mole ratio is 5:1 and higher. This diesel fuel is produced by from a feed containing at least 40% C10+ normal paraffins and at least 20% C26+ normal paraffins. It is produced by contacting that feed in an isomerization/cracking reaction zone a feed with a catalyst comprising a SAPO-11 and platinum in the presence of hydrogen (hydrogen:feed ratio of from 1,000 to 10,000 SCFB) at a temperature of from 340° C. to 420° C., a pressure of from 100 psig to 600 psig, and a liquid hourly space velocity of from 0.1 hr−1 to 1.0 hr−1.
摘要翻译：一种制备具有至少70％的C 10 +烷烃的柴油的方法，其中异链烷烃与正常的石蜡摩尔比为5:1以上。该柴油由含有至少40％C 10 +正链烷烃和至少20％C26 +正链烷烃的原料生产。通过在异构化/裂化反应区中将进料与含有SAPO-11和铂的催化剂在氢气存在下（氢气：进料比为1,000至10,000SCFB），使该进料在340℃的温度下接触而制备至420℃，压力为100psig至600psig，液时空速为0.1小时-1.0小时-1。

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