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51. 发明授权

US07902309B2 Process and catalyst system for polydiene production 有权
标题翻译：聚二烯生产工艺和催化剂体系
公开(公告)号：US07902309B2
公开(公告)日：2011-03-08
申请号：US12390857
申请日：2009-02-23
申请人： Steven Luo , Jason T. Poulton , Daniel F. Graves
发明人： Steven Luo , Jason T. Poulton , Daniel F. Graves
IPC分类号： C08F4/44
CPC分类号： C08F36/04 , C08F2/06 , C08F4/545
摘要： Compositions and polydiene production processes involving catalyst systems comprising at least one lanthanide-containing compound, at least one alkylating agent, at least one halogen source, and at least one N,N-dihydrocarbylhydroxylamine.
摘要翻译：包含至少一种含镧系元素的化合物，至少一种烷基化剂，至少一种卤素源和至少一种N，N-二烃基羟胺的催化剂体系的组合物和聚二烯生产方法。

52. 发明申请

US20100216956A1 PROCESS AND CATALYST SYSTEM FOR POLYDIENE PRODUCTION 有权
标题翻译：聚氨酯生产工艺和催化剂体系
公开(公告)号：US20100216956A1
公开(公告)日：2010-08-26
申请号：US12390857
申请日：2009-02-23
申请人： Steven Luo , Jason T. Poulton , Daniel F. Graves
发明人： Steven Luo , Jason T. Poulton , Daniel F. Graves
IPC分类号： C08F4/52 , B01J31/02
CPC分类号： C08F36/04 , C08F2/06 , C08F4/545
摘要： Compositions and polydiene production processes involving catalyst systems comprising at least one lanthanide-containing compound, at least one alkylating agent, at least one halogen source, and at least one N,N-dihydrocarbylhydroxylamine.
摘要翻译：包含至少一种含镧系元素的化合物，至少一种烷基化剂，至少一种卤素源和至少一种N，N-二烃基羟胺的催化剂体系的组合物和聚二烯生产方法。

53. 发明授权

US07781503B2 Modified asphalt binders and asphalt paving compositions 有权
标题翻译：改性沥青结合料和沥青铺路料
公开(公告)号：US07781503B2
公开(公告)日：2010-08-24
申请号：US11644557
申请日：2006-12-22
申请人： William L. Hergenrother , Peter W. Boerner , Christine Rademacher , Daniel F. Graves , Timothy P. Reece , Herbert L. Wissel
发明人： William L. Hergenrother , Peter W. Boerner , Christine Rademacher , Daniel F. Graves , Timothy P. Reece , Herbert L. Wissel
IPC分类号： C08L95/00
CPC分类号： C08L95/00 , C08L25/10 , C08L53/02 , C08L2666/74 , C08L53/00 , C08L2666/24 , C08L2666/04
摘要： A process for preparing a modified asphalt binder composition, the process comprising mixing asphalt, an unsaturated polymer, and phosphorus pentasulfide to form a modified asphalt composition.
摘要翻译：一种制备改性沥青粘合剂组合物的方法，该方法包括混合沥青，不饱和聚合物和五硫化二磷以形成改性沥青组合物。

54. 发明申请

US20100029850A1 Adducts Of Metathesis Polymers And Preparation Thereof 有权
标题翻译：复分解聚合物的加合物及其制备方法
公开(公告)号：US20100029850A1
公开(公告)日：2010-02-04
申请号：US12535449
申请日：2009-08-04
申请人： James H. Pawlow , William L. Hergenrother , Mark N. Dedecker , Daniel F. Graves
发明人： James H. Pawlow , William L. Hergenrother , Mark N. Dedecker , Daniel F. Graves
IPC分类号： C08L67/02
CPC分类号： C08G61/08 , C08F8/46 , C08F283/14 , C08G2261/1426 , C08G2261/3322 , C08G2261/418 , F03B17/02 , Y02E10/20 , C08F222/06 , C08F110/14 , C08F132/06
摘要： Adducts of an unsaturated metathesis polymer or interpolymer and an unsaturated diacid anhydride. A process for producing adducts of an unsaturated metathesis polymer or interpolymer and unsaturated diacid anhydride.
摘要翻译：不饱和分解聚合物或互聚物和不饱和二酸酐的加合物。一种制备不饱和分解聚合物或互聚物和不饱和二酸酐的加合物的方法。

55. 发明授权

US06596798B1 Preparation of low hysteresis rubber by reacting a lithium polymer with oxazoline compounds 有权
公开(公告)号：US06596798B1
公开(公告)日：2003-07-22
申请号：US10012842
申请日：2001-11-05
申请人： Christine M. Rademacher , William L. Hergenrother , Daniel F. Graves , James D. Ulmer
发明人： Christine M. Rademacher , William L. Hergenrother , Daniel F. Graves , James D. Ulmer
IPC分类号： C08K506
CPC分类号： B60C1/00 , B60C1/0025 , B60C15/06 , C08C19/44 , C08L19/006
摘要： The present invention provides a method of forming a functionalized polymer. The method includes the steps of providing a living lithium polymer and terminating the polymer with an oxazoline compound selected from an organic halide oxazoline and a branched or unbranched vinyl oxazoline compound. The present invention also provides a compounded rubber article wherein carbon black is compounded with a terminated rubber that is the reaction product of a living lithium polymer and such oxazoline compounds.

56. 发明授权

US06417270B1 Means of producing high diblock content thermoplastic elastomers with functional termination 有权
标题翻译：具有功能终止的高二嵌段含量的热塑性弹性体的方法
公开(公告)号：US06417270B1
公开(公告)日：2002-07-09
申请号：US09757140
申请日：2001-01-09
申请人： Mark H. Wollum , Daniel F. Graves
发明人： Mark H. Wollum , Daniel F. Graves
IPC分类号： C08F25506
CPC分类号： C08F297/04
摘要： A process of preparing a diblock/triblock composition in a single reaction vessel includes reacting a first monomer, such as styrene, with a first portion of an anionic catalyst in a suitable solvent to form a first polymer block of the triblock. A second step includes adding a second monomer, such as butadiene (when the first monomer is styrene). This forms a second block of the triblock and a first block of the diblock. A further addition of the first monomer completes the diblock and triblock interpolymers. At least a portion of the diblock and/or triblock interpolymers are functionally terminated with a functional terminating agent, such as cyclohexene oxide or isopropanol, to provide the blocks with a functional group. The functional group and the proportion of the interpolymers functionally terminated are selected to provide desired adhesive properties for a particular application.
摘要翻译：在单个反应容器中制备二嵌段/三嵌段组合物的方法包括使第一单体如苯乙烯与阴离子催化剂的第一部分在合适的溶剂中反应以形成三嵌段的第一聚合物嵌段。第二步包括加入第二单体，如丁二烯（当第一单体是苯乙烯时）。这形成了三次锁的第二块，并且形成了二块的第一块。另外加入第一单体可完成二嵌段和三嵌段互聚物。二嵌段和/或三嵌段互聚物的至少一部分用功能性终止剂如环己烯氧化物或异丙醇在功能上终止，以提供具有官能团的嵌段。选择官能团和功能性终止的互聚物的比例以为特定应用提供期望的粘合剂性质。

57. 发明授权

US06313232B1 Continuous addition of tin halides to solution SBR 有权
标题翻译：将锡卤锡连续添加到溶液SBR中
公开(公告)号：US06313232B1
公开(公告)日：2001-11-06
申请号：US09324669
申请日：1999-06-03
申请人： David M. Roggeman , Daniel F. Graves , William J. Kern , Yasuo Horikawa
发明人： David M. Roggeman , Daniel F. Graves , William J. Kern , Yasuo Horikawa
IPC分类号： C08F842
CPC分类号： C08C19/44 , C08F8/42 , C08F212/08
摘要： A method of continuously polymerizing a conjugated diene monomer and a vinyl aromatic hydrocarbon monomer in a hydrocarbon solvent by using an organolithium initiator, adding to the polymerization mixture a tin compound and again adding a tin compound after the polymerization mixture has been withdrawn from the polymerization vessel. The resulting diene polymers possess a significantly reduced Payne Effect and a substantial reduction (over 10%) in tan delta at 50° C. which results in tires having decreased hysteresis loss, excellent wear resistance and rolling resistance and good wet skid resistance.
摘要翻译：通过使用有机锂引发剂在烃溶剂中连续聚合共轭二烯单体和乙烯基芳族烃单体的方法，在聚合混合物从聚合容器中取出之后，向聚合混合物中加入锡化合物并再次加入锡化合物。所得二烯聚合物在50℃下具有显着降低的佩恩效应和显着降低（超过10％）的tanδ，这导致轮胎具有降低的滞后损耗，优异的耐磨性和滚动阻力以及良好的抗湿滑性。

58. 发明授权

US5659056A Stabilization of siloxane terminated polymers 失效
标题翻译：硅氧烷封端的聚合物的稳定化
公开(公告)号：US5659056A
公开(公告)日：1997-08-19
申请号：US630298
申请日：1996-04-10
申请人： William L. Hergenrother , David M. Roggeman , Daniel F. Graves , Mark L. Stayer, Jr.
发明人： William L. Hergenrother , David M. Roggeman , Daniel F. Graves , Mark L. Stayer, Jr.
IPC分类号： C08C19/00 , C08C2/04 , C08C19/44 , C08F8/00 , C07F7/08
CPC分类号： C08C2/04 , C08C19/44
摘要： The present invention relates to a method of reducing hydrolysis and coupling of substituents of siloxane end capped polymers containing hydrolyzable substituents during contact with water. The Mooney viscosity of siloxane terminated polymers is stabilized during such contact by treating the polymer with a stabilizing amount of stabilizing agent selected from the group consisting of: an acid, an acyl halide, methane sulfonic acid, toluene sulfonic acid, sulfuryl chloride, thionylchloride, phosgene, carbon dioxide, sulfur dioxide, sulfur trioxide, SOCl.sub.2 and SO.sub.2 Cl.sub.2, prior to contacting the siloxane terminated polymer with water.
摘要翻译：本发明涉及在与水接触期间减少含有可水解取代基的硅氧烷封端聚合物的水解和偶联的方法。硅烷封端的聚合物的门尼粘度在这种接触期间通过用稳定量的稳定剂处理聚合物而稳定，稳定剂选自：酸，酰卤，甲磺酸，甲苯磺酸，磺酰氯，亚硫酰氯，在将硅氧烷封端的聚合物与水接触之前，将光气，二氧化碳，二氧化硫，三氧化硫，SOCl 2和SO 2 Cl 2。

59. 发明授权

US5593701A Rubber curing bladders having self release or low adhesion to curing adhesion to curing or cured hydrocarbon rubbers 失效
标题翻译：具有自身释放或低粘合性以固化或固化烃橡胶的粘合剂的橡胶固化气囊
公开(公告)号：US5593701A
公开(公告)日：1997-01-14
申请号：US623283
申请日：1996-03-28
申请人： Daniel F. Graves , William L. Hergenrother
发明人： Daniel F. Graves , William L. Hergenrother
IPC分类号： C08L9/06 , B29C33/02 , B29C33/50 , B29C33/62 , B29C35/02 , B29C43/10 , B29C43/36 , B29D30/26 , B29K21/00 , B29L30/00 , B60C1/00 , C08G81/02 , C08L9/02 , C08L13/00 , C08L15/00 , C08L23/16 , C08L23/18 , C08L23/22 , C08L23/26 , C08L23/28 , C08L51/00 , C08L67/00 , C08L69/00 , C08L71/00 , B29C35/00 , B29D30/00
CPC分类号： B29D30/0654 , B29C33/505 , B29C33/62 , B29C43/3642 , B60C1/00 , B60C1/0008 , C08G81/024 , C08G81/025 , C08L13/00 , C08L15/00 , C08L23/16 , C08L23/26 , C08L23/283 , C08L9/02 , B29D2030/0655 , B29L2022/025 , B29L2030/00 , C08L67/00 , C08L69/00 , C08L71/00
摘要： Hydrocarbon polymers with grafts of polyethers, polylactones, or polyesters from the reaction of phosgene with glycols having from 1 to 4 carbon atoms are disclosed as having good release properties or low adhesion to hydrocarbon rubber materials. The hydrocarbon backbone polymers include EPDM, hydrogenated polybutadiene, and hydrogenated poly(styrene-butadiene) all said polymers having pendant succinic anhydride groups or brominated p-methylstyrene-isobutylene copolymers. The above-referenced graft copolymers along with butadiene-acrylonitrile rubber or epichlorohydrin polymers or copolymers are described as useful polymers to make self-release curing bladders or sleeves for use in making molded articles such as pneumatic tires.
摘要翻译：公开了与光气与具有1至4个碳原子的二醇反应的聚醚，聚内酯或聚酯的接枝物的烃聚合物具有良好的脱模性能或对烃类橡胶材料的低附着性。烃主链聚合物包括EPDM，氢化聚丁二烯和氢化聚（苯乙烯 - 丁二烯），所有所述聚合物都具有琥珀酸酐基侧基或溴化对甲基苯乙烯 - 异丁烯共聚物。上述参考的接枝共聚物以及丁二烯 - 丙烯腈橡胶或表氯醇聚合物或共聚物被描述为用于制造用于制造模制品如充气轮胎的自释放固化气囊或套筒的有用聚合物。

60. 发明授权

US5385459A Rubber curing bladders having self release or low adhesion to curing or cured hydrocarbon rubbers 失效
标题翻译：对固化或固化的烃橡胶具有自我释放或低粘附性的橡胶固化囊
公开(公告)号：US5385459A
公开(公告)日：1995-01-31
申请号：US222154
申请日：1994-04-04
申请人： Daniel F. Graves , William L. Hergenrother
发明人： Daniel F. Graves , William L. Hergenrother
IPC分类号： C08L9/06 , B29C33/02 , B29C33/50 , B29C33/62 , B29C35/02 , B29C43/10 , B29C43/36 , B29D30/26 , B29K21/00 , B29L30/00 , B60C1/00 , C08G81/02 , C08L9/02 , C08L13/00 , C08L15/00 , C08L23/16 , C08L23/18 , C08L23/22 , C08L23/26 , C08L23/28 , C08L51/00 , C08L67/00 , C08L69/00 , C08L71/00 , B29C35/00 , B29D30/00
CPC分类号： B29D30/0654 , B29C33/505 , B29C33/62 , B29C43/3642 , B60C1/00 , B60C1/0008 , C08G81/024 , C08G81/025 , C08L13/00 , C08L15/00 , C08L23/16 , C08L23/26 , C08L23/283 , C08L9/02 , B29D2030/0655 , B29L2022/025 , B29L2030/00 , C08L67/00 , C08L69/00 , C08L71/00
摘要： Hydrocarbon polymers with grafts of polyethers, polylactones, or polyesters from the reaction of phosgene with glycols having from 1 to 4 carbon atoms are disclosed as having good release properties or low adhesion to hydrocarbon rubber materials. The hydrocarbon backbone polymers include EPDM, hydrogenated polybutadiene, and hydrogenated poly(styrene-butadiene) all said polymers having pendant succinic anhydride groups or brominated p-methylstyrene-isobutylene copolymers. The above-referenced graft copolymers along with butadiene-acrylonitrile rubber or epichlorohydrin polymers or copolymers are described as useful polymers to make self-release curing bladders or sleeves for use in making molded articles such as pneumatic tires.
摘要翻译：公开了与光气与具有1至4个碳原子的二醇反应的聚醚，聚内酯或聚酯的接枝物的烃聚合物具有良好的脱模性能或对烃类橡胶材料的低附着性。烃主链聚合物包括EPDM，氢化聚丁二烯和氢化聚（苯乙烯 - 丁二烯），所有所述聚合物都具有琥珀酸酐基侧基或溴化对甲基苯乙烯 - 异丁烯共聚物。上述参考的接枝共聚物以及丁二烯 - 丙烯腈橡胶或表氯醇聚合物或共聚物被描述为用于制造用于制造模制品如充气轮胎的自释放固化气囊或套筒的有用聚合物。

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