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51. 发明授权

US5247046A RTV silicone rubber compositions and cured products 失效
标题翻译： RTV硅橡胶组合物和固化产品
公开(公告)号：US5247046A
公开(公告)日：1993-09-21
申请号：US987681
申请日：1992-12-09
申请人： Toshio Takago , Shinichi Sato , Noriyuki Koike , Takashi Matsuda
发明人： Toshio Takago , Shinichi Sato , Noriyuki Koike , Takashi Matsuda
IPC分类号： C08L83/05 , C08L83/07 , C08L83/14
CPC分类号： C08L83/14 , Y10S528/901
摘要： A RTV silicone rubber composition comprising (A) an organopolysiloxane composed predominantly of a silalkylenesiloxane unit and containing an aliphatic unsaturated group in a molecule, (B) an organohydrogenpolysiloxane having at least two SiH groups in a molecule, and (C) a platinum group compound cures into a transparent elastomer which is increased in rubbery strength without adding a filler.

52. 发明授权

US5194648A Fluorinated carboxylic acid derivatives and methods for making 失效
标题翻译：氟化羧酸衍生物及其制备方法
公开(公告)号：US5194648A
公开(公告)日：1993-03-16
申请号：US562321
申请日：1990-08-03
申请人： Shinichi Satoh , Noriyuki Koike , Hideki Fujii
发明人： Shinichi Satoh , Noriyuki Koike , Hideki Fujii
IPC分类号： C07C51/04 , C07C51/58 , C07C59/60 , C07F7/18 , C08G65/22 , C08G65/32
CPC分类号： C07F7/1828 , C07C59/60 , C07F7/182 , C07F7/1896
摘要： Novel fluorinated carboxylic acid derivatives of the general formula: ##STR1## wherein Rf is a divalent perfluoroalkyl or perfluoropolyether group and Z is halogen, hydroxyl or triorganosiloxy are useful intermediate for the synthesis of various fluorinated compounds. Compounds [I-i] wherein Z in formula [I] is F are prepared by reacting acid fluoride-terminated compounds of the formula: ##STR2## with an alkali fluoride and further with an allyl halide. Compounds [I-ii] wherein Z in formula [I] is a halogen are preparred by reacting compounds [I-i] with lithium halide. Compounds [I-iii] wherein Z in formula [I] is OH are prepared through hydrolysis of compounds [I-ii]. Compounds [I-iv] wherein Z in formula [I] is triorganosiloxy are prepared by reacting compounds [I-iii] with a triorganosilylating agent.

53. 发明授权

US08492478B2 Curable perfluoropolyether gel composition and gel product produced by using cured perfluoropolyether gel composition 有权
标题翻译：可固化的全氟聚醚凝胶组合物和通过使用固化的全氟聚醚凝胶组合物制备的凝胶产物
公开(公告)号：US08492478B2
公开(公告)日：2013-07-23
申请号：US13180966
申请日：2011-07-12
申请人： Kenichi Fukuda , Noriyuki Koike , Mikio Shiono
发明人： Kenichi Fukuda , Noriyuki Koike , Mikio Shiono
IPC分类号： C08F290/14 , C08F283/00 , A61K9/70 , B60C1/00 , C08G18/77 , C08K5/24
CPC分类号： C08G65/007 , C08G65/336 , C08G2650/48 , C08L71/00
摘要： A curable perfluoropolyether gel composition is provided. The composition comprises (A) a straight chain fluorine-containing polymer represented by the following formula (1): (B) a polyfluoromonoalkenyl compound containing one alkenyl group per molecule and having a perfluoropolyether structure in its backbone, (C) an organosilicon compound containing at least two hydrogen atoms bonded to the silicon atom per molecule, and (D) a hydrosilylation catalyst. The composition can be produced into a cured product having excellent heat resistance, solvent resistance, chemical resistance, weatherability, releasability, water repellency, oil repellency, and the like as well as an improved acid resistance.
摘要翻译：提供可固化的全氟聚醚凝胶组合物。该组合物包含（A）由下式（1）表示的直链含氟聚合物：（B）每分子含有一个烯基并在其主链上具有全氟聚醚结构的多氟单链烯基化合物，（C）含有每分子与硅原子键合的至少两个氢原子，和（D）氢化硅烷化催化剂。可以将该组合物制成具有优异的耐热性，耐溶剂性，耐化学性，耐候性，脱模性，防水性，拒油性等的固化产品，以及改进的耐酸性。

54. 发明授权

US08247592B2 Method of preparing disilanol compound and method of storing disilanol compound 有权
标题翻译：制备二硅烷醇化合物的方法和二硅烷醇化合物的储存方法
公开(公告)号：US08247592B2
公开(公告)日：2012-08-21
申请号：US13111647
申请日：2011-05-19
申请人： Yasunori Sakano , Takashi Matsuda , Noriyuki Koike
发明人： Yasunori Sakano , Takashi Matsuda , Noriyuki Koike
IPC分类号： C07F7/08
CPC分类号： C07F7/0836 , C08G65/007 , C08G65/336
摘要： Disclosed is a method of storing a fluorine-containing disilanol compound represented by the following formula (3) in the presence of a tertiary amine in such an amount that a molar ratio of the tertiary amine to a silanol group of the fluorine-containing disilanol compound ranges from 0.001 to 20, HO—Z—R1—Rf—R1—Z—OH (3) wherein Rf is a divalent fluorinated hydrocarbon group or a divalent fluorinated polyether group, R1 may be the same with or different from each other and is a substituted or unsubstituted divalent hydrocarbon group which may have at least one atom selected from the group consisting of oxygen, nitrogen, silicon, and sulfur atoms, and Z is a group represented by the following formula (2) —SiR2R3— (2) wherein R2 and R3 may be the same with or different from each other and are monovalent organic groups.
摘要翻译：本发明公开了一种在叔胺存在下，使下式（3）表示的含氟二硅烷醇化合物的存在量使得含氟二硅烷醇化合物的叔胺与硅烷醇基的摩尔比范围为0.001〜20，HO-Z-R1-Rf-R1-Z-OH（3）其中Rf为二价氟化烃基或二价氟化聚醚基，R 1可以相同或不同，可以具有选自氧，氮，硅和硫原子中的至少一个原子的取代或未取代的二价烃基，Z是由下式（2）-SiR 2 R 3 - （2）表示的基团，其中 R2和R3可以彼此相同或不同，并且是一价有机基团。

55. 发明授权

US08143359B2 Organic silicone compound 有权
标题翻译：有机硅化合物
公开(公告)号：US08143359B2
公开(公告)日：2012-03-27
申请号：US12620782
申请日：2009-11-18
申请人： Noriyuki Koike , Takashi Matsuda , Hirofumi Kishita
发明人： Noriyuki Koike , Takashi Matsuda , Hirofumi Kishita
IPC分类号： C08F30/08
CPC分类号： C07F7/081
摘要： The purpose of the present invention is to provide an organic silicon compound which has a vinyl group more reactive than those of the conventional organic silicon compounds and can be bonded with another compound.The present organic silicon compound is represented by the following formula (1), wherein R1 is, independently of each other, a vinyl group or an alkyl group having 1 to 4 carbon atoms, R2 is an alkylene group having 3 to 6 carbon atoms, and R3 is, independently of each other, a hydrogen atom or an alkyl group having 1 to 4 carbon atoms and optionally substituted with one or more fluorine atoms.
摘要翻译：本发明的目的是提供一种有机硅化合物，其具有比常规有机硅化合物更具反应活性的乙烯基，并可与另一种化合物结合。本发明的有机硅化合物由下式（1）表示，其中R 1彼此独立地为乙烯基或具有1至4个碳原子的烷基，R 2为具有3至6个碳原子的亚烷基，并且R 3彼此独立地为氢原子或具有1至4个碳原子并且任选被一个或多个氟原子取代的烷基。

56. 发明申请

US20120016081A1 CURABLE PERFLUOROPOLYETHER GEL COMPOSITION AND GEL PRODUCT PRODUCED BY USING CURED PERFLUOROPOLYETHER GEL COMPOSITION 有权
标题翻译：可固化全氟聚醚凝胶组合物和使用固化的全氟聚醚凝胶组合物生产的凝胶产品
公开(公告)号：US20120016081A1
公开(公告)日：2012-01-19
申请号：US13180966
申请日：2011-07-12
申请人： Kenichi Fukuda , Noriyuki Koike , Mikio Shiono
发明人： Kenichi Fukuda , Noriyuki Koike , Mikio Shiono
IPC分类号： C08G65/48 , C08G79/00 , C08G77/00 , C08G69/00
CPC分类号： C08G65/007 , C08G65/336 , C08G2650/48 , C08L71/00
摘要： A curable perfluoropolyether gel composition is provided. The composition comprises (A) a straight chain fluorine-containing polymer represented by the following formula (1): (B) a polyfluoromonoalkenyl compound containing one alkenyl group per molecule and having a perfluoropolyether structure in its backbone, (C) an organosilicon compound containing at least two hydrogen atoms bonded to the silicon atom per molecule, and (D) a hydrosilylation catalyst. The composition can be produced into a cured product having excellent heat resistance, solvent resistance, chemical resistance, weatherability, releasability, water repellency, oil repellency, and the like as well as an improved acid resistance.
摘要翻译：提供可固化的全氟聚醚凝胶组合物。该组合物包含（A）由下式（1）表示的直链含氟聚合物：（B）每分子含有一个烯基并在其主链上具有全氟聚醚结构的多氟单链烯基化合物，（C）含有每分子与硅原子键合的至少两个氢原子，和（D）氢化硅烷化催化剂。可以将该组合物制成具有优异的耐热性，耐溶剂性，耐化学性，耐候性，脱模性，防水性，拒油性等的固化产品，以及改进的耐酸性。

57. 发明授权

US07829649B2 Perfluoropolyether-polyorganosiloxane block copolymer and a surface treatment agent comprising the same 有权
标题翻译：全氟聚醚 - 聚有机硅氧烷嵌段共聚物和包含其的表面处理剂
公开(公告)号：US07829649B2
公开(公告)日：2010-11-09
申请号：US12323282
申请日：2008-11-25
申请人： Yuji Yamane , Noriyuki Koike , Koichi Yamaguchi
发明人： Yuji Yamane , Noriyuki Koike , Koichi Yamaguchi
IPC分类号： C08G77/04
CPC分类号： C08G77/46 , C08L83/12
摘要： A perfluoropolyether-polyorganosiloxane block copolymer represented by the following formula (1), the block copolymer having a number average molecular weight, reduced to polystyrene, of from 2,000 to 20,000, W2-Q-Rf-Q-(W1-Q-Rf-Q)g-W2 (1) wherein Rf is a perfluoropolyether block, W1 is a polyorganosiloxane block having at least one group represented by the following formula (2) wherein X is a hydrolyzable group, R1 is a C1-4 alkyl group or a phenyl group, y is an integer of from 1 to 5, and a is 2 or 3, Q is a C2-12 divalent connecting group which may contain an oxygen atom and/or nitrogen atom, W2 is an organosiloxane residue having a group represented by the aforesaid formula (1), and g is an integer of from 1 to 11.
摘要翻译：由下式（1）表示的全氟聚醚 - 聚有机硅氧烷嵌段共聚物，数均分子量为2,000〜20,000的数均分子量，聚苯乙烯换算为W2-Q-Rf-Q-（W1-Q-Rf- Q）g-W2（1）其中Rf是全氟聚醚嵌段，W1是具有至少一个由下式（2）表示的基团的聚有机硅氧烷嵌段，其中X是可水解基团，R1是C1-4烷基或苯基，y为1〜5的整数，a为2或3，Q为可含有氧原子和/或氮原子的C2-12二价连接基团，W2为具有以下基团的有机硅氧烷残基由上述式（1）表示，g为1〜11的整数。

58. 发明申请

US20070197758A1 Fluorine-containing organopolysiloxane, a surface treatment composition comprising the same and an article treated with the composition 有权
标题翻译：含氟有机聚硅氧烷，包含其的表面处理组合物和用该组合物处理的制品
公开(公告)号：US20070197758A1
公开(公告)日：2007-08-23
申请号：US11657108
申请日：2007-01-24
申请人： Yuii Yamane , Noriyuki Koike , Koichi Yamaguchi , Hirofumi Kishita
发明人： Yuii Yamane , Noriyuki Koike , Koichi Yamaguchi , Hirofumi Kishita
IPC分类号： C08G77/24 , B32B9/04
CPC分类号： C09D183/12 , C08G65/007 , C08G77/48 , Y10T428/31663
摘要： A fluorine-containing organopolysiloxane represented by the following average compositional formula (1) (Z2Q)βRf(QZ1Aα)2-β (1) wherein Rf is a divalent group containing a perfluoroether residue, Q is a divalent organic group, Z1 is a di- to nona-valent organopolysiloxane residue and may contain a silalkylene bond, α is an integer of from 1 to 8, β is a number larger than 0 and smaller than 2, Z2 is a monovalent group represented by the following formula (2) wherein b is an integer of from 1 to 10, R1 may be the same with and different from each other and is an alkyl group having 1 to 4 carbon atoms or a phenyl group, and A is a monovalent group represented by the following formula (3) wherein R2 is an alkyl group having 1 to 4 carbon atoms or a phenyl group, X is a hydrolyzable group, a is 2 or 3, and c is an integer of from 1 to 6.
摘要翻译：由以下平均组成式（1）表示的含氟有机聚硅氧烷<？in-line-formula description =“In-line formula”end =“lead”→>（Z < β（β-β）β（β-β）2-β（1）<β在线公式描述= “直列式”末端=“尾”→其中，Rf是含有全氟醚残基的二价基团，Q是二价有机基团，Z 1是二至少价的有机聚硅氧烷残基并且可以含有亚硅烷基键，α为1〜8的整数，β为大于0且小于2的数，Z 2是由下式（2）表示的一价基团，其中b为1〜10的整数，R 1可以相同也可以不同，为碳原子数为1〜4的烷基或苯基，A为由下式（3）表示的一价基团，其中R 2是具有1至4个碳原子的烷基或ph 烯基，X为水解性基团，a为2或3，c为1〜6的整数。

59. 发明申请

US20070149746A1 Fluorine-containing organopolysiloxane, a surface treatment composition comprising the same and an article treated with the composition 有权
公开(公告)号：US20070149746A1
公开(公告)日：2007-06-28
申请号：US11643988
申请日：2006-12-22
申请人： Yuji Yamane , Noriyuki Koike , Koichi Yamaguchi , Hirofumi Kishita
发明人： Yuji Yamane , Noriyuki Koike , Koichi Yamaguchi , Hirofumi Kishita
IPC分类号： C08G77/24
CPC分类号： C08G77/385 , C07F7/21 , C08G77/50 , Y10T428/31663
摘要： An organopolysiloxane represented by the following general formula (A), (B) or (C) SinR12n+2On−1 (A) SinR12nOn (B) SinR12n+2R2kOn−k (C) wherein R1 may be the same with or different from each other and is a hydrogen atom or a monovalent organic group, R2 is an alkylene group having 2 to 6 carbon atoms, n is an integer of from 2 to 40 and k is an integer of 1 to 3, characterized in that at least two R1's are represented by the following formula (i): wherein X is a hydrolyzable group, R3 is an alkyl group having 1 to 4 carbon atoms or a phenyl group, y is an integer of from 1 to 5 and a is 2 or 3; and one SiR1 bond is represented by the following formula (ii) or one SiOSi bond is replaced with a bond represented by the following formula (iii): SiQRf1 (ii) SiQRf2QSi (iii) wherein Rf1 is a monovalent group containing a perfluoroether residue, Rf is a divalent group containing a perfluoroether residue, and Q is a divalent organic group.

60. 发明授权

US07087673B2 Fluororubber compositions and articles thereof 有权
标题翻译：氟橡胶组合物及其制品
公开(公告)号：US07087673B2
公开(公告)日：2006-08-08
申请号：US10337290
申请日：2003-01-07
申请人： Takashi Matsuda , Yasuhisa Osawa , Noriyuki Koike , Yasunori Sakano
发明人： Takashi Matsuda , Yasuhisa Osawa , Noriyuki Koike , Yasunori Sakano
IPC分类号： C08L27/12 , C08F114/18 , C08K5/14
CPC分类号： C08G65/336 , C08G65/007 , C08K9/06 , C08L71/00
摘要： A crosslinkable fluororubber composition comprising (A) a polymer of the formula: Z-(Rf-Q)n—Rf-Z wherein n is an integer of at least 1, Rf is a divalent perfluoroalkylene or perfluorooxyalkylene radical, Q is a divalent organic radical, and Z is a monovalent organic radical, having a viscosity of at least 1,000 Pa·s at 25° C., (B) a reinforcing filler, and (C) a peroxide crosslinking agent is effectively roll milled and experiences minimal changes of viscosity after milling. Molded parts can be produced on a mass scale.
摘要翻译：一种可交联氟橡胶组合物，其包含（A）下式的聚合物：Z-（R f -Q）n -R f-Z其中n是至少为1的整数，R f是二价全氟亚烷基或全氟氧化烯自由基，Q为二价有机基团，Z为单价有机基团，其在25℃下的粘度至少为1,000Pa.s，（B）增强填料，（C）过氧化物交联剂有效地辊磨，经过磨碎后粘度变化最小。模制件可以大规模生产。

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