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51. 发明授权

US5383942A Fuel composition 失效
标题翻译：燃油组成
公开(公告)号：US5383942A
公开(公告)日：1995-01-24
申请号：US79571
申请日：1993-06-22
申请人： Wei-Yang Su , Sheldon Herbstman , Joseph M. Russo , Robert L. Zimmerman , Michael Cuscurida
发明人： Wei-Yang Su , Sheldon Herbstman , Joseph M. Russo , Robert L. Zimmerman , Michael Cuscurida
IPC分类号： C07C231/10 , C07C237/08 , C07D265/32 , C08G65/331 , C08G65/333 , C10L1/22 , C10L1/222 , C10L1/224 , C10L1/233 , C10L1/10
CPC分类号： C10L1/2225 , C07D265/32 , C08G65/3318 , C08G65/33317 , C10L1/221 , C10L1/2335
摘要： An amido alkanolamine composition obtained by reacting, at a temperature of 10.degree. C.-200.degree. C.:(a) a 4-alkyl-2-morpholinone represented by the formula: ##STR1## in which R represents a monovalent aliphatic radical having from 1 to 10 carbon atoms; and(b) a hydrocarbyl oxypolyoxyalkylene amine represented by the formula ##STR2## in which R' represents an alkyl, an alicyclic or an alkyl-alicyclic radical having from 12 to 30 carbon atoms or ##STR3## wherein R" represents a hydrocarbyl radical having from 4 to 30 carbon atoms, x has a value of from about 5 to 50, and R'" is an ethyl radical or a mixture of methyl and ethyl radicals.
摘要翻译：通过在10℃-200℃的温度下反应获得的酰胺链烷醇胺组合物：（a）由下式表示的4-烷基-2-吗啉酮：其中R表示具有 1至10个碳原子; 和（b）由式“IMAGE”表示的烃基氧基聚氧化烯胺，其中R'表示烷基，具有12至30个碳原子的脂环族或烷基脂环族基团或其中R“表示烃基具有4至30个碳原子，x具有约5至50的值，R“'是乙基或甲基和乙基的混合物。

52. 发明授权

US5286267A Polyether hydroxyethylaminoethyl oxalamide motor fuel detergent additives 失效
标题翻译：聚醚羟乙基氨基乙基草酰胺马达燃油洗涤剂添加剂
公开(公告)号：US5286267A
公开(公告)日：1994-02-15
申请号：US993798
申请日：1992-12-21
申请人： Wei-Yang Su , Sheldon Herbstman , Robert L. Zimmerman , Michael Cuscurida
发明人： Wei-Yang Su , Sheldon Herbstman , Robert L. Zimmerman , Michael Cuscurida
IPC分类号： C07C233/56 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/224 , C10L1/238 , C10L10/00 , C07C233/00
CPC分类号： C10L1/224 , C07C233/56 , C10L1/143 , C10L1/238 , C10L10/04 , C10L10/06 , C10L1/1608 , C10L1/1616 , C10L1/1985
摘要： The present invention provides a novel class of compounds, useful as gasoline detergent additives, which is a polyether hydroxyethylaminoethyl oxalamide represented by the formula ##STR1## where R is a (C.sub.5 -C.sub.25) alkyl group and n is an integer between about 5 and about 20.
摘要翻译：本发明提供一类新颖的化合物，其可用作汽油洗涤剂添加剂，其为式（* CHEMICAL STRUCTURE *）（* CHEMICAL STRUCTURE *）（其中R为（C 5 -C 25）烷基）和 n为约5至约20之间的整数。

53. 发明授权

US5254737A Continuous preparation of secondary amines from nitriles using a two-step process 失效
标题翻译：使用两步法从腈中连续制备仲胺
公开(公告)号：US5254737A
公开(公告)日：1993-10-19
申请号：US583109
申请日：1990-09-17
申请人： Robert L. Zimmerman
发明人： Robert L. Zimmerman
IPC分类号： C07C209/48 , C07C211/07 , C07C209/00
CPC分类号： C07C211/07 , C07C209/48
摘要： A method for producing secondary amines, particularly fatty secondary amines such as ditallowamine from fatty nitriles, such as tallow nitrile over a reduction, hydrogenation catalyst, such as nickel or cobalt, in two steps has been discovered. The reaction gives high selectivity of secondary amine over the coproduced primary and tertiary amines. The first step of the reaction is conducted continuously in the presence of ammonia and hydrogen. The secondary amine proportion is increased by a second stage using the same catalyst as the first stage, but in the absence of ammonia.
摘要翻译：已经发现了两个步骤中产生仲胺，特别是脂肪仲胺如脂肪腈的方法，例如脂肪腈如牛脂腈，还原反应，氢化催化剂如镍或钴。该反应使得仲胺比共制的伯胺和叔胺具有高的选择性。反应的第一步在氨和氢的存在下连续进行。使用与第一阶段相同的催化剂，但在不存在氨的情况下，仲胺比例增加第二阶段。

54. 发明授权

US5218005A Polyurea elastomers made using polyamine/carbonyl adducts as chain extenders 失效
标题翻译：使用聚氨酯/碳酮助剂作为链延长剂制备聚氨酯弹性体
公开(公告)号：US5218005A
公开(公告)日：1993-06-08
申请号：US777847
申请日：1991-10-16
申请人： Robert L. Zimmerman , Dudley J. Primeaux
发明人： Robert L. Zimmerman , Dudley J. Primeaux
IPC分类号： C08G18/10 , C08G18/50 , C08G18/65 , C08G18/76
CPC分类号： C08G18/765 , C08G18/10 , C08G18/503 , C08G2150/50
摘要： Low molecular weight, polyoxyalkylene polyamine reacts with carbonyl compound making polyamine adduct used as chain extender in preparing tack-free, smooth polyurea elastomers, useful in solventless spray coatings.

55. 发明授权

US5216154A Process for the preparation of n-methylmorpholine oxide 失效
标题翻译：制备正甲基吗啉氧化物的方法
公开(公告)号：US5216154A
公开(公告)日：1993-06-01
申请号：US825898
申请日：1992-01-27
申请人： Robert L. Zimmerman
发明人： Robert L. Zimmerman
IPC分类号： C07D295/22 , C07D295/24
CPC分类号： C07D295/24
摘要： N-methylmorpholine oxide which is essentially free from nitrosamine contaminants is prepared by oxidizing a feedstock consisting essentially of N-methylmorpholine with an oxidant consisting essentially of aqueous hydrogen peroxide in an atmosphere consisting essentially of carbon dioxide to thereby form a nitrosamine-free reaction product from which N-methylmorpholine oxide essentially free from nitrosamine can be recovered.

56. 发明授权

US5091585A Continuous preparatin of tertiary aliphatic methyl amines 失效
标题翻译：叔脂肪族甲基胺的连续制备
公开(公告)号：US5091585A
公开(公告)日：1992-02-25
申请号：US631844
申请日：1990-12-21
申请人： Wei-Yang Su , Robert L. Zimmerman
发明人： Wei-Yang Su , Robert L. Zimmerman
IPC分类号： B01J23/86 , C07B61/00 , C07C209/24 , C07C209/26 , C07C211/08
CPC分类号： C07C209/26
摘要： A method for continuous production of tertiary aliphatic methyl amines, particularly fatty aliphatic methyl amines such as di-hydrogenated tallow methyl amine from fatty alkyl amines, such as di-hydrogenated tallow amine over a nickel catalyst has been discovered. The reaction gives high selectivity of tertiary methyl amine over the coproduced secondary amines. The reaction may be conducted continuously in the presence of hydrogen and a formaldehyde source. The formaldehyde source may be selected from the group consisting of formaldehyde alone, formalin, a solution of mixed formaldehyde and paraformaldehyde in methanol and water, trioxane and mixtures thereof. The nickel catalyst may be promoted with copper and/or chromium, in one embodiment.
摘要翻译：已经发现了通过镍催化剂连续生产叔脂肪族甲基胺，特别是脂肪族甲基胺如脂肪烷基胺如二氢化牛油胺的二氢化牛油甲胺的方法。该反应使叔甲基胺的高选择性高于共生产的仲胺。反应可以在氢气和甲醛源的存在下连续进行。甲醛源可以选自单独的甲醛，福尔马林，甲醇和水中的混合甲醛和多聚甲醛的溶液，三恶烷及其混合物。在一个实施方案中，镍催化剂可以用铜和/或铬促进。

57. 发明授权

US4789689A Amine catalyst for urethanes 失效
标题翻译：胺催化剂用于聚氨酯
公开(公告)号：US4789689A
公开(公告)日：1988-12-06
申请号：US113854
申请日：1987-10-29
申请人： Robert L. Zimmerman , Terry L. Renken
发明人： Robert L. Zimmerman , Terry L. Renken
IPC分类号： C08G18/18 , C08J9/00 , C08K9/00
CPC分类号： C08G18/1833
摘要： Covers a method of producing a polyurethane by utilizing specific amine compounds of high activity as a catalyst in reacting an organic polyisocyanate with an organic polyester polyol or polyether polyol in the presence of said catalyst. Said amines fall within the following structural formula: ##STR1## where R.sub.1 and R are lower alkyl and x is 2-4.
摘要翻译：包括在所述催化剂存在下，使有机多异氰酸酯与有机聚酯多元醇或聚醚多元醇反应，利用高活性的特定胺化合物作为催化剂制备聚氨酯的方法。所述胺属于以下结构式：其中R 1和R 2为低级烷基且x为2-4。

58. 发明授权

US4615771A Method of separating bis-(2-aminoethyl)ether from N-(2-methoxyethyl)morpholine by azeotropic distillation and extraction 失效
标题翻译：通过共沸蒸馏和萃取从N-（2-甲氧基乙基）吗啉分离双 - （2-氨基乙基）醚的方法
公开(公告)号：US4615771A
公开(公告)日：1986-10-07
申请号：US818519
申请日：1986-01-13
申请人： Robert L. Zimmerman , Roger G. Duranleau
发明人： Robert L. Zimmerman , Roger G. Duranleau
IPC分类号： C07D295/023 , B01D3/36 , C07D265/32
CPC分类号： C07D295/023
摘要： A method for the separation of bis-(2-aminoethyl)ether from N-(2-methoxyethyl)morpholine via azeotropic distillation using an entrainer such as monoethanolamine is described. The N-(2-methoxyethyl)morpholine is selectively removed by the monoethanolamine. The N-(2-methoxyethyl)morpholine is then separated from the monoethanolamine by liquid-liquid extraction using a non polar hydrocarbon or aromatic extraction solvent and distillation.The N-(2-methoxyethyl)morpholine-monoethanolamine stream previously had no economic use. The separation is now economically effected and the N-(2-methoxyethyl)morpholine used as a polyurethane catalyst.
摘要翻译：描述了通过使用夹带剂如单乙醇胺通过共沸蒸馏从N-（2-甲氧基乙基）吗啉分离双 - （2-氨基乙基）醚的方法。通过单乙醇胺选择性地除去N-（2-甲氧基乙基）吗啉。然后通过使用非极性烃或芳族萃取溶剂的液 - 液萃取将N-（2-甲氧基乙基）吗啉与单乙醇胺分离并蒸馏。 N-（2-甲氧基乙基）吗啉 - 单乙醇胺流以前没有经济用途。现在经济上分离，N-（2-甲氧基乙基）吗啉用作聚氨酯催化剂。

59. 发明授权

US4482743A Hydroxyalkyl bis(dialkylaminoalkyl)amine manufacture 失效
标题翻译：羟烷基双（二烷基氨基烷基）胺制造
公开(公告)号：US4482743A
公开(公告)日：1984-11-13
申请号：US518170
申请日：1983-07-28
申请人： Ernest L. Yeakey , Robert L. Zimmerman
发明人： Ernest L. Yeakey , Robert L. Zimmerman
IPC分类号： C07C215/14 , C07C85/00 , C07C85/02 , C07C85/18
CPC分类号： C07C215/14
摘要： A process for manufacturing hydroxyalkyl bis(dialkylaminoalkyl)amine is disclosed wherein dialkylaminopropylaminopropionitrile is separated from a mixture of dialkylaminopropylaminopropionitrile and bis(dialkylaminoalkyl)amine by adding to the mixture under alkoxylation conditions alkylene oxide sufficient to react with substantially all of the bis(alkylaminoalkyl)amine and then separating the reacted materials by distillation. This process yields very pure hydroxyalkyl bis(dialkylaminoalkyl)amine which is useful as a urethane catalyst.
摘要翻译：公开了制备羟基烷基双（二烷基氨基烷基）胺的方法，其中二烷基氨基丙基氨基丙腈与二烷基氨基丙基氨基丙腈和双（二烷基氨基烷基）胺的混合物通过在烷氧基化条件下向混合物中加入足以与基本上所有的双（烷基氨基烷基）胺反应的烯化氧然后通过蒸馏分离反应的物质。该方法产生非常纯的羟烷基双（二烷基氨基烷基）胺，其可用作氨基甲酸酯催化剂。

60. 发明授权

US4469823A Flexible polyurethane foams made using an aromatic polyester polyol 失效
标题翻译：使用芳族聚酯多元醇制成的柔性聚氨酯泡沫
公开(公告)号：US4469823A
公开(公告)日：1984-09-04
申请号：US518171
申请日：1983-07-28
申请人： Ernest L. Yeakey , Robert L. Zimmerman , Michael E. Brennan
发明人： Ernest L. Yeakey , Robert L. Zimmerman , Michael E. Brennan
IPC分类号： C08G18/40 , C08G18/42 , C08G18/14
CPC分类号： C08G18/4009 , C08G18/4216 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： A method for producing a flexible polyurethane foam from reacting a polyol blend with a polyisocyanate in the presence of a polyurethane formation catalyst is described. The polyol blend contains from 0.5 to 10 wt. % of an aromatic polyester polyol extender typically used in rigid foams. The polyol extender is made from dibasic acids, alkylene glycols and recycled polyethylene terephthalate. Commercial extenders cause flexible foams to shrink, a problem not found in the foams of this invention.
摘要翻译：描述了在聚氨酯形成催化剂存在下使多元醇共混物与多异氰酸酯反应制备柔性聚氨酯泡沫的方法。多元醇共混物含有0.5至10wt。通常用于硬质泡沫的芳族聚酯多元醇增量剂的％。多元醇增量剂由二元酸，亚烷基二醇和再生聚对苯二甲酸乙二醇酯制成。商业增长剂导致柔性泡沫收缩，这在本发明的泡沫中没有发现。

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